methyl 4-amino-2-hydroxy-3-(2-methylprop-2-en-1-yl)-5-nitrobenzoate

Base Information

Chemical Name:methyl 4-amino-2-hydroxy-3-(2-methylprop-2-en-1-yl)-5-nitrobenzoate
CAS No.:1374298-17-5
Molecular Formula:C₁₂H₁₄N₂O₅
Molecular Weight:266.254
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 4-amino-2-hydroxy-3-(2-methylprop-2-en-1-yl)-5-nitrobenzoate

Chemical Property:

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Technology Process of methyl 4-amino-2-hydroxy-3-(2-methylprop-2-en-1-yl)-5-nitrobenzoate

There total 6 articles about methyl 4-amino-2-hydroxy-3-(2-methylprop-2-en-1-yl)-5-nitrobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1583-58-0
2,4-difluoro-benzoic acid

: 1374298-17-5
methyl 4-amino-2-hydroxy-3-(2-methylprop-2-en-1-yl)-5-nitrobenzoate

Guidance literature:: Multi-step reaction with 7 steps

1.1: sulfuric acid; nitric acid / water / 14 h / 0 - 5 °C

2.1: sulfuric acid / ethanol / 24 h / Reflux

3.1: triethylamine / tetrahydrofuran / 0 - 26 °C

4.1: sodium methylate / methanol; water / 0 - 26 °C

5.1: aluminum (III) chloride / 1,2-dichloro-ethane / Reflux

6.1: potassium carbonate / N,N-dimethyl-formamide / 0.5 h / 80 °C

6.2: 80 °C

7.1: N,N-diethylaniline / 1.3 h / Reflux

With aluminum (III) chloride; sulfuric acid; nitric acid; sodium methylate; potassium carbonate; triethylamine; N,N-diethylaniline; sulfuric acid; In tetrahydrofuran; methanol; ethanol; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide;

Reference yield:

: 153775-33-8
2,4-difluoro-5-nitro-benzoic acid

: 1374298-17-5
methyl 4-amino-2-hydroxy-3-(2-methylprop-2-en-1-yl)-5-nitrobenzoate

Guidance literature:: Multi-step reaction with 6 steps

1.1: sulfuric acid / ethanol / 24 h / Reflux

2.1: triethylamine / tetrahydrofuran / 0 - 26 °C

3.1: sodium methylate / methanol; water / 0 - 26 °C

4.1: aluminum (III) chloride / 1,2-dichloro-ethane / Reflux

5.1: potassium carbonate / N,N-dimethyl-formamide / 0.5 h / 80 °C

5.2: 80 °C

6.1: N,N-diethylaniline / 1.3 h / Reflux

With aluminum (III) chloride; sodium methylate; potassium carbonate; triethylamine; N,N-diethylaniline; sulfuric acid; In tetrahydrofuran; methanol; ethanol; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide;

Reference yield:

: 106125-55-7
methyl 4-amino-2-hydroxy-5-nitrobenzoate

: 1374298-17-5
methyl 4-amino-2-hydroxy-3-(2-methylprop-2-en-1-yl)-5-nitrobenzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 0.5 h / 80 °C

1.2: 80 °C

2.1: N,N-diethylaniline / 1.3 h / Reflux

With potassium carbonate; N,N-diethylaniline; In N,N-dimethyl-formamide;