methyl (2R,3R)-2-benzamide-3-phenylbutanoate

Base Information

Chemical Name:methyl (2R,3R)-2-benzamide-3-phenylbutanoate
CAS No.:675608-51-2
Molecular Formula:C₁₈H₁₉NO₃
Molecular Weight:297.354
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (2R,3R)-2-benzamide-3-phenylbutanoate

Chemical Property:

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Technology Process of methyl (2R,3R)-2-benzamide-3-phenylbutanoate

There total 6 articles about methyl (2R,3R)-2-benzamide-3-phenylbutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98-86-2
acetophenone

: 675608-51-2
methyl (2R,3R)-2-benzamide-3-phenylbutanoate

Guidance literature:: Multi-step reaction with 4 steps

1: acetic anhydride; lead(IV) acetate / tetrahydrofuran / 24 h / Heating

2: 97 percent / methanol / 0.5 h / 20 °C

3: 97 percent / H₂ / Pd/C / ethyl acetate / 10 h / 30 °C

4: amylose 10-undecenoate/3,5-di(Me)phenylcarbamate on AllSiO₂ / hexane; propan-2-ol; CHCl₃ / 6 h / 25 °C

With lead(IV) acetate; 3,5-dimethylphenyl carbamate; amylose 10-undecenoate; hydrogen; acetic anhydride; palladium on activated charcoal; In tetrahydrofuran; methanol; hexane; chloroform; ethyl acetate; isopropyl alcohol;
DOI:10.1016/j.tet.2003.11.044

Reference yield:

: 495-69-2,140480-84-8,21251-67-2,91787-63-2,66407-11-2
Hippuric Acid

: 675608-51-2
methyl (2R,3R)-2-benzamide-3-phenylbutanoate

Guidance literature:: Multi-step reaction with 5 steps

1: 38 percent / acetic anhydride; lead(IV) acetate / tetrahydrofuran / 24 h / Heating

2: 94 percent / HBr; benzoyl peroxide / toluene / cooling

3: 97 percent / methanol / 0.5 h / 20 °C

4: 97 percent / H₂ / Pd/C / ethyl acetate / 10 h / 30 °C

5: amylose 10-undecenoate/3,5-di(Me)phenylcarbamate on AllSiO₂ / hexane; propan-2-ol; CHCl₃ / 6 h / 25 °C

With lead(IV) acetate; 3,5-dimethylphenyl carbamate; amylose 10-undecenoate; hydrogen bromide; hydrogen; acetic anhydride; dibenzoyl peroxide; palladium on activated charcoal; In tetrahydrofuran; methanol; hexane; chloroform; ethyl acetate; isopropyl alcohol; toluene;
DOI:10.1016/j.tet.2003.11.044

Reference yield:

: 57427-91-5
(E)-2-phenyl-4-(α-phenylethylidene)-5-(4H)-oxazolone

: 675608-51-2
methyl (2R,3R)-2-benzamide-3-phenylbutanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / methanol / 0.5 h / 20 °C

2: 97 percent / H₂ / Pd/C / ethyl acetate / 10 h / 30 °C

3: amylose 10-undecenoate/3,5-di(Me)phenylcarbamate on AllSiO₂ / hexane; propan-2-ol; CHCl₃ / 6 h / 25 °C

With 3,5-dimethylphenyl carbamate; amylose 10-undecenoate; hydrogen; palladium on activated charcoal; In methanol; hexane; chloroform; ethyl acetate; isopropyl alcohol;
DOI:10.1016/j.tet.2003.11.044