(cobalt)(1,2-bis(3-pyridylcarboxamide)benzene)2(thiocyanate)2(methanol)2

Base Information

Chemical Name:(cobalt)(1,2-bis(3-pyridylcarboxamide)benzene)2(thiocyanate)2(methanol)2
CAS No.:1096033-82-7
Molecular Formula:C₄₀H₃₆CoN₁₀O₆S₂
Molecular Weight:875.914
Hs Code.:

Synonyms:(cobalt)(1,2-bis(3-pyridylcarboxamide)benzene)2(thiocyanate)2(methanol)2

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Chemical Property of (cobalt)(1,2-bis(3-pyridylcarboxamide)benzene)2(thiocyanate)2(methanol)2

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Technology Process of (cobalt)(1,2-bis(3-pyridylcarboxamide)benzene)2(thiocyanate)2(methanol)2

There total 1 articles about (cobalt)(1,2-bis(3-pyridylcarboxamide)benzene)2(thiocyanate)2(methanol)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 67-56-1
methanol

: cobalt(II) sulfate

: 333-20-0
potassium thioacyanate

: 39642-80-3
1,2-bis(3-pyridylcarboxylamide)benzene

: 1096033-82-7
(cobalt)(1,2-bis(3-pyridylcarboxamide)benzene)2(thiocyanate)2(methanol)2

Guidance literature:: In N,N-dimethyl-formamide; DMF soln. of benzene deriv. added to methanol soln. of CoSO4, then MeOH soln. of KNCS added with stirring fir 30 min; filtered; filtrate allowed to stand at ambient temp.; collected by filtration, washed with MeOH and acetone;
DOI:10.1080/15533170701606498