(2E)-N,1,3-trimethyltriaz-2-ene-1-carboxamide

Base Information

• Chemical Name: (2E)-N,1,3-trimethyltriaz-2-ene-1-carboxamide
• CAS No.: 103711-40-6
• Molecular Formula: C4H10 N4 O
• Molecular Weight: 130.15
• Mol file: 103711-40-6.mol

Synonyms:NSC378853

Chemical Property of (2E)-N,1,3-trimethyltriaz-2-ene-1-carboxamide

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• Density: 1.11g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (2E)-N,1,3-trimethyltriaz-2-ene-1-carboxamide

There total 1 articles about (2E)-N,1,3-trimethyltriaz-2-ene-1-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

1,3-dimethyl-1-triazene (3585-32-8,115246-94-1,115246-96-3,467426-36-4) + methyl isocyanate (624-83-9) → 1,3-dimethyl-3-(N-methylcarbamoyl)triazene (103711-40-6)

Guidance literature:

In pentane; Heating;

DOI:10.1021/jo00370a002

Reference yield:

C4H10N4O (103711-40-6) → methanol (67-56-1) + methylphosphate (812-00-0) + N,N'-Dimethylurea (96-31-1) + 1,3-Dimethyltriazene (3585-32-8,115246-94-1,115246-96-3,467426-36-4) + methylamine (74-89-5)

Guidance literature:

With 2,6-diaminocaproic acid; sodium perchlorate; In acetonitrile; at 70 ℃; Rate constant; variation of pH, solvent deuterium isotope effect;

DOI:10.1021/jo00050a016

Reference yield:

1,3-dimethyl-3-(N-methylcarbamoyl)triazene (103711-40-6) → methanol (67-56-1) + N,N'-Dimethylurea (96-31-1)

Guidance literature:

With water; In acetonitrile; at 70 ℃; Rate constant; Mechanism; Product distribution; hydrolytic decomposition in acidic and neutral buffers; pH-dependence of the rate of decomposition; solvent deuterium isotope effect (k_H2O/k_D2O);

DOI:10.1021/jo00028a047

upstream raw materials:

1,3-dimethyl-1-triazene

methyl isocyanate

Downstream raw materials:

methanol

N,N'-Dimethylurea

methylphosphate

1,3-Dimethyltriazene

Refernces