3-Iodo-4-pivalamidobenzoic acid

Base Information

Chemical Name:3-Iodo-4-pivalamidobenzoic acid
CAS No.:139078-63-0
Molecular Formula:C₁₂H₁₄INO₃
Molecular Weight:347.153
Hs Code.:
DSSTox Substance ID:DTXSID70577355
Wikidata:Q82467318

Synonyms:3-iodo-4-pivalamidobenzoic acid;139078-63-0;3-Iodo-4-pivalamidobenzoicacid;4-(2,2-dimethylpropanoylamino)-3-iodobenzoic acid;DTXSID70577355;AKOS015916087;4-(2,2-Dimethylpropanamido)-3-iodobenzoic acid

Suppliers and Price of 3-Iodo-4-pivalamidobenzoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 3-Iodo-4-pivalamidobenzoic acid

Chemical Property:

XLogP3:2.7
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:347.00184
Heavy Atom Count:17
Complexity:311

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(C)(C)C(=O)NC1=C(C=C(C=C1)C(=O)O)I

Technology Process of 3-Iodo-4-pivalamidobenzoic acid

There total 4 articles about 3-Iodo-4-pivalamidobenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-bromo-p-toluidine: 583-68-6
2-bromo-p-toluidine

: 139078-63-0
4-(2,2-dimethylpropanoylamino)-3-iodobenzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / diethyl ether / 1 h

2: 40 percent / KMnO₄, MgSO₄ / H₂O / 1 h / Heating

3: 1.) CH₃Li, t-butyllithium, 2.) allyl iodide / 1.) THF, -78 deg C, 1 min, 2.) THF, -78 deg C, 5 min

With potassium permanganate; allyl iodid; methyllithium; tert.-butyl lithium; magnesium sulfate; In diethyl ether; water;

Reference yield:

: 3282-30-2
pivaloyl chloride

: 139078-63-0
4-(2,2-dimethylpropanoylamino)-3-iodobenzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / diethyl ether / 1 h

2: 40 percent / KMnO₄, MgSO₄ / H₂O / 1 h / Heating

3: 1.) CH₃Li, t-butyllithium, 2.) allyl iodide / 1.) THF, -78 deg C, 1 min, 2.) THF, -78 deg C, 5 min

With potassium permanganate; allyl iodid; methyllithium; tert.-butyl lithium; magnesium sulfate; In diethyl ether; water;

Reference yield:

: 87995-50-4
N-(2-bromo-4-methylphenyl)-2,2-dimethylpropanamide

: 139078-63-0
4-(2,2-dimethylpropanoylamino)-3-iodobenzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 40 percent / KMnO₄, MgSO₄ / H₂O / 1 h / Heating

2: 1.) CH₃Li, t-butyllithium, 2.) allyl iodide / 1.) THF, -78 deg C, 1 min, 2.) THF, -78 deg C, 5 min

With potassium permanganate; allyl iodid; methyllithium; tert.-butyl lithium; magnesium sulfate; In water;