2-(3-tert-butoxycarbonylamino-4-methoxyphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Base Information

Chemical Name:2-(3-tert-butoxycarbonylamino-4-methoxyphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
CAS No.:262433-23-8
Molecular Formula:C₁₈H₂₈BNO₅
Molecular Weight:349.235
Hs Code.:

Synonyms:2-(3-tert-butoxycarbonylamino-4-methoxyphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Chemical Property of 2-(3-tert-butoxycarbonylamino-4-methoxyphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Technology Process of 2-(3-tert-butoxycarbonylamino-4-methoxyphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

There total 8 articles about 2-(3-tert-butoxycarbonylamino-4-methoxyphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1474060-74-6
3-(N-tert-butyloxycarbonylamino)-4-methoxyphenyl iodide

: 73183-34-3
bis(pinacol)diborane

: 262433-23-8
2-(3-tert-butoxycarbonylamino-4-methoxyphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; In dimethyl sulfoxide; at 80 ℃; for 2h; Inert atmosphere;
DOI:10.1007/s11172-013-0149-3

Reference yield: 40.0%

: 262433-22-7
tert-butyl (5-bromo-2-methoxyphenyl)carbamate

: 73183-34-3
bis(pinacol)diborane

: 262433-23-8
2-(3-tert-butoxycarbonylamino-4-methoxyphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: With potassium acetate; In dimethyl sulfoxide; at 80 ℃; for 4h; Inert atmosphere;

Reference yield:

: 52692-09-8
4-iodo-2-nitroanisole

: 262433-23-8
2-(3-tert-butoxycarbonylamino-4-methoxyphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: Multi-step reaction with 3 steps

1: tin(II) chloride hydrate / ethanol; ethyl acetate / 0.5 h / 70 °C

2: ethanol / 36 h / 20 °C

3: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / dimethyl sulfoxide / 2 h / 80 °C / Inert atmosphere

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tin(II) chloride hydrate; potassium acetate; In ethanol; dimethyl sulfoxide; ethyl acetate;
DOI:10.1007/s11172-013-0149-3