α-methyl-o-methoxybenzyl methyl ether

Base Information

Chemical Name:α-methyl-o-methoxybenzyl methyl ether
CAS No.:22800-73-3
Molecular Formula:C₁₀H₁₄O₂
Molecular Weight:166.22
Hs Code.:

Synonyms:α-methyl-o-methoxybenzyl methyl ether

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of α-methyl-o-methoxybenzyl methyl ether

Chemical Property:

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Technology Process of α-methyl-o-methoxybenzyl methyl ether

There total 9 articles about α-methyl-o-methoxybenzyl methyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 67-56-1
methanol

: 579-74-8
2-Methoxyacetophenone

: 22800-73-3
α-methyl-o-methoxybenzyl methyl ether

Guidance literature:: With sodium hydroxide; potassium borohydride; for 4h; Heating;

Reference yield: 77.0%

: 13513-82-1
1-(2-methoxyphenyl)ethanol

: 74-88-4
methyl iodide

: 22800-73-3
α-methyl-o-methoxybenzyl methyl ether

Guidance literature:: 1-(2-methoxyphenyl)ethanol; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 1h; Schlenk technique; Inert atmosphere;

methyl iodide; In tetrahydrofuran; at 20 ℃; for 6h; Cooling;
DOI:10.1002/ejoc.201901592

Reference yield:

: 67-56-1
methanol

: 14804-32-1
2-ethylanisole

: 22800-73-3
α-methyl-o-methoxybenzyl methyl ether

Guidance literature:: With dipotassium hydrogenphosphate; [Ir(2-(2,4-difluorophenyl)-4-(trifluoromethyl)pyridine)₂(5,5'-bis(trifluoromethyl)-2,2'-bipyridine)]PF₆; Cu(TFA)₂(MeCN); In acetonitrile; at 20 ℃; for 72h; Schlenk technique; Inert atmosphere; Irradiation;
DOI:10.1002/anie.201910602