C₉H₉⁽²⁾H₅Si

Base Information

• Chemical Name: C₉H₉⁽²⁾H₅Si
• CAS No.: 95450-75-2
• Molecular Formula: C₉H₁₄Si
• Molecular Weight: 155.256
• Mol file: 95450-75-2.mol

Synonyms:

Chemical Property of C₉H₉⁽²⁾H₅Si

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of C₉H₉⁽²⁾H₅Si

There total 3 articles about C₉H₉⁽²⁾H₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 9.0%

1,1,1,2,2,2-hexamethyldisilane (1450-14-2) + fluorobenzene-d5 (1423-10-5) → C9H9(2)H5Si (95450-75-2) + C9H9(2)H4FSi + C9H9(2)H4FSi

Guidance literature:

With sodium methylate; In N,N,N,N,N,N-hexamethylphosphoric triamide; for 0.5h;

DOI:10.1021/ol015666s

Reference yield: 6.4%

1,1,1,2,2,2-hexamethyldisilane (1450-14-2) + benzene-d6 (1076-43-3) → C9H9(2)H5Si (95450-75-2)

Guidance literature:

With sodium methylate; In N,N,N,N,N,N-hexamethylphosphoric triamide;

DOI:10.1021/ol015666s

Reference yield:

chloro-trimethyl-silane (75-77-4) + benzene-d6 (1076-43-3) → deuterio-trimethyl-silane (18026-91-0) + C9H9(2)H5Si (95450-75-2)

Guidance literature:

With calcium; Yield given. Multistep reaction. Yields of byproduct given; 1) 900 deg C, 0.005 Torr, 2) 1 h, r.t., 0.005 Torr;

DOI:10.1246/cl.1984.1989

upstream raw materials:

chloro-trimethyl-silane

benzene-d6

1,1,1,2,2,2-hexamethyldisilane

fluorobenzene-d5