cis-[Pd(NO₃)2(PPh₃)2]

Base Information

Chemical Name:cis-[Pd(NO₃)2(PPh₃)2]
CAS No.:1221962-18-0
Molecular Formula:C₃₆H₃₀N₂O₆P₂Pd
Molecular Weight:755.012
Hs Code.:

cis-[Pd(NO<sub>3</sub>)2(PPh<sub>3</sub>)2]

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Chemical Property of cis-[Pd(NO₃)2(PPh₃)2]

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Technology Process of cis-[Pd(NO₃)2(PPh₃)2]

There total 2 articles about cis-[Pd(NO₃)2(PPh₃)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 7697-37-2,78989-43-2
nitric acid

: 3375-31-3
palladium diacetate

: 603-35-0
triphenylphosphine

: 1221962-18-0,15640-81-0,30153-56-1
cis-[Pd(NO₃)2(PPh₃)2]

Guidance literature:: In nitric acid; acetone; aq. HNO3; addn. of phosphine deriv. to acetone soln. of palladium compd. at roomt emp., addn. of aq. HNO3 at room temp., stirring for 30 min; filtration, washing with ether, drying in vac., elem. anal.;
DOI:10.1021/ic901569w

Reference yield: 90.0%

: 14409-50-8
bis-(triphenylphosphine)dinitro-palladium(II)

: 15640-81-0,30153-56-1,1221962-18-0
[Pd(NO₃)2(P(C₆H₅)3)2]

Guidance literature:: With NO₂; In dichloromethane; (N2); NO2 passed through soln. of Pd(NO2)2(PPh3)2 for 10-15 min; soln. purged with N2; evapd. in vacuo; recrystd. (dichloromethane/n-hexane); filtered off; dried in vacuo; elem. anal.;

Reference yield: 77.0%

: 67-56-1
methanol

: 201230-82-2
carbon monoxide

: 1221962-18-0,15640-81-0,30153-56-1
cis-[Pd(NO₃)2(PPh₃)2]

: trans-[Pd(nitro)(carbomethoxy)(triphenylphosphine)2]

: trans-[Pd(nitrito)(carbomethoxy)(triphenylphosphine)2]

: 1221575-94-5
trans-[Pd(COOMe)(NO₃)(PPh₃)2]

Guidance literature:: With C₅H₅N; P(C₆H₅)3; In methanol; byproducts: [C5H5NH]NO3; High Pressure; mixing methanolic soln. of palladium compd., phosphine deriv. and pyridine, heating at 50°C for 2 h at 5 atm of CO; filtration, addn. of diethyl ether, stirring for 30 min, filtration, washing with ether, drying in vac., elem. anal.;
DOI:10.1021/ic901569w