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100-83-4

Basic Information
CAS No.: 100-83-4
Name: 3-Hydroxybenzaldehyde
Article Data: 172
Cas Database
Molecular Structure:
Molecular Structure of 100-83-4 (3-Hydroxybenzaldehyde)
Formula: C7H6O2
Molecular Weight: 122.123
Synonyms: meta-Hydroxybenzaldehyde;Benzaldehyde, 3-hydroxy-;m-Formylphenol;3-Formylphenol;3-hydroxyBenzaldehyde;m-hydroxyBenzaldehyde;m-hydroxybenzaldehyde;Benzaldehyde, m-hydroxy-;
EINECS: 202-892-9
Density: 1.226 g/cm 3
Melting Point: 100-103 °C(lit.)
Boiling Point: 240.9 °C at 760 mmHg
Flash Point: 98.6 °C
Solubility: soluble in water
Appearance: off-white solid
Hazard Symbols: IrritantXi
Risk Codes: 36/37/38
Safety: 26-36-24/25
Transport Information: N/A
PSA: 37.30000
LogP: 1.20470
Synthetic route
620-24-6

3-Hydroxybenzyl alcohol

100-83-4

meta-hydroxybenzaldehyde

Conditions
ConditionsYield
With silica gel; 4-acetylamino-2,2,6,6-tetramethylpiperidine-1-oxoammonium perchlorate In dichloromethane100%
With manganese(IV) oxide; manganese(II) nitrate tetrahydrate; dibenzoyl peroxide In hexane at 70℃; under 760.051 Torr; for 0.0833333h; chemoselective reaction;99%
In neat (no solvent) at 20℃; for 0.0333333h; Microwave irradiation;99%

Sodium; 6-{[1-(3-hydroxy-phenyl)-meth-(E)-ylidene]-amino}-hexanoate

100-83-4

meta-hydroxybenzaldehyde

Conditions
ConditionsYield
With hydrogenchloride for 0.0416667h; Product distribution; Ambient temperature; pH = 4-6, regeneration of aldehyde;100%
1700-37-4

3-Benzyloxybenzaldehyde

100-83-4

meta-hydroxybenzaldehyde

Conditions
ConditionsYield
With iron(III) chloride on silica In neat (no solvent) at 80℃; for 0.5h;99%
With magnesium iodide for 5h; neat (no solvent);93%
96013-95-5

3-(tert-butyl-dimethyl-sylanyloxy)benzaldehyde

100-83-4

meta-hydroxybenzaldehyde

Conditions
ConditionsYield
With lithium acetate In water; N,N-dimethyl-formamide at 25℃; for 8h; Inert atmosphere;96%
With triethylamine N-oxide In methanol for 1h;91%
In water; dimethyl sulfoxide at 90℃; for 8h;87%
27004-28-0

2-(3-hydroxyphenyl)-1,3-dithiolane

100-83-4

meta-hydroxybenzaldehyde

Conditions
ConditionsYield
With ammonium iodide; dihydrogen peroxide; sodium dodecyl-sulfate In water at 20℃; for 1h; micellar medium;96%
With 2,4,4,6-Tetrabromo-2,5-cyclohexadien-1-one; dihydrogen peroxide In water; acetonitrile at 20℃; for 1h;94%
With dihydrogen peroxide; iodine; sodium dodecyl-sulfate In water at 20℃; for 3h; Micellar solution;90%
24393-20-2

2-(3-hydroxyphenyl)-1,3-dithiane

100-83-4

meta-hydroxybenzaldehyde

Conditions
ConditionsYield
With dihydrogen peroxide; iodine; sodium dodecyl-sulfate In water at 20℃; for 0.666667h; Micellar solution;95%
With acetic acid at 25℃; for 15h;51%
13493-49-7

3-benzenesulfonyloxy-benzaldehyde

100-83-4

meta-hydroxybenzaldehyde

Conditions
ConditionsYield
With potassium hydroxide In toluene; tert-butyl alcohol at 100℃; for 0.5h; Inert atmosphere;95%
87199-16-4

3-Formylphenylboronic acid

100-83-4

meta-hydroxybenzaldehyde

Conditions
ConditionsYield
With C100H52N4O16Sn(6-)*2In(3+); N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide for 3.5h; Irradiation;94%
With C18H28Cl2CuN2O4 In water at 26℃; for 0.333333h;92%
With 10-methylacridine-3(10H)-one; oxygen; N-ethyl-N,N-diisopropylamine In water at 20℃; for 20h; Irradiation; Green chemistry;90%
40359-32-8

3-allyloxy-benzaldehyde

100-83-4

meta-hydroxybenzaldehyde

Conditions
ConditionsYield
With bis(benzonitrile)palladium(II) dichloride In benzene for 20h; Heating;92%
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In methanol at 20℃; for 6h;82%
817166-73-7

3-((triisopropylsilyl)oxy)benzaldehyde

100-83-4

meta-hydroxybenzaldehyde

Conditions
ConditionsYield
With potassium acetate In water; N,N-dimethyl-formamide at 25℃; for 13h;92%
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Chemistry

Product Name: 3-Hydroxybenzaldehyde
Synonyms: hydroxybenzaldehyde;m-Aldehydophenol;m-Formylphenol;m-hydroxy-benzaldehyd;3-hydroxy-benzaldehyd;Benzaldehyde, m-hydroxy-;HYDROXYBENZALDEHYDE-3; META-HYDROXY BENZALDEHYDE;
The Molecular formula of m-FORMYLPHENOL(100-83-4): C7H6O2
The Molecular Weight of m-FORMYLPHENOL(100-83-4): 122.12
Molecular Structure : 
EINECS: 202-892-9
Melting point: 100-103 °C(lit.)
Boiling point: 191 °C50 mm Hg(lit.)
Flash point: 191°C/50mm
Water Solubility: SOLUBLE
Sensitive: Air Sensitive
Appearance: Off-White Solid

Toxicity Data With Reference

1.   

sce-hmn:lyms 1 mmol/L

   MUREAV    Mutation Research. 206 (1988),17.

Consensus Reports

Reported in EPA TSCA Inventory.

Safety Profile

Human mutation data reported. When heated to decomposition it emits acrid smoke and irritating vapors.
The Hazard Codes of  m-FORMYLPHENOL(100-83-4):   Xi
The Risk Statements information of  m-FORMYLPHENOL(100-83-4):
36/37/38:  Irritating to eyes, respiratory system and skin
The Safety Statements information of  m-FORMYLPHENOL(100-83-4):
26:  In case of contact with eyes, rinse immediately with plenty of water and seek medical advice  
36:  Wear suitable protective clothing 
24/25:  Avoid contact with skin and eyes 
WGK Germany: 3
RTECS: CU6450000
F: 8-9-23