chloroiron(III) meso-α,α,α,α-tetrakis(o-pivalamidophenyl)porphyrinate

Base Information

Chemical Name:chloroiron(III) meso-α,α,α,α-tetrakis(o-pivalamidophenyl)porphyrinate
CAS No.:87334-92-7
Molecular Formula:C₆₄H₆₄ClFeN₈O₄
Molecular Weight:1100.56
Hs Code.:

Synonyms:

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Chemical Property of chloroiron(III) meso-α,α,α,α-tetrakis(o-pivalamidophenyl)porphyrinate

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Technology Process of chloroiron(III) meso-α,α,α,α-tetrakis(o-pivalamidophenyl)porphyrinate

There total 4 articles about chloroiron(III) meso-α,α,α,α-tetrakis(o-pivalamidophenyl)porphyrinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 52275-89-5,75557-96-9
{Fe(meso-5,10,15,20-tetrakis(o-pivalamidophenyl)porphyrinato)(1-methylimidazole)2}

: 105118-92-1,92078-42-7,87334-91-6,86107-94-0,87334-93-8,87334-92-7,104486-25-1
chloroiron(III) meso-α,α,α,α-tetrakis(o-pivalamidophenyl)porphyrinate

Guidance literature:: With hydrogenchloride; hydrogen; oxygen; In ethanol; toluene; a toluene-ethanol soln. of the initial complex was placed in the flask filled with Ar at 25°C, then Ar was replaced by flushing with H2-O2 mixt., a soln. containing HCl and colloidal Pt on polyvinylpyrrolidone satd. with H2-O2 was added; monitored by UV spectrum; Kinetics;
DOI:10.1021/ja00301a016

Reference yield:

: 5,10,15,20-tetrakis(α,α,α,α-o-pivalamidophenyl)porphyrin

: 7789-46-0
iron(II) bromide

: 105118-92-1,92078-42-7,87334-91-6,86107-94-0,87334-93-8,87334-92-7,104486-25-1
chloroiron(III) meso-α,α,α,α-tetrakis(o-pivalamidophenyl)porphyrinate

Guidance literature:: With pyridine; hydrogenchloride; In tetrahydrofuran; dichloromethane; soln. of FeBr2, pyridine, ligand in THF refluxed for 2.5-3 h, under Ar,evapd., dissolved in CH2Cl2, HCl gas passed; evapd.;
DOI:10.1021/ja00361a030

Reference yield:

: 616-47-7
1-methyl-1H-imidazole

: 55449-22-4,75559-87-4
(5,10,15,20-tetrakis(α,α,α,α-O-pivalamidophenyl)porphyrinato)iron(II)(1-methylimidazole)(O2)

: 105118-92-1,92078-42-7,87334-91-6,86107-94-0,87334-93-8,87334-92-7,104486-25-1
chloroiron(III) meso-α,α,α,α-tetrakis(o-pivalamidophenyl)porphyrinate

Guidance literature:: With hydrogenchloride; hydrogen; oxygen; In further solvent(s); a toluene soln. of the porphyrin and Me-imidazole satd. with H2-O2 gas mixt. was added at once to a toluene-EtOH saln. of Me-imidazole, HCl, Pton polyvinylpyrrolidone, cyclohexene and PhCO2Me satd. with H2-O2 mixt.at 25°C and stirred; UV monitoring; Kinetics;
DOI:10.1021/ja00301a016