CAS No.102-69-2,N,N-Dipropyl-1-propanamine Suppliers,MSDS download

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Basic Information

Molecular Structure:
CAS No.:	102-69-2
Name:	N,N-Dipropyl-1-propanamine
Article Data:	50

Formula:	C₉H₂₁N
Molecular Weight:	143.272
Synonyms:	Tripropylamine(6CI,8CI);N,N-Dipropyl-1-propanamine;Propyldi-n-propylamine;Tri-n-propylamine;
EINECS:	203-047-7
Density:	0.777 g/cm³
Melting Point:	-93.5 °C(lit.)
Boiling Point:	158.1 °C at 760 mmHg
Flash Point:	36.7 °C
Solubility:	2.6 g/L (20 °C) in water
Appearance:	colourless liquid
Hazard Symbols:	T
Risk Codes:	10-20/21-25-34-52/53-23/25-21
Safety:	26-36/37/39-45-16
Transport Information:	UN 2260 3/PG 3
PSA:	3.24000
LogP:	2.51840

Synthetic route

: 74-85-1
ethene

: 201230-82-2
carbon monoxide

: 142-84-7
di-n-propylamine

: 102-69-2
tri-n-propylamine

Conditions

Conditions	Yield
di(rhodium)tetracarbonyl dichloride In ethanol at 115℃; under 37503 Torr; for 1.5h;	100%

...Expand

: 107-10-8
propylamine

: 74-85-1
ethene

: 201230-82-2
carbon monoxide

A: 102-69-2
tri-n-propylamine

B: 142-84-7
di-n-propylamine

Conditions

Conditions	Yield
di(rhodium)tetracarbonyl dichloride In ethanol at 119℃; under 44253.5 Torr; for 1h;	A 1% B 99%
di(rhodium)tetracarbonyl dichloride In ethanol at 119℃; under 44253.5 Torr; for 1h;	A 2% B 98%

...Expand

: 71-23-8
propan-1-ol

: 111-87-5
octanol

: 107-12-0
propiononitrile

A: 102-69-2
tri-n-propylamine

B: 99209-95-7
Dipropyloctylamin

Conditions

Conditions	Yield
With hydrogen; copper at 240℃; under 7600 Torr;	A n/a B 95%

...Expand

: 71-23-8
propan-1-ol

: 107-12-0
propiononitrile

: 143-08-8
nonyl alcohol

A: 102-69-2
tri-n-propylamine

B: N,N-dipropylnonylamine

Conditions

Conditions	Yield
With hydrogen; copper at 240℃; under 7600 Torr;	A n/a B 90%

...Expand

: 107-12-0
propiononitrile

A: 102-69-2
tri-n-propylamine

B: 7707-70-2
N-propylidenepropylamine

C: 142-84-7
di-n-propylamine

Conditions

Conditions	Yield
With hydrogen at 220℃;	A 8.5% B 2.5% C 89%
With hydrogen at 240℃; Temperature; Flow reactor;	A 13% B 2.5% C 80%

...Expand

: 71-23-8
propan-1-ol

: 112-30-1
1-Decanol

: 107-12-0
propiononitrile

A: 102-69-2
tri-n-propylamine

B: 88090-10-2
N,N-dipropyldecylamine

Conditions

Conditions	Yield
With hydrogen; copper at 240℃; under 7600 Torr;	A n/a B 86%

...Expand

: 71-23-8
propan-1-ol

: 112-42-5
undecyl alcohol

: 107-12-0
propiononitrile

A: 102-69-2
tri-n-propylamine

B: N,N-dipropylundecylamine

Conditions

Conditions	Yield
With hydrogen; copper at 240℃; under 7600 Torr;	A n/a B 80%

...Expand

: 71-23-8
propan-1-ol

: 112-53-8
1-dodecyl alcohol

: 107-12-0
propiononitrile

A: 102-69-2
tri-n-propylamine

B: 30427-39-5
N,N-Dipropyl-dodecyl amine

Conditions

Conditions	Yield
With hydrogen; copper at 240℃; under 7600 Torr;	A n/a B 80%

...Expand

: 71-23-8
propan-1-ol

: 112-72-1
1-Tetradecanol

: 107-12-0
propiononitrile

A: 102-69-2
tri-n-propylamine

B: N,N-dipropyl-tetradecylamine

Conditions

Conditions	Yield
With hydrogen; copper at 240℃; under 7600 Torr;	A n/a B 76%

...Expand

: 71-23-8
propan-1-ol

: 629-76-5
pentadecanol

: 107-12-0
propiononitrile

A: 102-69-2
tri-n-propylamine

B: N,N-dipropylpentadecylamine

Conditions

Conditions	Yield
With hydrogen; copper at 240℃; under 7600 Torr;	A n/a B 75%

...Expand

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Consensus Reports

Reported in EPA TSCA Inventory.

Standards and Recommendations

DOT Classification: 3; Label: Flammable Liquid, Corrosive

Specification

The Tripropylamine is an organic compound with the formula C₉H₂₁N. The IUPAC name of this chemical is N,N-dipropylpropan-1-amine. With the CAS registry number 102-69-2, it is also named as 1-propanamine, N,N-dipropyl-. The product's categories are Amines; C9 to C10; Nitrogen Compounds. Besides, it is colourless liquid, which is used for producting drugs, pesticides, rubber and fiber processing aids, etc.

Physical properties about Tripropylamine are: (1)ACD/LogP: 3.25; (2)ACD/LogD (pH 5.5): 0.17; (3)ACD/LogD (pH 7.4): 0.78; (4)ACD/BCF (pH 5.5): 1; (5)ACD/BCF (pH 7.4): 1; (6)ACD/KOC (pH 5.5): 1.16; (7)ACD/KOC (pH 7.4): 4.71; (8)#H bond acceptors: 1; (9)#Freely Rotating Bonds: 6; (10)Polar Surface Area: 3.24 Å²; (11)Index of Refraction: 1.428; (12)Molar Refractivity: 47.46 cm³; (13)Molar Volume: 184.3 cm³; (14)Polarizability: 18.81×10^-24cm³; (15)Surface Tension: 25.9 dyne/cm; (16)Density: 0.777 g/cm³; (17)Flash Point: 36.7 °C; (18)Enthalpy of Vaporization: 39.48 kJ/mol; (19)Boiling Point: 158.1 °C at 760 mmHg; (20)Vapour Pressure: 2.66 mmHg at 25°C.

Preparation: this chemical can be prepared by 1-nitro-propane. This reaction will need reagent CO, H₂O, catalyst Rh₆(CO)₁₆-amine polymer and solvent 2-ethoxy-ethanol. The reaction time is 48 hours with reaction temperature of 40 °C. The yield is about 32%.

Uses of Tripropylamine: it can be used to produce ethyl-tripropyl-ammonium; iodide by heating. It will need reagent butan-2-one with reaction time of 2 hours. The yield is about 40%.

When you are using this chemical, please be cautious about it as the following:
It is flammable and harmful by inhalation and in contact with skin. It is toxic by inhalation and if swallowed and can cause burns. Please keep away from sources of ignition - No smoking. In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. Besides, this chemical is harmful to aquatic organisms, may cause long-term adverse effects in the aquatic environment. When you are using it, wear suitable gloves and eye/face protection. In case of accident or if you feel unwell seek medical advice immediately (show the label where possible).

You can still convert the following datas into molecular structure:
(1)SMILES: N(CCC)(CCC)CCC
(2)InChI: InChI=1/C9H21N/c1-4-7-10(8-5-2)9-6-3/h4-9H2,1-3H3
(3)InChIKey: YFTHZRPMJXBUME-UHFFFAOYAE
(4)Std. InChI: InChI=1S/C9H21N/c1-4-7-10(8-5-2)9-6-3/h4-9H2,1-3H3
(5)Std. InChIKey: YFTHZRPMJXBUME-UHFFFAOYSA-N

The toxicity data is as follows:

Organism	Test Type	Route	Reported Dose (Normalized Dose)	Source
mammal (species unspecified)	LC50	inhalation	5100mg/m³ (5100mg/m³)	Toksikologiya Novykh Promyshlennykh Khimicheskikh Veshchestv. Toxicology of New Industrial Chemical Substances. For English translation, see TNICS*. Vol. 14, Pg. 80, 1975.
mammal (species unspecified)	LD50	unreported	740mg/kg (740mg/kg)	Toksikologiya Novykh Promyshlennykh Khimicheskikh Veshchestv. Toxicology of New Industrial Chemical Substances. For English translation, see TNICS*. Vol. 14, Pg. 80, 1975.
mouse	LC50	inhalation	3800mg/m³/2H (3800mg/m³)	"Toxicometric Parameters of Industrial Toxic Chemicals Under Single Exposure," Izmerov, N.F., et al., Moscow, Centre of International Projects, GKNT, 1982Vol. -, Pg. 118, 1982.
rabbit	LD50	skin	570uL/kg (0.57mL/kg)	American Industrial Hygiene Association Journal. Vol. 30, Pg. 470, 1969.
rat	LC50	inhalation	5100mg/m³/4H (5100mg/m³)	"Toxicometric Parameters of Industrial Toxic Chemicals Under Single Exposure," Izmerov, N.F., et al., Moscow, Centre of International Projects, GKNT, 1982Vol. -, Pg. 118, 1982.
rat	LD50	oral	96mg/kg (96mg/kg)	American Industrial Hygiene Association Journal. Vol. 30, Pg. 470, 1969.