Tert-butyl 5-iodopentylcarbamate

Base Information

Chemical Name:Tert-butyl 5-iodopentylcarbamate
CAS No.:262278-05-7
Molecular Formula:C₁₀H₂₀INO₂
Molecular Weight:313.179
Hs Code.:
European Community (EC) Number:849-505-5

Synonyms:tert-butyl 5-iodopentylcarbamate;262278-05-7;(5-Iodo-pentyl)-carbamic acid tert-butyl ester;tert-butyl N-(5-iodopentyl)carbamate;tert-butyl (5-iodopentyl)carbamate;tert-butyl5-iodopentylcarbamate;SCHEMBL2702906;ARXOWAUDEJFDNC-UHFFFAOYSA-N;BS-52396;CS-0312164;E83936;EN300-7210604

Suppliers and Price of Tert-butyl 5-iodopentylcarbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of Tert-butyl 5-iodopentylcarbamate

Chemical Property:

XLogP3:3.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:7
Exact Mass:313.05388
Heavy Atom Count:14
Complexity:166

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(C)(C)OC(=O)NCCCCCI

Technology Process of Tert-butyl 5-iodopentylcarbamate

There total 5 articles about Tert-butyl 5-iodopentylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 142342-55-0
diethyl {5-[(tert-butoxycarbonyl)amino]pentyl }-propanedioate

: 262278-05-7
tert-butyl (5-iodo-pentyl)-carbamate

Guidance literature:: With potassium iodide; In N,N-dimethyl-formamide; at 70 ℃; for 2h;
DOI:10.1016/j.bmcl.2012.06.051

Reference yield: 92.0%

: 75178-90-4
N-(tert-butyloxycarbonyl)-5-aminopentanol

: 262278-05-7
tert-butyl (5-iodo-pentyl)-carbamate

Guidance literature:: With 1H-imidazole; iodine; triphenylphosphine; In dichloromethane; at 0 - 20 ℃; for 4h; Inert atmosphere; Cooling with ice;
DOI:10.1021/jacs.7b04312

Reference yield:

: 2508-29-4
5-hydroxypentylamine

: 262278-05-7
tert-butyl (5-iodo-pentyl)-carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: dichloromethane / 2 h / 20 °C / Inert atmosphere

2: triethylamine / dichloromethane / 3 h / -10 °C

3: potassium iodide / N,N-dimethyl-formamide / 2 h / 70 °C

With triethylamine; potassium iodide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.06.051