Pyridine, 3-ethyl-, radical ion(1+) (9CI)

Base Information

• Chemical Name: Pyridine, 3-ethyl-, radical ion(1+) (9CI)
• CAS No.: 151103-56-9
• Molecular Formula: C₇H₉N
• Molecular Weight: 107.155
• Mol file: 151103-56-9.mol

Synonyms:Pyridine, 3-ethyl-, radical ion(1+) (9CI)

Chemical Property of Pyridine, 3-ethyl-, radical ion(1+) (9CI)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Pyridine, 3-ethyl-, radical ion(1+) (9CI)

There total 51 articles about Pyridine, 3-ethyl-, radical ion(1+) (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

methyl (E)-2-(1-(pyridin-3-yl)ethylidene)hydrazine-1-carboxylate → 3-ethylpyridine (536-78-7,151103-56-9)

Guidance literature:

With potassium hydroxide; In 2,2'-[1,2-ethanediylbis(oxy)]bisethanol; at 140 ℃; for 4h;

DOI:10.1055/s-0035-1560805

Reference yield: 75.0%

4-methyl-N′-(1-(pyridin-3-yl)ethylidene)benzenesulfonohydrazide (453523-36-9) → 3-ethylpyridine (536-78-7,151103-56-9)

Guidance literature:

With dichloro bis(1,4-diazabicyclo[2.2.2]octane)(BH₄)Zr(IV); toluene-4-sulfonic acid; In sulfolane; N,N-dimethyl-formamide; at 110 ℃; for 4.1h;

DOI:10.1055/s-2004-836038

Reference yield: 72.0%

3-hydroxymethylpyridin (100-55-0) + dimethylsulfone (67-71-0) → 3-ethylpyridine (536-78-7,151103-56-9)

Guidance literature:

With platinum on carbon; potassium tert-butylate; hydrogen; In toluene; for 24h; under 1875.19 Torr; Inert atmosphere; Reflux;

DOI:10.1002/chem.201505109

upstream raw materials:

brucine

1-methylpiperidine

methyl-3-pyridylketone

5-ethylpyridine-2-carboxylic acid

Downstream raw materials:

3-ethylpyridine N-oxide

2-amino-3-ethylpyridine

(+/–)-3-ethylpiperidine

1-phenyl-2-(pyridin-3-yl)-1-propanone