bis(2,2,2-trichloroethyl)((1R,2R)-1,2-bis(4-methoxyphenyl)ethane-1,2-diyl)dicarbamate

Base Information

• Chemical Name: bis(2,2,2-trichloroethyl)((1R,2R)-1,2-bis(4-methoxyphenyl)ethane-1,2-diyl)dicarbamate
• CAS No.: 1413934-40-3
• Molecular Formula: C₂₂H₂₂Cl₆N₂O₆
• Molecular Weight: 623.144
• Mol file: 1413934-40-3.mol

Synonyms:

Chemical Property of bis(2,2,2-trichloroethyl)((1R,2R)-1,2-bis(4-methoxyphenyl)ethane-1,2-diyl)dicarbamate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of bis(2,2,2-trichloroethyl)((1R,2R)-1,2-bis(4-methoxyphenyl)ethane-1,2-diyl)dicarbamate

There total 1 articles about bis(2,2,2-trichloroethyl)((1R,2R)-1,2-bis(4-methoxyphenyl)ethane-1,2-diyl)dicarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzoic acid anhydride (93-97-0) + d,l-1,2-diamino-1,2-bis(4-methoxyphenyl)ethane (117106-36-2) + 2,2,2-Trichloroethyl chloroformate (17341-93-4) → 2,2,2-trichloroethyl((1R,2R)-2-benzamido-1,2-bis(4-methoxyphenyl)ethyl)carbamate (1413934-30-1) + bis(2,2,2-trichloroethyl)((1S,2S)-1,2-bis(4-methoxyphenyl)ethane-1,2-diyl)dicarbamate + 2,2,2-trichloroethyl((1S,2S)-2-benzamido-1,2-bis(4-methoxyphenyl)ethyl)carbamate + bis(2,2,2-trichloroethyl)((1R,2R)-1,2-bis(4-methoxyphenyl)ethane-1,2-diyl)dicarbamate (1413934-40-3)

Guidance literature:

benzoic acid anhydride; With dmap; N-((1R,2R)-2-(3-(3,5-bis(trifluoromethyl)phenyl)thioureido)cyclohexyl)-3,5-bis(trifluoromethyl)benzamide; In toluene; at -78 ℃; for 0.25h; Molecular sieve; Inert atmosphere;

d,l-1,2-diamino-1,2-bis(4-methoxyphenyl)ethane; In toluene; at -78 - 20 ℃; Molecular sieve; Inert atmosphere;

2,2,2-Trichloroethyl chloroformate; With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 ℃; Inert atmosphere;

DOI:10.1039/c2cc36361e

upstream raw materials:

benzoic acid anhydride

d,l-1,2-diamino-1,2-bis(4-methoxyphenyl)ethane

2,2,2-Trichloroethyl chloroformate