3-Methoxycyclohexanone

Base Information

• Chemical Name: 3-Methoxycyclohexanone
• CAS No.: 17429-00-4
• Molecular Formula: C7H12O2
• Molecular Weight: 128.171
• Mol file: 17429-00-4.mol

Synonyms:3-methoxy-cyclohexanone;3-methoxy-cyclo-hexanone;3-Methoxy-cyclohexanon;3-methoxycylohexanone;

Chemical Property of 3-Methoxycyclohexanone

Chemical Property:

• Vapor Pressure: 0.574mmHg at 25°C
• PSA: 26.30000
• LogP: 1.14450
• Storage Temp.: 2-8°C

Purity/Quality:

98%min ^*data from raw suppliers

3-Methoxy-cyclohexanone ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-Methoxycyclohexanone

There total 9 articles about 3-Methoxycyclohexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

1,1,3-trimethoxycyclohexane (114377-54-7) → 3-methoxy-cyclohexanone (17429-00-4)

Guidance literature:

acidic hydrolysis;

DOI:10.1021/jo00246a051

Reference yield: 93.0%

methanol (67-56-1) + cyclohexenone (930-68-7) → 3-methoxy-cyclohexanone (17429-00-4)

Guidance literature:

With dmap; lithium perchlorate; at -20 ℃; for 85h; under 1520000 Torr;

DOI:10.1246/cl.2002.296

Reference yield:

methanol (67-56-1) + cyclohexene (110-83-8) → cyclohexenone (930-68-7) + 1-methoxy-cyclohex-1-ene (931-57-7) + 3-methoxy-cyclohexanone (17429-00-4)

Guidance literature:

With oxygen; at 100 ℃; under 4137.29 Torr; Autoclave;

DOI:10.1007/s11164-010-0169-7

upstream raw materials:

cyclohexane-1,3-diol

methyl iodide

1,1,3-trimethoxycyclohexane

methanol

Downstream raw materials:

2-cyclohexenone 2,4-dinitrophenylhydrazone

O-methylresorcine

7-methoxycoumarin