3-Methoxy-4-[(trimethylsilyl)oxy]benzoic acid methyl ester

Base Information

• Chemical Name: 3-Methoxy-4-[(trimethylsilyl)oxy]benzoic acid methyl ester
• CAS No.: 27798-53-4
• Molecular Formula: C₁₂H₁₈O₄Si
• Molecular Weight: 254.358
• Hs Code.: 2931900090
• Mol file: 27798-53-4.mol

Synonyms:Benzoic acid,3-methoxy-4-[(trimethylsilyl)oxy]-,methyl ester;m-Anisic acid,4-(trimethylsiloxy)-,methyl ester;Methyl 3-methoxy-4-[(trimethylsilyl)oxy]benzoate;3-methoxy-4-trimethylsilyloxy-benzoic acid methyl ester;

Chemical Property of 3-Methoxy-4-[(trimethylsilyl)oxy]benzoic acid methyl ester

Chemical Property:

• PSA: 44.76000
• LogP: 2.69550

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-Methoxy-4-[(trimethylsilyl)oxy]benzoic acid methyl ester

There total 4 articles about 3-Methoxy-4-[(trimethylsilyl)oxy]benzoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methanol (67-56-1) + 2-(4-hydroxy-3-methoxyphenyl)-2-methoxyacetonitrile (1000180-41-5) + N-methyl-N-trimethylsilyl-2,2,2-trifluoroacetamide (24589-78-4) → C14H21NO4Si (1000180-56-2) + 3-methoxy-4-trimethylsilyloxy-benzoic acid methyl ester (27798-53-4)

Guidance literature:

methanol; 2-(4-hydroxy-3-methoxyphenyl)-2-methoxyacetonitrile; With manganese(IV) oxide; water; for 24h;

N-methyl-N-trimethylsilyl-2,2,2-trifluoroacetamide; Further stages.;

DOI:10.1002/anie.200702481

Reference yield:

4-hydroxy-3-methoxybenzoic acid methyl ester (3943-74-6) + N,O-Bis(trimethylsilyl)trifluoroacetamide (25561-30-2) → 3-methoxy-4-trimethylsilyloxy-benzoic acid methyl ester (27798-53-4)

Guidance literature:

at 20 ℃; for 16h;

DOI:10.3109/00498259509046666

Reference yield:

N,O-bis-(trimethylsilyl)-acetamide (10416-59-8) + 4-hydroxy-3-methoxybenzoic acid methyl ester (3943-74-6) → 3-methoxy-4-trimethylsilyloxy-benzoic acid methyl ester (27798-53-4)

Guidance literature:

In tetrachloromethane;

DOI:10.1002/oms.1210201005

upstream raw materials:

N,O-bis-(trimethylsilyl)-acetamide

4-hydroxy-3-methoxybenzoic acid methyl ester

N,N-bis(trimethylsilyl)acetamide

N,O-Bis(trimethylsilyl)trifluoroacetamide

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