Benzenamine, 2-methoxy-N-methyl-6-nitro-

Base Information

• Chemical Name: Benzenamine, 2-methoxy-N-methyl-6-nitro-
• CAS No.: 410092-91-0
• Molecular Formula: C8H10 N2 O3
• Molecular Weight: 182.179
• Hs Code.: 2922299090
• Mol file: 410092-91-0.mol

Synonyms:2-methoxy-N-methyl-6-nitro-aniline;Benzenamine,2-methoxy-N-methyl-6-nitro;3-Nitro-2-methylamino-phenol-methylaether;2-Methoxy-N-methyl-6-nitro-anilin;N-methyl-2-methoxy-6-nitroaniline;3-Nitro-2-methylamino-anisol;

Chemical Property of Benzenamine, 2-methoxy-N-methyl-6-nitro-

Chemical Property:

• PSA: 67.08000
• LogP: 2.24130

Purity/Quality:

97% ^*data from raw suppliers

2-Methoxy-N-methyl-6-nitroaniline 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzenamine, 2-methoxy-N-methyl-6-nitro-

There total 4 articles about Benzenamine, 2-methoxy-N-methyl-6-nitro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.2%

2-Amino-3-nitrophenol (603-85-0) + methyl iodide (74-88-4) → N-methyl-2-methoxy-6-nitroaniline (410092-91-0)

Guidance literature:

2-Amino-3-nitrophenol; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.5h;

methyl iodide; In tetrahydrofuran; at 20 ℃; for 6h;

DOI:10.1016/j.ejmech.2013.08.006

Reference yield: 32.0%

2,3-dinitroanisole (16315-07-4) + methylamine (74-89-5) → N-methyl-2-methoxy-6-nitroaniline (410092-91-0)

Guidance literature:

In ethanol; at 160 ℃; for 6h;

DOI:10.1135/cccc20011638

Reference yield:

2-fluoro-1-methoxy-3-nitrobenzene (445-68-1) + methylamine (74-89-5) → N-methyl-2-methoxy-6-nitroaniline (410092-91-0)

Guidance literature:

In ethanol; for 16h; Heating;

DOI:10.1016/j.bmcl.2008.01.074

upstream raw materials:

2,3-dinitroanisole

dimethyl amine

methylamine

2-fluoro-1-methoxy-3-nitrobenzene

Downstream raw materials:

3-methoxy-N²-methyl-o-phenylenediamine

2-methoxy-N-methyl-4,6,N-trinitro-aniline

4-(3,4,5-trimethoxyphenyl)-5-(7-methoxy-N¹-methylbenzo[d]imidazole-4yl)oxazole