3,4'-dinitrophenyl sulfone

Base Information

• Chemical Name: 3,4'-dinitrophenyl sulfone
• CAS No.: 34418-85-4
• Molecular Formula: C₁₂H₈N₂O₆S
• Molecular Weight: 308.271
• Mol file: 34418-85-4.mol

Synonyms:3,4'-dinitrophenyl sulfone

Chemical Property of 3,4'-dinitrophenyl sulfone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3,4'-dinitrophenyl sulfone

There total 8 articles about 3,4'-dinitrophenyl sulfone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diphenyl sulfide (139-66-2) → 3,3'-dinitrodiphenyl sulfone (1228-53-1) + 4-nitrophenyl sulfone (1156-50-9) + 1-nitro-2-((3-nitrophenyl)sulfonyl)benzene (34418-84-3) + 3,4'-dinitrophenyl sulfone (34418-85-4)

Guidance literature:

With sulfuric acid; nitric acid; In dichloromethane; at 80 ℃; for 12h; Title compound not separated from byproducts;

DOI:10.1055/s-2002-31950

Reference yield:

diphenyl sulfide (139-66-2) → 3,3'-dinitrodiphenyl sulfone (1228-53-1) + 1-nitro-2-((3-nitrophenyl)sulfonyl)benzene (34418-84-3) + 3,4'-dinitrophenyl sulfone (34418-85-4)

Guidance literature:

diphenyl sulfide; With Nitrogen dioxide; In dichloromethane; at -10 ℃; for 0.25h;

With ozone; In dichloromethane; at -10 ℃;

DOI:10.1055/s-2002-31950

Reference yield:

diphenyl sulphone (127-63-9) → 3,3'-dinitrodiphenyl sulfone (1228-53-1) + 1-nitro-2-((3-nitrophenyl)sulfonyl)benzene (34418-84-3) + 3,4'-dinitrophenyl sulfone (34418-85-4)

Guidance literature:

With methylsulfinic acid; Nitrogen dioxide; ozone; In dichloromethane; at -10 ℃; for 4h; Further Variations:; Reagents; Solvents; Temperatures; time; Product distribution;

DOI:10.1055/s-2002-31950

upstream raw materials:

4-nitrophenyl phenyl sulfone

3-nitrophenyl 4′-nitrophenyl sulfide

diphenyl sulfide

diphenyl sulphone

Downstream raw materials:

(3-aminophenyl)(4-aminophenyl)-sulfone

(3,5-dinitro-phenyl)-(4-nitro-phenyl)-sulfone