Diphenyl 8-Methyl-1-nonanol Phosphate

Base Information

• Chemical Name: Diphenyl 8-Methyl-1-nonanol Phosphate
• CAS No.: 1346599-15-2
• Molecular Formula: C₂₂H₃₁O₄P
• Molecular Weight: 390.459
• Mol file: 1346599-15-2.mol

Synonyms:

Chemical Property of Diphenyl 8-Methyl-1-nonanol Phosphate

Chemical Property:

Purity/Quality:

Diphenyl8-Methyl-1-nonanolPhosphate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Uses: An intermediate of Capsaicin (C175682).

Technology Process of Diphenyl 8-Methyl-1-nonanol Phosphate

There total 3 articles about Diphenyl 8-Methyl-1-nonanol Phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

8-methyl-1-nonanol (55505-26-5) + phosphoric acid triphenyl ester (115-86-6) + O-phenyl phosphorodichloridate (770-12-7) + chlorophosphoric acid diphenyl ester (2524-64-3) → isodecyl diphenyl phosphate (1346599-15-2) + diphenyl hydrogen phosphate (838-85-7) + isodecyl chloride + bis(isodecyl) phenyl phosphate

Guidance literature:

magnesium chloride; at 20 - 120 ℃; for 4h; under 50 - 100 Torr; Product distribution / selectivity;

Reference yield:

8-methyl-1-nonanol (55505-26-5) + phosphoric acid triphenyl ester (115-86-6) + O-phenyl phosphorodichloridate (770-12-7) + chlorophosphoric acid diphenyl ester (2524-64-3) → isodecyl diphenyl phosphate (1346599-15-2) + diphenyl hydrogen phosphate (838-85-7) + isodecyl chloride + bis(isodecyl) phenyl phosphate + phenol (108-95-2,27073-41-2)

Guidance literature:

magnesium chloride; at 90 - 100 ℃; for 7h; under 50 Torr; Product distribution / selectivity;

Reference yield:

→ isodecyl diphenyl phosphate (1346599-15-2)

Guidance literature:

upstream raw materials:

8-methyl-1-nonanol

phosphoric acid triphenyl ester

O-phenyl phosphorodichloridate

chlorophosphoric acid diphenyl ester

Refernces

• 1、 -. "Process for the production of organic phosphates". . . Retrieved 2008/06/13.