[Au(2-diphenylphosphino-3-methylindole)2]PF₆

Base Information

Chemical Name:[Au(2-diphenylphosphino-3-methylindole)2]PF₆
CAS No.:1321502-78-6
Molecular Formula:C₄₂H₃₆AuN₂P₂*F₆P
Molecular Weight:972.639
Hs Code.:

[Au(2-diphenylphosphino-3-methylindole)2]PF<sub>6</sub>

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Chemical Property of [Au(2-diphenylphosphino-3-methylindole)2]PF₆

Chemical Property:

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Technology Process of [Au(2-diphenylphosphino-3-methylindole)2]PF₆

There total 2 articles about [Au(2-diphenylphosphino-3-methylindole)2]PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 800369-69-1
diphenyl-2-(3-methylindolyl)phosphine

: 26042-63-7
silver(I) hexafluorophosphate

: 39929-21-0
(tetrahydrothiophene)gold(I) chloride

: 1321502-78-6
[Au(2-diphenylphosphino-3-methylindole)2]PF₆

Guidance literature:: In dichloromethane; byproducts: AgCl; to soln. Au complex in CH2Cl2 ligand was added, stirred for 15 min, soln. AgPF6 in acetone was added, stirred for 15 min; soln. was filtered and evapd., residue was washed with Et2O and recrystd. by Et2O vapor diffusion into CH2Cl2 soln.; elem. anal.;
DOI:10.1039/c1dt10564g

Reference yield:

: 800369-69-1
diphenyl-2-(3-methylindolyl)phosphine

: 1321502-81-1
Au₂(2-diphenylphosphino-3-methylindole^(1-))2

: 2923-28-6
silver trifluoromethanesulfonate

: 1321502-93-5
Ag₂(2-diphenylphosphino-3-methylindole^(1-))2

: 1321502-89-9,1321503-00-7
AuAg(2-diphenylphosphino-3-methylindole^(1-))2

: 1321502-89-9,1321503-00-7
AuAg(2-diphenylphosphino-3-methylindole^(1-))2

: 1321502-78-6
[Au(2-diphenylphosphino-3-methylindole)2]PF₆

Guidance literature:: With triethylamine; In methanol; dichloromethane; to soln. CF3COOAg in MeOH soln. ligand in CH2Cl2 was added, this soln. was added to soln. Au complex in CH2Cl2 followed by Et3N, stirred for 1.5h; soln. was evapd., residue was washed with MeOH and Et2O and recrystd. from CHCl3-heptane at room temp.;
DOI:10.1039/c1dt10564g

Reference yield: 93.0%

: 64443-05-6
tetrakis(actonitrile)copper(I) hexafluorophosphate

: 1321502-78-6
[Au(2-diphenylphosphino-3-methylindole)2]PF₆

: 1321502-85-5
AuCu(2-diphenylphosphino-3-methylindole^(1-))2

Guidance literature:: With triethylamine; In dichloromethane; to soln. Au complex in CH2Cl2 soln. Cu complex in CH2Cl2 was added followed by Et3N, stirred for 30 min; soln. was evapd., residue was washed with MeOH and Et2O and recrystd. byEt2O vapor diffusion into CHCl3-EtOH soln. at 5°C;
DOI:10.1039/c1dt10564g