mono-tert-butyl oxalic acid N-methoxy-N-methylamide

Base Information

Chemical Name:mono-tert-butyl oxalic acid N-methoxy-N-methylamide
CAS No.:1218815-84-9
Molecular Formula:C₈H₁₅NO₄
Molecular Weight:189.211
Hs Code.:

Synonyms:mono-tert-butyl oxalic acid N-methoxy-N-methylamide

Suppliers and Price of mono-tert-butyl oxalic acid N-methoxy-N-methylamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 2 raw suppliers

Chemical Property of mono-tert-butyl oxalic acid N-methoxy-N-methylamide

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of mono-tert-butyl oxalic acid N-methoxy-N-methylamide

There total 5 articles about mono-tert-butyl oxalic acid N-methoxy-N-methylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 79-37-8
oxalyl dichloride

: 6638-79-5
N,O-dimethylhydroxylamine*hydrochloride

: 75-65-0
tert-butyl alcohol

: 1218815-84-9
mono-tert-butyl oxalic acid N-methoxy-N-methylamide

Guidance literature:: oxalyl dichloride; tert-butyl alcohol; In tetrahydrofuran; at 0 ℃; for 1h; Inert atmosphere;

N,O-dimethylhydroxylamine*hydrochloride; With triethylamine; In tetrahydrofuran; at 0 ℃; for 2h; Inert atmosphere;
DOI:10.1021/jacs.1c02833

Reference yield: 30.0%

: 35448-10-3
oxalic acid mono-tert-butyl ester

: 6638-79-5
N,O-dimethylhydroxylamine*hydrochloride

: 1218815-84-9
mono-tert-butyl oxalic acid N-methoxy-N-methylamide

Guidance literature:: oxalic acid mono-tert-butyl ester;

N,O-dimethylhydroxylamine*hydrochloride; With dmap; triethylamine; In dichloromethane; at 0 ℃; for 14h;
DOI:10.1002/asia.201801035