benzyl 2-(S)-[(tert-butoxycarbonyl)amino]-5-(trimethylsilyl)pent-4-ynoate

Base Information

Chemical Name:benzyl 2-(S)-[(tert-butoxycarbonyl)amino]-5-(trimethylsilyl)pent-4-ynoate
CAS No.:1364375-86-9
Molecular Formula:C₂₀H₂₉NO₄Si
Molecular Weight:375.54
Hs Code.:

Synonyms:benzyl 2-(S)-[(tert-butoxycarbonyl)amino]-5-(trimethylsilyl)pent-4-ynoate

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Chemical Property of benzyl 2-(S)-[(tert-butoxycarbonyl)amino]-5-(trimethylsilyl)pent-4-ynoate

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Technology Process of benzyl 2-(S)-[(tert-butoxycarbonyl)amino]-5-(trimethylsilyl)pent-4-ynoate

There total 3 articles about benzyl 2-(S)-[(tert-butoxycarbonyl)amino]-5-(trimethylsilyl)pent-4-ynoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 18243-59-9
(2-bromoethynyl)trimethylsilane

: 108957-20-6,125942-79-2
benzyl 2(S)-<(tert-butoxycarbonyl)amino>-3-iodopropionate

: 1364375-86-9
benzyl 2-(S)-[(tert-butoxycarbonyl)amino]-5-(trimethylsilyl)pent-4-ynoate

Guidance literature:: benzyl 2(S)-<(tert-butoxycarbonyl)amino>-3-iodopropionate; With chloro-trimethyl-silane; zinc; In N,N-dimethyl-formamide; at 20 ℃; for 0.0833333h; Inert atmosphere;

With copper(l) cyanide; lithium chloride; In N,N-dimethyl-formamide; at -20 ℃; for 0.25h; Inert atmosphere;

(2-bromoethynyl)trimethylsilane; In N,N-dimethyl-formamide; at -20 - 20 ℃; for 16h; Inert atmosphere;
DOI:10.1246/bcsj.20140394

Reference yield:

: 75-77-4
chloro-trimethyl-silane

: 18243-59-9
(2-bromoethynyl)trimethylsilane

: copper(l) cyanide

: 108957-20-6,125942-79-2
benzyl 2(S)-<(tert-butoxycarbonyl)amino>-3-iodopropionate

: 1364375-86-9
benzyl 2-(S)-[(tert-butoxycarbonyl)amino]-5-(trimethylsilyl)pent-4-ynoate

Guidance literature:: chloro-trimethyl-silane; copper(l) cyanide; benzyl 2(S)-<(tert-butoxycarbonyl)amino>-3-iodopropionate; With lithium chloride; zinc; In N,N-dimethyl-formamide; at -20 - 20 ℃; Inert atmosphere;

(2-bromoethynyl)trimethylsilane; In N,N-dimethyl-formamide; at -20 - 20 ℃; Inert atmosphere;
DOI:10.1039/c2cc17958j

Reference yield:

: 75-77-4
chloro-trimethyl-silane

: 18163-47-8
iodoethynyltrimethylsilane

: copper(l) cyanide

: 108957-20-6,125942-79-2
benzyl 2(S)-<(tert-butoxycarbonyl)amino>-3-iodopropionate

: 1364375-86-9
benzyl 2-(S)-[(tert-butoxycarbonyl)amino]-5-(trimethylsilyl)pent-4-ynoate

Guidance literature:: chloro-trimethyl-silane; copper(l) cyanide; benzyl 2(S)-<(tert-butoxycarbonyl)amino>-3-iodopropionate; With lithium chloride; zinc; In N,N-dimethyl-formamide; at -20 - 20 ℃; Inert atmosphere;

iodoethynyltrimethylsilane; In N,N-dimethyl-formamide; at -20 - 20 ℃; Inert atmosphere;
DOI:10.1039/c2cc17958j