3,5-dichloro-N-Methoxy-N-MethylbenzaMide

Base Information

• Chemical Name: 3,5-dichloro-N-Methoxy-N-MethylbenzaMide
• CAS No.: 259796-12-8
• Molecular Formula: C9H9Cl2NO2
• Molecular Weight: 234.082
• Hs Code.: 2924299090
• Mol file: 259796-12-8.mol

Synonyms:Benzamide,3,5-dichloro-N-methoxy-N-methyl;3,5-dichloro-N-methoxy-N-methyl-benzamide;

Chemical Property of 3,5-dichloro-N-Methoxy-N-MethylbenzaMide

Chemical Property:

• PSA: 29.54000
• LogP: 2.62680
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

3,5-Dichloro-N-methoxy-N-methylbenzamide 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3,5-dichloro-N-Methoxy-N-MethylbenzaMide

There total 4 articles about 3,5-dichloro-N-Methoxy-N-MethylbenzaMide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

3,5-dichlorobenzoyl chloride (2905-62-6) + N,O-dimethylhydroxylamine*hydrochloride (6638-79-5) → 3,5-dichloro-N-methoxy-N-methylbenzamide (259796-12-8)

Guidance literature:

With pyridine; In dichloromethane; at 0 ℃; for 5h;

Reference yield: 93.0%

ring-opening metathesis polymer; monomer(s): exo-N-(3,5-dichlorobenzoyl)oxy-7-oxabicyclo[2.2.1]hept-5-ene-2,3-dicarboximide; benzylidenebis(tricyclohexylphosphine)dichlororuthenium; ethyl vinyl ester + N,0-dimethylhydroxylamine (1117-97-1) → 3,5-dichloro-N-methoxy-N-methylbenzamide (259796-12-8)

Guidance literature:

With triethylamine;

DOI:10.1021/ol991208w

Reference yield:

3,5-dichlorobenzoic acid (51-36-5) + N,O-dimethylhydroxylamine*hydrochloride (6638-79-5) → 3,5-dichloro-N-methoxy-N-methylbenzamide (259796-12-8)

Guidance literature:

3,5-dichlorobenzoic acid; With thionyl chloride; In toluene; for 4h; Reflux;

N,O-dimethylhydroxylamine*hydrochloride; With potassium carbonate; In toluene; at 0 - 20 ℃; for 6.5h; Temperature;

upstream raw materials:

N,0-dimethylhydroxylamine

3,5-dichlorobenzoyl chloride

N,O-dimethylhydroxylamine*hydrochloride

3,5-dichlorobenzoic acid

Downstream raw materials:

3',5'-dichloroacetophenone

(3-bromophenyl)-(3,5-dichlorophenyl)methanone

(5-bromopyridin-2-yl)-(3,5-dichlorophenyl)methanone

1-(3,5-dichlorophenyl)propan-1-one

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