4'-Methoxyacetophenone dimethyl acetal

Base Information

• Chemical Name: 4'-Methoxyacetophenone dimethyl acetal
• CAS No.: 27150-99-8
• Molecular Formula: C11H16O3
• Molecular Weight: 196.246
• Hs Code.: 2911000000
• Mol file: 27150-99-8.mol

Synonyms:1,1-dimethoxy-1-(4-methoxyphenyl)ethane;4-methoxyacetophenone dimethyl ketal;4-methoxy-(1,1-dimethoxyethyl)benzene;4-methoxyacetophenone dimethyl acetal;4-methoxy-(1,1-dimethoxyethyl)-benzene;p-methoxyacetophenone dimethyl acetal;

Chemical Property of 4'-Methoxyacetophenone dimethyl acetal

Chemical Property:

• PSA: 27.69000
• LogP: 2.16070

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4'-Methoxyacetophenone dimethyl acetal

There total 11 articles about 4'-Methoxyacetophenone dimethyl acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

1-(4-methoxyphenyl)ethanone (100-06-1) + trimethyl orthoformate (149-73-5) → 1,1-dimethoxy-1-(4-methoxyphenyl)ethane (27150-99-8)

Guidance literature:

With Pd(PhCN)₂(OTf)₂; In methanol; at 20 ℃; Inert atmosphere;

DOI:10.1055/s-0039-1690497

Reference yield: 85.0%

methanol (67-56-1) + 1-(4-methoxyphenyl)ethanone (100-06-1) + trimethyl orthoformate (149-73-5) → 1,1-dimethoxy-1-(4-methoxyphenyl)ethane (27150-99-8)

Guidance literature:

With toluene-4-sulfonic acid; Heating;

Reference yield:

methanol (67-56-1) + 4-Methoxystyrene (637-69-4,24936-44-5) → 1,1-dimethoxy-1-(4-methoxyphenyl)ethane (27150-99-8) + 1-(4-methoxyphenyl)ethanone (100-06-1)

Guidance literature:

With Pd((-)-sparteine)2Cl₂; 3 A molecular sieve; oxygen; copper dichloride; at 20 ℃; for 24h;

DOI:10.1021/ol053110p

upstream raw materials:

methanol

1-Methoxy-4-(1-methoxy-vinyl)-benzene

2,2-dimethoxy-propane

1-(4-methoxyphenyl)ethanone

Downstream raw materials:

methyl 4,6-O-<(4-methoxyphenyl)ethylidene>-α-D-glucopyranoside

2,3-O-<(4-methoxyphenyl)ethylidene>ribonic acid γ-lactone

methanol

1-Methoxy-4-(1-methoxy-vinyl)-benzene