1,1,5-Trichloro-1-pentene

Base Information

• Chemical Name: 1,1,5-Trichloro-1-pentene
• CAS No.: 2677-33-0
• Molecular Formula: C5H7Cl3
• Molecular Weight: 173.47
• Hs Code.: 2903299090
• Mol file: 2677-33-0.mol

Synonyms:1,1,5-trichloropentene;1,1-Dichloro-1-pentenyl chloride;1,1,5-Trichlor-pent-1-en;1,1,5-Trichlor-penten-(1);1-Pentene,1,1,5-trichloro;1,1,5-trichloro-1-pentene;1,1,5-trichloro-pent-1-ene;1,1,5-Trichlor-1-penten;1,1,5-Trichloro-1-penten;1-Pentene, 1,1,5-trichloro-;

Chemical Property of 1,1,5-Trichloro-1-pentene

Chemical Property:

• PSA: 0.00000
• LogP: 3.32440

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,1,5-Trichloro-1-pentene

There total 2 articles about 1,1,5-Trichloro-1-pentene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tetrachloromethane (56-23-5) + ethene (74-85-1) → 1,1,1,5-tetrachloropentane (2467-10-9) + 1,1,5-trichloro-pent-1-ene (2677-33-0) + 1,1,1,3-tetrachloropropane (1070-78-6) + 1,1,1,3-tetrachlorobutane (13275-19-9)

Guidance literature:

With diethyl amine hydrochloride; 2-hydroxy-2-phenylacetophenone; iron(III) chloride; In isopropyl alcohol; Further byproducts given;

DOI:10.1021/jo00981a028

Reference yield:

tetrachloromethane (56-23-5) + ethene (74-85-1) → 1,1,1,5-tetrachloropentane (2467-10-9) + 1,1,5-trichloro-pent-1-ene (2677-33-0) + 1,1,1,3-tetrachloropropane (1070-78-6) + 1,3,5-trichloro-2-pentene (34909-84-7)

Guidance literature:

With diethyl amine hydrochloride; 2-hydroxy-2-phenylacetophenone; In isopropyl alcohol; Further byproducts given;

DOI:10.1021/jo00981a028

Reference yield: 54.0%

1,1,5-trichloro-pent-1-ene (2677-33-0) + methylmagnesium chloride (676-58-4) → 1-chloro-5-methyl-4-hexene (100959-06-6) + 1-chloro-4-octyne (51575-84-9) + (E)-1-Chloro-oct-4-ene (85217-45-4)

Guidance literature:

bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; Heating;

upstream raw materials:

tetrachloromethane

ethene

Downstream raw materials:

5-chloro-valeric acid

1,1,5-Trichlor-2-p-xylylpentan

1,1-Dichlor-5-(p-tolylsulfonyl)-1-penten

1,1,5,5-Tetrachlor-pentan