Triisopropylgallium

Base Information

• Chemical Name: Triisopropylgallium
• CAS No.: 54514-59-9
• Molecular Formula: C9H24Ga
• Molecular Weight: 0
• Hs Code.: 2931900090
• European Community (EC) Number: 633-379-1
• DSSTox Substance ID: DTXSID60560473
• Mol file: 54514-59-9.mol

Synonyms:Triisopropylgallium;Tri(propan-2-yl)gallane;54514-59-9;DTXSID60560473

Chemical Property of Triisopropylgallium

Chemical Property:

• Boiling Point: 175 °C
• PSA: 0.00000
• LogP: 3.64820
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 3
• Exact Mass: 198.08990
• Heavy Atom Count: 10
• Complexity: 65.7

Purity/Quality:

99% ^*data from raw suppliers

TRIISOPROPYLGALLIUM 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(C)[Ga](C(C)C)C(C)C

Technology Process of Triisopropylgallium

There total 4 articles about Triisopropylgallium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

1,3,5-tris(3,3-dimethyl-1-butynyl)benzene (851961-39-2) + diisopropylgallium hydride → ((CH3)2CH)3Ga3(C6H3(CCHC(CH3)3)3)2 + triisopropylgallium (54514-59-9)

Guidance literature:

In hexane; under Ar; soln. of (i-Pr)2GaH in n-hexane added to soln. of C6H3(C2CMe3)3 in n-hexane at room temp.; heated under reflux for 16 h; filtered; filtrate concd. under vac. at room temp.; ppt. collected;

DOI:10.1039/b614003c

Reference yield:

i-PrBr + i-PrMgBr + isopropylmagnesium bromide (920-39-8) + isopropyl bromide (75-26-3) → triisopropylgallium (54514-59-9)

Guidance literature:

GaCl₃; In NMe₂ Et; N,N-dimethyl-ethanamine; pentane;

Reference yield:

isopropylmagnesium chloride (1068-55-9) + Gallium trichloride (13450-90-3) → triisopropylgallium (54514-59-9)

Guidance literature:

In not given;

DOI:10.1016/j.jorganchem.2006.12.005

upstream raw materials:

isopropylmagnesium bromide

isopropyl bromide

isopropylmagnesium chloride

Gallium trichloride

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