N,N-dimethyl O,S-dimethyl phosphoramidothioate

Base Information

• Chemical Name: N,N-dimethyl O,S-dimethyl phosphoramidothioate
• CAS No.: 65960-94-3
• Molecular Formula: C₄H₁₂NO₂PS
• Molecular Weight: 169.185
• Mol file: 65960-94-3.mol

Synonyms:

Chemical Property of N,N-dimethyl O,S-dimethyl phosphoramidothioate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N,N-dimethyl O,S-dimethyl phosphoramidothioate

There total 3 articles about N,N-dimethyl O,S-dimethyl phosphoramidothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

N-methyl O,O-dimethyl phosphoramidothioate (31464-99-0) + dimethyl amine (124-40-3) + methyl iodide (74-88-4) → N,N-dimethyl O,S-dimethyl phosphoramidothioate (65960-94-3,87000-69-9,25218-42-2)

Guidance literature:

With 18-crown-6 ether; potassium iodide; In dichloromethane; acetonitrile; at 80 ℃;

DOI:10.1007/BF03245903

Reference yield:

N,N-dimethyl O,O-dimethyl phosphoramidothioate (28167-51-3) + methyl iodide (74-88-4) → N,N-dimethyl O,S-dimethyl phosphoramidothioate (65960-94-3,87000-69-9,25218-42-2)

Guidance literature:

With potassium iodide; In chloroform; acetonitrile; at 70 ℃;

DOI:10.1007/BF03245903

Reference yield:

→ N,N-dimethyl O,S-dimethyl phosphoramidothioate (65960-94-3,87000-69-9,25218-42-2)

Guidance literature:

O,O-Dimethyl-N-dimethylphosphoramidothioat, MeI (Δ);

DOI:10.1021/jf60192a013

upstream raw materials:

N-methyl O,O-dimethyl phosphoramidothioate

dimethyl amine

methyl iodide

N,N-dimethyl O,O-dimethyl phosphoramidothioate

Downstream raw materials:

O,O,S-trimethyl phosphorothioate