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102-85-2

Basic Information
CAS No.: 102-85-2
Name: TRIBUTYL PHOSPHITE
Article Data: 45
Molecular Structure:
Molecular Structure of 102-85-2 (TRIBUTYL PHOSPHITE)
Formula: C12H27 O3 P
Molecular Weight: 250.318
Synonyms: 1-Butanol,1,1',1''-phosphinidynetri- (6CI); Butyl phosphite, (BuO)3P (4CI); JP 304; NSC2675; Phosphorus tributoxide (P(OBu)3); Tri-n-butyl phosphite;Tributoxyphosphine; Tributyl phosphite
EINECS: 203-061-3
Density: g/cm3
Melting Point: -80 °C
Boiling Point: 125 °C
Flash Point: 121.1°C
Solubility: Not miscible or difficult to mix in water.
Appearance: Clear colorless liquid
Hazard Symbols:
Risk Codes: 21-34
Safety: Moderately toxic by ingestion and skin contact. A skin and eye irritant. Has been known to damage eyes. Combustible when exposed to heat or flame. To fight fire, use CO2, dry chemical. When heated to decomposition it emits toxic fumes of POx.
PSA: 41.28000
LogP: 4.66340
Synthetic route

O,O-dibutyl (tributoxymethyl)phosphonate

A

102-85-2

tri-n-butyl phosphite

B

542-52-9

Dibutyl carbonate

Conditions
ConditionsYield
With boron trifluoride diethyl etherate under 8 Torr; Heating;A 71%
B n/a

O,O-dibutyl (tributoxymethyl)phosphonate

102-85-2

tri-n-butyl phosphite

Conditions
ConditionsYield
With boron trifluoride diethyl etherate under 8 Torr; Heating;71%
71-36-3

butan-1-ol

102-85-2

tri-n-butyl phosphite

Conditions
ConditionsYield
With potassium phosphate; tetrahexylammonium chloride; phosphorus trichloride In dichloromethane at 20℃; for 3h;69%
With sodium hexachloroplatinate; phosphan at 24.9℃; Rate constant; Kinetics; also in the presence of LiCl, HCl, H2O, LiBr, NaI; var. conc. of reactants;
With ammonia; Petroleum ether; phosphorus trichloride
51104-80-4

diethyl ester of 2-phenylethynylphosphonous acid

71-36-3

butan-1-ol

A

102-85-2

tri-n-butyl phosphite

B

536-74-3

phenylacetylene

Conditions
ConditionsYield
With C4H9ONa Product distribution; Heating; oth. alcohols;A 63%
B n/a
42964-63-6

S,S-diethyl-N-diethylamidodithiophosphite

71-36-3

butan-1-ol

A

688-62-0

triethyl trithiophosphite

B

102-85-2

tri-n-butyl phosphite

Conditions
ConditionsYield
at 160℃; for 8h; Product distribution; Mechanism;A 36%
B 40%
42964-63-6

S,S-diethyl-N-diethylamidodithiophosphite

71-36-3

butan-1-ol

A

688-62-0

triethyl trithiophosphite

B

102-85-2

tri-n-butyl phosphite

C

109-89-7

diethylamine

D

75-08-1

ethanethiol

Conditions
ConditionsYield
at 160℃; for 8h;A 36%
B 40%
C n/a
D n/a
110-86-1

pyridine

10496-13-6

butyl dichlorophosphite

71-36-3

butan-1-ol

102-85-2

tri-n-butyl phosphite

101-02-0

triphenyl phosphite

2372-45-4

sodium butanolate

102-85-2

tri-n-butyl phosphite

Conditions
ConditionsYield
With benzene
10496-13-6

butyl dichlorophosphite

2372-45-4

sodium butanolate

A

4124-92-9

dibutyl chlorophosphite

B

102-85-2

tri-n-butyl phosphite

2372-45-4

sodium butanolate

A

1809-19-4

dibutyl hydrogen phosphite

B

102-85-2

tri-n-butyl phosphite

Conditions
ConditionsYield
With diethyl ether; phosphorus trichloride
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Chemistry

IUPAC Name:Tributyl phosphite (102-85-2)
Synonyms: 1,1,1-Phosphinidynetri-1-butano ; Butyl phosphite ((C4H9O)3P) ; jp304 ; Phosphorus derivative ; Phosphorustributoxide(p(obu)3) ; Syn-O-Ad P-312 ; Tributoxyphosphine ; Tributylfosfit
Product Categories: Organic Building Blocks;Organic Phosphates/Phosphites;Phosphorus Compounds
CAS: 102-85-2
Molecular Formula :C12H27O3P
Molecular Weight: 250.31
Molecular Structure:
EINECS: 203-061-3
Mol File: 102-85-2.mol
Flash Point: 121.1 °C
Enthalpy of Vaporization: 48.57 kJ/mol
Melting point: -80 °C
Boiling Point: 268.1 °C at 760 mmHg
Vapour Pressure: 0.013 mmHg at 25°C
Density : 0.925 g/mL at 25 °C(lit.)
Refractive index: n20/D 1.431(lit.)
BRN: 1703866
Appearance: Clear colorless liquid 

Uses

Tributyl phosphite (102-85-2) is used as lubricants, preservatives, heat stabilizers of Intensifier.

Toxicity Data With Reference

1.    

skn-rbt 10 mg/24H

    JIHTAB    Journal of Industrial Hygiene and Toxicology. 26 (1944),269.
2.    

eye-rbt 500 mg

    AJOPAA    American Journal of Ophthalmology. 29 (1946),1363.
3.    

orl-rat LD50:3000 mg/kg

    JIHTAB    Journal of Industrial Hygiene and Toxicology. 26 (1944),269.
4.    

skn-rbt LD50:2 g/kg

    AIHAAP    American Industrial Hygiene Association Journal. 34 (1973),286.

Consensus Reports

Reported in EPA TSCA Inventory.

Safety Profile

Hazard Codes  C
Risk Statements  21-34
21:Tributyl phosphite (102-85-2) is harmful in contact with skin.
34: Tributyl phosphite (102-85-2) can causes burns.
Safety Statements  26-36/37/39-45
25:  Avoid contact with eyes
45:  In case of accident or if you feel unwell, seek medical advice immediately (show label where possible)
36/37/39:  Wear suitable protective clothing, gloves and eye/face protection
RIDADR  UN 3265 8/PG 3
WGK Germany  3
RTECS  TH0875000

Specification

1.General Information: As in any fire, wear a self-contained breathing apparatus in pressure-demand, MSHA/NIOSH (approved or equivalent), and full protective gear.
2.Extinguishing Media: Use water spray, dry chemical, carbon dioxide, or chemical foam 
3.Handling: Avoid breathing dust, vapor, mist, or gas. Avoid contact with skin and eyes.
4.Storage: Store Tributyl phosphite (102-85-2)  in a cool, dry place. Store in a tightly closed container.