3,5-Pyridinedicarboxylic acid, 4-(2,3-dichlorophenyl)-2-[[2-(1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)eth oxy]methyl]-1,4-dihydro-6-methyl-, 5-methyl 3-(1-methylethyl) ester

Base Information

Chemical Name:3,5-Pyridinedicarboxylic acid, 4-(2,3-dichlorophenyl)-2-[[2-(1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)eth oxy]methyl]-1,4-dihydro-6-methyl-, 5-methyl 3-(1-methylethyl) ester
CAS No.:140171-54-6
Molecular Formula:C29H28Cl2N2O7
Molecular Weight:587.457
Hs Code.:

3,5-Pyridinedicarboxylic acid,
4-(2,3-dichlorophenyl)-2-[[2-(1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)eth
oxy]methyl]-1,4-dihydro-6-methyl-, 5-methyl 3-(1-methylethyl) ester

Synonyms:

Suppliers and Price of 3,5-Pyridinedicarboxylic acid, 4-(2,3-dichlorophenyl)-2-[[2-(1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)eth oxy]methyl]-1,4-dihydro-6-methyl-, 5-methyl 3-(1-methylethyl) ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,5-Pyridinedicarboxylic acid, 4-(2,3-dichlorophenyl)-2-[[2-(1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)eth oxy]methyl]-1,4-dihydro-6-methyl-, 5-methyl 3-(1-methylethyl) ester

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Technology Process of 3,5-Pyridinedicarboxylic acid, 4-(2,3-dichlorophenyl)-2-[[2-(1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)eth oxy]methyl]-1,4-dihydro-6-methyl-, 5-methyl 3-(1-methylethyl) ester

There total 4 articles about 3,5-Pyridinedicarboxylic acid, 4-(2,3-dichlorophenyl)-2-[[2-(1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)eth oxy]methyl]-1,4-dihydro-6-methyl-, 5-methyl 3-(1-methylethyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 21731-17-9
methyl 3-aminocrotonate

: 112641-83-5
2-propyl 4-<2-(phthalimido)ethoxy>acetoacetate

: 6334-18-5
2,3-dichlorobenzylaldehyde

: 140171-54-6
4-(2,3-Dichloro-phenyl)-2-[2-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-ethoxymethyl]-6-methyl-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-isopropyl ester 5-methyl ester

Guidance literature:: Heating;
DOI:10.1016/0223-5234(91)90132-7

Reference yield:

: 105-45-3
acetoacetic acid methyl ester

: 140171-54-6
4-(2,3-Dichloro-phenyl)-2-[2-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-ethoxymethyl]-6-methyl-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-isopropyl ester 5-methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: NH₃ / ethanol

2: 63 percent / Heating

With ammonia; In ethanol;
DOI:10.1016/0223-5234(91)90132-7

Reference yield:

: 3891-07-4
N-(2-Hydroxyethyl)phthalimide

: 140171-54-6
4-(2,3-Dichloro-phenyl)-2-[2-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-ethoxymethyl]-6-methyl-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-isopropyl ester 5-methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: NaH / 1.) THF, RT, 1 h, 2.) THF, RT, 18 h

2: 63 percent / Heating

With sodium hydride;
DOI:10.1016/0223-5234(91)90132-7