(2,4-(CF₃)2C₆H₃)2BF*OEt₂

Base Information

Chemical Name:(2,4-(CF₃)2C₆H₃)2BF*OEt₂
CAS No.:681812-10-2
Molecular Formula:C₂₀H₁₆BF₁₃O
Molecular Weight:530.137
Hs Code.:

(2,4-(CF<sub>3</sub>)2C<sub>6</sub>H<sub>3</sub>)2BF*OEt<sub>2</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2,4-(CF₃)2C₆H₃)2BF*OEt₂

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Technology Process of (2,4-(CF₃)2C₆H₃)2BF*OEt₂

There total 1 articles about (2,4-(CF₃)2C₆H₃)2BF*OEt₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 136664-85-2
2,4-(CF₃)2C₆H₃Li

: 60-29-7,927820-24-4
diethyl ether

: 10294-34-5
boron trichloride

: 80426-23-9
(2,6-bis(trifluoromethyl)-phenyl)lithium

: 681812-10-2
(2,4-(CF₃)2C₆H₃)2BF*OEt₂

: 681812-04-4
2,6-(CF₃)2C₆H₃BCl₂

: 681812-05-5
bis(2,6-bis(trifluoromethyl)phenyl)fluoroborane

: tris-(2,4-bis(trifluoromethyl)phenyl) borane

Guidance literature:: In diethyl ether; under an inert atm.; to a soln. of an excess of Li-contg. compds. in hexanes and Et2O was added dropwise B-contg. compd. (1 M in heptane) at -78°C ; the react. mixt. was allowed to warm to room temp. for 1 h; further addn. of BCl3; the solvents were removed under vac.; a mixt. of yellow oil and white solid; detd. by NMR;
DOI:10.1039/b309820f