dichloro(α-hydroxyiminopropiophenone)(α-hydroxyiminopropiophenonato)ruthenium(III)

Base Information

Chemical Name:dichloro(α-hydroxyiminopropiophenone)(α-hydroxyiminopropiophenonato)ruthenium(III)
CAS No.:82108-96-1
Molecular Formula:C₁₈H₁₇Cl₂N₂O₄Ru
Molecular Weight:497.32
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dichloro(α-hydroxyiminopropiophenone)(α-hydroxyiminopropiophenonato)ruthenium(III)

Chemical Property:

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Technology Process of dichloro(α-hydroxyiminopropiophenone)(α-hydroxyiminopropiophenonato)ruthenium(III)

There total 1 articles about dichloro(α-hydroxyiminopropiophenone)(α-hydroxyiminopropiophenonato)ruthenium(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 14898-67-0
ruthenium(III) chloride trihydrate

: 119-51-7
1-phenyl-1,2-propanedione 2-oxime

: 82108-96-1
dichloro(α-hydroxyiminopropiophenone)(α-hydroxyiminopropiophenonato)ruthenium(III)

Guidance literature:: With LiCl; In ethanol; byproducts: HCl; stirring of starting compds. in ethanol at 50°C for 2 h; cooling to 0°C, filtration, washing with water and diethyl ether, vac. drying over P4O10, dissolving in CH2Cl2, chromy. (SiO2, benzene),crystn. by addn. of hexane to benzene eluate at 25°C, elem. anal.;
DOI:10.1039/DT9820000615

Reference yield:

: 82108-96-1
dichloro(α-hydroxyiminopropiophenone)(α-hydroxyiminopropiophenonato)ruthenium(III)

: 7632-00-0
sodium nitrite

: 174094-72-5
[RuC₉H₈N₂O₃Cl₂]2

Guidance literature:: With HCl; In methanol; trituration (323 K, 2 h), extn. (CHCl3); soln. evapn. (red. pressure), pptn., washing (ether), redissoln. (methanol-water), soln. evapn., pptn., drying (vac.); IR monitoring at 1900 cm**-1, elem. anal.;

Reference yield:

: 544-16-1
n-Butyl nitrite

: 82108-96-1
dichloro(α-hydroxyiminopropiophenone)(α-hydroxyiminopropiophenonato)ruthenium(III)

: 174094-72-5
[RuC₉H₈N₂O₃Cl₂]2

Guidance literature:: In methanol; stirring (298 K, 1 h), cooling; filtration, soln. evapn. (red. pressure), pptn., washing (ether), redissoln. (methanol-water), soln. evapn., pptn., drying (vac.); IR monitoringat 1900 cm**-1, elem. anal.;