O-(bis-p-methoxyphenylphosphinyl)acetone oxime

Base Information

• Chemical Name: O-(bis-p-methoxyphenylphosphinyl)acetone oxime
• CAS No.: 80717-31-3
• Molecular Formula: C₁₇H₂₀NO₄P
• Molecular Weight: 333.324
• Mol file: 80717-31-3.mol

Synonyms:

Chemical Property of O-(bis-p-methoxyphenylphosphinyl)acetone oxime

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of O-(bis-p-methoxyphenylphosphinyl)acetone oxime

There total 5 articles about O-(bis-p-methoxyphenylphosphinyl)acetone oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

O-(bis-p-methoxyphenylphosphinyl)hydroxylamine (72805-00-6) + acetone (67-64-1) → O-(bis-p-methoxyphenylphosphinyl)acetone oxime (80717-31-3)

Guidance literature:

at 25 ℃; for 2h;

DOI:10.1039/P19810003284

Reference yield:

bis(4-methoxyphenyl)phosphinic acid (20434-05-3) → O-(bis-p-methoxyphenylphosphinyl)acetone oxime (80717-31-3)

Guidance literature:

Multi-step reaction with 2 steps

1: thionyl chloride / 2 h / Heating

2: CH₂Cl₂ / 1 h / Ambient temperature

With thionyl chloride; In dichloromethane;

DOI:10.1039/P19810003284

Reference yield:

4-methoxyphenyl magnesium bromide (13139-86-1) → O-(bis-p-methoxyphenylphosphinyl)acetone oxime (80717-31-3)

Guidance literature:

Multi-step reaction with 3 steps

1: 2.) bromine

2: thionyl chloride / 2 h / Heating

3: CH₂Cl₂ / 1 h / Ambient temperature

With thionyl chloride; bromine; In dichloromethane;

DOI:10.1039/P19810003284

upstream raw materials:

bis(4-methoxyphenyl)phosphinic acid chloride

acetone oxime

O-(bis-p-methoxyphenylphosphinyl)hydroxylamine

acetone