4-(5-(4-(N-phenyl-N-(4-methoxyphenyl)amino)phenyl)-thien-2-yl)-7-(4-(di-(4-methoxyphenyl)amino)phenyl)-2,1,3-benzothiadiazole

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Chemical Name:4-(5-(4-(N-phenyl-N-(4-methoxyphenyl)amino)phenyl)-thien-2-yl)-7-(4-(di-(4-methoxyphenyl)amino)phenyl)-2,1,3-benzothiadiazole
CAS No.:1253294-10-8
Molecular Formula:C₄₉H₃₈N₄O₃S₂
Molecular Weight:794.998
Hs Code.:

Synonyms:4-(5-(4-(N-phenyl-N-(4-methoxyphenyl)amino)phenyl)-thien-2-yl)-7-(4-(di-(4-methoxyphenyl)amino)phenyl)-2,1,3-benzothiadiazole

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Chemical Property of 4-(5-(4-(N-phenyl-N-(4-methoxyphenyl)amino)phenyl)-thien-2-yl)-7-(4-(di-(4-methoxyphenyl)amino)phenyl)-2,1,3-benzothiadiazole

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Technology Process of 4-(5-(4-(N-phenyl-N-(4-methoxyphenyl)amino)phenyl)-thien-2-yl)-7-(4-(di-(4-methoxyphenyl)amino)phenyl)-2,1,3-benzothiadiazole

There total 8 articles about 4-(5-(4-(N-phenyl-N-(4-methoxyphenyl)amino)phenyl)-thien-2-yl)-7-(4-(di-(4-methoxyphenyl)amino)phenyl)-2,1,3-benzothiadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.7%

: 1253294-07-3
4-(5-(4-(N-phenyl-N-(4-hydroxyphenyl)amino)phenyl)-thien-2-yl)-7-(4-(di-(4-methoxyphenyl)-amino)-phenyl)-2,1,3-benzothiadiazole

: 74-88-4
methyl iodide

: 1253294-10-8
4-(5-(4-(N-phenyl-N-(4-methoxyphenyl)amino)phenyl)-thien-2-yl)-7-(4-(di-(4-methoxyphenyl)amino)phenyl)-2,1,3-benzothiadiazole

Guidance literature:: With potassium carbonate; In acetone; at 60 ℃; for 6h;
DOI:10.1002/adfm.201000840

Reference yield:

: 194416-45-0
4-bromo-N,N-bis-(4-methoxyphenyl)aniline

: 1253294-10-8
4-(5-(4-(N-phenyl-N-(4-methoxyphenyl)amino)phenyl)-thien-2-yl)-7-(4-(di-(4-methoxyphenyl)amino)phenyl)-2,1,3-benzothiadiazole

Guidance literature:: Multi-step reaction with 5 steps

1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate / N,N-dimethyl-formamide / 12 h / 80 °C

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; Aliquat 336; potassium carbonate / toluene / 12 h / 90 °C / Darkness

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 24 h / 100 °C / Darkness

4: hydrogenchloride / tetrahydrofuran; water

5: potassium carbonate / acetone / 6 h / 60 °C

With hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; Aliquat 336; potassium carbonate; In tetrahydrofuran; water; N,N-dimethyl-formamide; acetone; toluene; 2: Suzuki coupling / 3: Stille coupling;
DOI:10.1002/adfm.201000840

Reference yield:

: 1253294-06-2
4-(5-(4-(N-phenyl-N-(4-(tert-butyldimethylsilyloxy)phenyl)amino)phenyl)-thien-2-yl)-7-(4-(di-(4-methoxyphenyl)-amino)phenyl)-2,1,3-benzothiadiazole

: 1253294-10-8
4-(5-(4-(N-phenyl-N-(4-methoxyphenyl)amino)phenyl)-thien-2-yl)-7-(4-(di-(4-methoxyphenyl)amino)phenyl)-2,1,3-benzothiadiazole

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / tetrahydrofuran; water

2: potassium carbonate / acetone / 6 h / 60 °C

With hydrogenchloride; potassium carbonate; In tetrahydrofuran; water; acetone;
DOI:10.1002/adfm.201000840