(E)-β-methoxy-α-phenylcinnamaldehyde

Base Information

• Chemical Name: (E)-β-methoxy-α-phenylcinnamaldehyde
• CAS No.: 96746-52-0
• Molecular Formula: C₁₆H₁₄O₂
• Molecular Weight: 238.286

Synonyms:

Chemical Property of (E)-β-methoxy-α-phenylcinnamaldehyde

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Technology Process of (E)-β-methoxy-α-phenylcinnamaldehyde

There total 4 articles about (E)-β-methoxy-α-phenylcinnamaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 8.0%

methanol (67-56-1) + (E)-β-chloro-α,β-diphenylacrolein (50460-72-5) → 2,4-diphenyl-1,3-oxazole (838-41-5) + 1-benzyl-5-phenyl-1H-tetrazole (96746-54-2) + (E)-β-methoxy-α-phenylcinnamaldehyde (96746-52-0)

Guidance literature:

With sodium azide; In acetonitrile; for 46h; Ambient temperature;

DOI:10.1021/jo00217a033

Reference yield: 3.0%

(E)-β-chloro-α,β-diphenylacrolein (50460-72-5) → 2,4-diphenyl-1,3-oxazole (838-41-5) + 1-benzyl-5-phenyl-1H-tetrazole (96746-54-2) + (E)-β-methoxy-α-phenylcinnamaldehyde (96746-52-0)

Guidance literature:

With sodium azide; In methanol; acetonitrile; for 46h; Ambient temperature;

DOI:10.1021/jo00217a033

Reference yield:

phenyl benzyl ketone (451-40-1) → (E)-β-methoxy-α-phenylcinnamaldehyde (96746-52-0)

Guidance literature:

Multi-step reaction with 2 steps

1: trichloroethylene, POCl₃ / 23 h / a) 90 deg C, 5 h, b) 20 deg C, 18 h

2: sodium methoxide / methanol / 40 h / Ambient temperature

With Trichloroethylene; sodium methylate; trichlorophosphate; In methanol;

DOI:10.1021/jo00217a033

upstream raw materials:

methanol

(Z)-β-chloro-α,β-diphenylacrolein

(E)-β-chloro-α,β-diphenylacrolein

phenyl benzyl ketone

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