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Basic Information
| CAS No.: | 100-83-4 |
|---|---|
| Name: | 3-Hydroxybenzaldehyde |
| Molecular Structure: | |
|
|
|
| Formula: | C7H6O2 |
| Molecular Weight: | 122.123 |
| Synonyms: | meta-Hydroxybenzaldehyde;Benzaldehyde, 3-hydroxy-;m-Formylphenol;3-Formylphenol;3-hydroxyBenzaldehyde;m-hydroxyBenzaldehyde;m-hydroxybenzaldehyde;Benzaldehyde, m-hydroxy-; |
| EINECS: | 202-892-9 |
| Density: | 1.226 g/cm 3 |
| Melting Point: | 100-103 °C(lit.) |
| Boiling Point: | 240.9 °C at 760 mmHg |
| Flash Point: | 98.6 °C |
| Solubility: | soluble in water |
| Appearance: | off-white solid |
| Hazard Symbols: |
 Xi
|
| Risk Codes: | 36/37/38 |
| Safety: | 26-36-24/25 |
| PSA: | 37.30000 |
| LogP: | 1.20470 |
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Synthetic route
Conditions
| Conditions | Yield |
|---|---|
| With silica gel; 4-acetylamino-2,2,6,6-tetramethylpiperidine-1-oxoammonium perchlorate In dichloromethane | 100% |
| With manganese(IV) oxide; manganese(II) nitrate tetrahydrate; dibenzoyl peroxide In hexane at 70℃; under 760.051 Torr; for 0.0833333h; chemoselective reaction; | 99% |
| In neat (no solvent) at 20℃; for 0.0333333h; Microwave irradiation; | 99% |
- 100-83-4
meta-hydroxybenzaldehyde
Conditions
| Conditions | Yield |
|---|---|
| With hydrogenchloride for 0.0416667h; Product distribution; Ambient temperature; pH = 4-6, regeneration of aldehyde; | 100% |
Conditions
| Conditions | Yield |
|---|---|
| With iron(III) chloride on silica In neat (no solvent) at 80℃; for 0.5h; | 99% |
| With magnesium iodide for 5h; neat (no solvent); | 93% |
- 96013-95-5
3-(tert-butyl-dimethyl-sylanyloxy)benzaldehyde
- 100-83-4
meta-hydroxybenzaldehyde
Conditions
| Conditions | Yield |
|---|---|
| With lithium acetate In water; N,N-dimethyl-formamide at 25℃; for 8h; Inert atmosphere; | 96% |
| With triethylamine N-oxide In methanol for 1h; | 91% |
| In water; dimethyl sulfoxide at 90℃; for 8h; | 87% |
- 27004-28-0
2-(3-hydroxyphenyl)-1,3-dithiolane
- 100-83-4
meta-hydroxybenzaldehyde
Conditions
| Conditions | Yield |
|---|---|
| With ammonium iodide; dihydrogen peroxide; sodium dodecyl-sulfate In water at 20℃; for 1h; micellar medium; | 96% |
| With 2,4,4,6-Tetrabromo-2,5-cyclohexadien-1-one; dihydrogen peroxide In water; acetonitrile at 20℃; for 1h; | 94% |
| With dihydrogen peroxide; iodine; sodium dodecyl-sulfate In water at 20℃; for 3h; Micellar solution; | 90% |
- 24393-20-2
2-(3-hydroxyphenyl)-1,3-dithiane
- 100-83-4
meta-hydroxybenzaldehyde
Conditions
| Conditions | Yield |
|---|---|
| With dihydrogen peroxide; iodine; sodium dodecyl-sulfate In water at 20℃; for 0.666667h; Micellar solution; | 95% |
| With acetic acid at 25℃; for 15h; | 51% |
- 13493-49-7
3-benzenesulfonyloxy-benzaldehyde
- 100-83-4
meta-hydroxybenzaldehyde
Conditions
| Conditions | Yield |
|---|---|
| With potassium hydroxide In toluene; tert-butyl alcohol at 100℃; for 0.5h; Inert atmosphere; | 95% |
- 87199-16-4
3-Formylphenylboronic acid
- 100-83-4
meta-hydroxybenzaldehyde
Conditions
| Conditions | Yield |
|---|---|
| With C100H52N4O16Sn(6-)*2In(3+); N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide for 3.5h; Irradiation; | 94% |
| With C18H28Cl2CuN2O4 In water at 26℃; for 0.333333h; | 92% |
| With 10-methylacridine-3(10H)-one; oxygen; N-ethyl-N,N-diisopropylamine In water at 20℃; for 20h; Irradiation; Green chemistry; | 90% |
- 40359-32-8
3-allyloxy-benzaldehyde
- 100-83-4
meta-hydroxybenzaldehyde
Conditions
| Conditions | Yield |
|---|---|
| With bis(benzonitrile)palladium(II) dichloride In benzene for 20h; Heating; | 92% |
| With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In methanol at 20℃; for 6h; | 82% |
- 817166-73-7
3-((triisopropylsilyl)oxy)benzaldehyde
- 100-83-4
meta-hydroxybenzaldehyde
Conditions
| Conditions | Yield |
|---|---|
| With potassium acetate In water; N,N-dimethyl-formamide at 25℃; for 13h; | 92% |
Raw Materials
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3-Hydroxybenzaldehyde
Chemistry
Product Name: 3-Hydroxybenzaldehyde
Synonyms: hydroxybenzaldehyde;m-Aldehydophenol;m-Formylphenol;m-hydroxy-benzaldehyd;3-hydroxy-benzaldehyd;Benzaldehyde, m-hydroxy-;HYDROXYBENZALDEHYDE-3; META-HYDROXY BENZALDEHYDE;
The Molecular formula of m-FORMYLPHENOL(100-83-4): C7H6O2
The Molecular Weight of m-FORMYLPHENOL(100-83-4): 122.12
Molecular Structure :
EINECS: 202-892-9
Melting point: 100-103 °C(lit.)
Boiling point: 191 °C50 mm Hg(lit.)
Flash point: 191°C/50mm
Water Solubility: SOLUBLE
Sensitive: Air Sensitive
Appearance: Off-White Solid
Synonyms: hydroxybenzaldehyde;m-Aldehydophenol;m-Formylphenol;m-hydroxy-benzaldehyd;3-hydroxy-benzaldehyd;Benzaldehyde, m-hydroxy-;HYDROXYBENZALDEHYDE-3; META-HYDROXY BENZALDEHYDE;
The Molecular formula of m-FORMYLPHENOL(100-83-4): C7H6O2
The Molecular Weight of m-FORMYLPHENOL(100-83-4): 122.12
Molecular Structure :
EINECS: 202-892-9
Melting point: 100-103 °C(lit.)
Boiling point: 191 °C50 mm Hg(lit.)
Flash point: 191°C/50mm
Water Solubility: SOLUBLE
Sensitive: Air Sensitive
Appearance: Off-White Solid
Toxicity Data With Reference
| 1. | sce-hmn:lyms 1 mmol/L | MUREAV Mutation Research. 206 (1988),17. |
Consensus Reports
Reported in EPA TSCA Inventory.
Safety Profile
Human mutation data reported. When heated to decomposition it emits acrid smoke and irritating vapors.
The Hazard Codes of m-FORMYLPHENOL(100-83-4):
Xi
The Risk Statements information of m-FORMYLPHENOL(100-83-4):
36/37/38: Irritating to eyes, respiratory system and skin
The Safety Statements information of m-FORMYLPHENOL(100-83-4):
26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice
36: Wear suitable protective clothing
24/25: Avoid contact with skin and eyes
WGK Germany: 3
RTECS: CU6450000
F: 8-9-23
The Hazard Codes of m-FORMYLPHENOL(100-83-4):
Xi The Risk Statements information of m-FORMYLPHENOL(100-83-4):
36/37/38: Irritating to eyes, respiratory system and skin
The Safety Statements information of m-FORMYLPHENOL(100-83-4):
26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice
36: Wear suitable protective clothing
24/25: Avoid contact with skin and eyes
WGK Germany: 3
RTECS: CU6450000
F: 8-9-23