Phosphoric acid (2S,3S,5R)-3-azido-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester 2-chloro-phenyl ester 2-(naphthalen-1-yloxy)-ethyl ester

Base Information

Chemical Name:Phosphoric acid (2S,3S,5R)-3-azido-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester 2-chloro-phenyl ester 2-(naphthalen-1-yloxy)-ethyl ester
CAS No.:179030-53-6
Molecular Formula:C₂₈H₂₇ClN₅O₈P
Molecular Weight:627.978
Hs Code.:

Phosphoric acid (2S,3S,5R)-3-azido-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester 2-chloro-phenyl ester 2-(naphthalen-1-yloxy)-ethyl ester

Synonyms:

Suppliers and Price of Phosphoric acid (2S,3S,5R)-3-azido-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester 2-chloro-phenyl ester 2-(naphthalen-1-yloxy)-ethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Phosphoric acid (2S,3S,5R)-3-azido-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester 2-chloro-phenyl ester 2-(naphthalen-1-yloxy)-ethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Phosphoric acid (2S,3S,5R)-3-azido-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester 2-chloro-phenyl ester 2-(naphthalen-1-yloxy)-ethyl ester

There total 5 articles about Phosphoric acid (2S,3S,5R)-3-azido-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester 2-chloro-phenyl ester 2-(naphthalen-1-yloxy)-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 90-15-3
α-naphthol

: 179030-53-6
Phosphoric acid (2S,3S,5R)-3-azido-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester 2-chloro-phenyl ester 2-(naphthalen-1-yloxy)-ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / K₂CO₃ / acetone / 12 h / Heating

2: pyridine, H₂O / acetonitrile / 0.17 h

3: pyridine, 1-(2-mesitylenesulfonyl)-3-nitro-1,2,4-triazole / 12 h / Ambient temperature

With pyridine; water; potassium carbonate; 1-(mesitylene-2-sulfonyl)-3-nitro-1H-1,2,4-triazole; In acetone; acetonitrile;
DOI:10.1021/jm950777g

Reference yield:

: 711-82-0
2-(1-naphthyloxy)-1-ethanol

: 179030-53-6
Phosphoric acid (2S,3S,5R)-3-azido-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester 2-chloro-phenyl ester 2-(naphthalen-1-yloxy)-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine, H₂O / acetonitrile / 0.17 h

2: pyridine, 1-(2-mesitylenesulfonyl)-3-nitro-1,2,4-triazole / 12 h / Ambient temperature

With pyridine; water; 1-(mesitylene-2-sulfonyl)-3-nitro-1H-1,2,4-triazole; In acetonitrile;
DOI:10.1021/jm950777g

Reference yield:

: 72351-28-1
2-chlorophenyl phosphordi(1H-1-[1,2,4]triazolide)

: 179030-53-6
Phosphoric acid (2S,3S,5R)-3-azido-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester 2-chloro-phenyl ester 2-(naphthalen-1-yloxy)-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine, H₂O / acetonitrile / 0.17 h

2: pyridine, 1-(2-mesitylenesulfonyl)-3-nitro-1,2,4-triazole / 12 h / Ambient temperature

With pyridine; water; 1-(mesitylene-2-sulfonyl)-3-nitro-1H-1,2,4-triazole; In acetonitrile;
DOI:10.1021/jm950777g