C₄I₂O₄Ru

Base Information

Chemical Name:C₄I₂O₄Ru
CAS No.:18475-75-7
Molecular Formula:C₄I₂O₄Ru
Molecular Weight:466.921
Hs Code.:

C<sub>4</sub>I<sub>2</sub>O<sub>4</sub>Ru

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Suppliers and Price of C₄I₂O₄Ru

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄I₂O₄Ru

Chemical Property:

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Technology Process of C₄I₂O₄Ru

There total 2 articles about C₄I₂O₄Ru which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: sodium tetracarbonylruthenate(II)

: 124-38-9,18923-20-1
carbon dioxide

: 7553-56-2,12190-71-5,8031-47-8
iodine

: 15663-30-6,18475-75-7,25322-72-9
cis-{RuI₂(CO)4}

: 497-19-8
sodium carbonate

Guidance literature:: In tetrahydrofuran; bubbling of excess CO2 through a suspension of Na2(Ru(CO)4) in THF (stirred 20min, 4°C), filtration of soln. onto I2 at 4°C;; pptg. of carbonate; soln.: removal of solvent (IR), sublimation off of excess iodine, extn. with THF;;
DOI:10.1021/ja00244a017

Reference yield:

: 201230-82-2
carbon monoxide

: 13896-65-6
ruthenium(III) iodide

: 15243-33-1
dodecacarbonyl-triangulo-triruthenium

: 15663-30-6,18475-75-7,25322-72-9
cis-{RuI₂(CO)4}

: α-{Ru2I4(CO)6}

Guidance literature:: With Co, or Fe, or steel; In ethanol; High Pressure; 10-50 bar CO, heated at 125°C for 3-20 h; cooled on ice bath, filtered, evapd. to dryness, dissolved (CH2Cl2), recrystd.; elem. anal.; Kinetics;
DOI:10.1002/ejic.200700341