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105-64-6

Basic Information
CAS No.: 105-64-6
Name: Peroxydicarbonic acid,C,C'-bis(1-methylethyl) ester
Molecular Structure:
Molecular Structure of 105-64-6 (Peroxydicarbonic acid,C,C'-bis(1-methylethyl) ester)
Formula: C8H14 O6
Molecular Weight: 206.196
Synonyms: Peroxydicarbonicacid, bis(1-methylethyl) ester (9CI); Peroxydicarbonic acid, diisopropyl ester(6CI,8CI); Bisisopropyl peroxydicarbonate; Di-iso-propyl peroxydicarbonate;Diisopropyl percarbonate; Diisopropyl perdicarbonate; Diisopropylperoxydicarbonate; Diisopropyl peroxydiformate; IPP; Isopropylperoxydicarbonate; Luperox IPP; Perkadox IPP; Peroyl IPP
EINECS: 203-317-4
Density: 1.138 g/cm3
Melting Point: 12 ºC
Boiling Point: 208 °C at 760 mmHg
Flash Point: 79.1 °C
Solubility: 30.5mg/L at 20℃
Appearance: Colorless, crystalline solid.
Hazard Symbols: Spontaneous decomposition at room temperature releases flammable and corrosive products; dangerous fire hazard; explodes on heating. Store in open containers at low temperature with adequate ventilation.
Risk Codes: R36/37/38
Safety: Moderately toxic by ingestion and skin contact. A severe eye irritant. Very dangerous fire hazard. Dangerously unstable above 10°C. An impact- and heat-sensitive explosive. Solutions may spontaneously explode (the hazard increases with concentration). Storage in sealed containers may be dangerous. Explodes on contact with amines or potassium iodide. May explode on contact with organic matter. When heated to decomposition it emits acrid smoke and fumes. See also PEROXIDES, ORGANIC.
Transport Information: UN 2133/2134
PSA: 71.06000
LogP: 2.02460
Synthetic route
108-23-6

isopropyl chloroformate

105-64-6

diisopropyl peroxydicarbonate

Conditions
ConditionsYield
With sodium hydroxide; dihydrogen peroxide99%
With sodium hydroxide; dihydrogen peroxide In water at 15℃; Product distribution / selectivity;94%
With dihydrogen peroxide; potassium hydroxide In water at 5 - 50℃; for 0.0766667h; Flow reactor;74.7%
With sodium peroxide
With sodium hydroxide; dihydrogen peroxide
2564-83-2, 45842-10-2

2,2,6,6-Tetramethyl-1-piperidinyloxy free radical

105-64-6

diisopropyl peroxydicarbonate

105-06-6

1,4-Divinylbenzene

262616-04-6

2-(isopropyloxycarbonyloxy)-1-(2',2',6',6'-tetramethyl-1'-piperidinyloxy)-1-(4'-vinylphenyl)ethane

Conditions
ConditionsYield
at 55℃; for 5h;76.1%
132969-46-1

4-acetoxy-2,2,6,6-tetramethylpiperidine-1-oxyl

105-64-6

diisopropyl peroxydicarbonate

105-06-6

1,4-Divinylbenzene

2-(isopropyloxycarbonyloxy)-1-(4'-acetoxy-2',2',6',6'-tetramethyl-1'-piperidinyloxy)-1-(4'-vinylphenyl)ethane

Conditions
ConditionsYield
at 0 - 55℃; for 5h;73%
2564-83-2, 45842-10-2

2,2,6,6-Tetramethyl-1-piperidinyloxy free radical

105-64-6

diisopropyl peroxydicarbonate

108-57-6

1,3-divinylbenzene

2-(isopropyloxycarbonyloxy)-1-(2',2',6',6'-tetramethyl-1'-piperidinyloxy)-1-(3'-vinylphenyl)ethane

Conditions
ConditionsYield
70.5%
3225-26-1

4-(benzyloxycarbonyl)-2,2,6,6-tetramethylpiperidine-1-oxyl

105-64-6

diisopropyl peroxydicarbonate

105-06-6

1,4-Divinylbenzene

2-(isopropyloxycarbonyloxy)-1-(4'-benzoyloxy-2',2',6',6'-tetramethyl-1'-piperidinyloxy)-1-(4'-vinylphenyl)ethane

Conditions
ConditionsYield
at 0 - 55℃; for 5h;62.1%
105-64-6

diisopropyl peroxydicarbonate

142505-38-2

N-(4-chlorophenylmethylene)-2-methylthiobenzenamine

A

6265-91-4

2-(4-chlorophenyl)benzothiazole

B

104-88-1

4-chlorobenzaldehyde

C

142505-43-9

(2-aminophenyl)thiomethyl isopropyl carbonate

Conditions
ConditionsYield
In benzene at 60℃; for 5h;A 36%
B 48%
C 54%
105-64-6

diisopropyl peroxydicarbonate

105-06-6

1,4-Divinylbenzene

2406-25-9, 44871-19-4

di-tert-butyl nitroxide

2-(isopropyloxycarbonyloxy)-1-(di-t-butylnitroxy)-1-(4'-vinylphenyl)ethane

Conditions
ConditionsYield
at 0 - 55℃; for 5h;53.2%
105-64-6

diisopropyl peroxydicarbonate

19860-20-9

benzylidene-(2-methylsulfanyl-phenyl)-amine

A

883-93-2

2-Phenylbenzothiazole

B

100-52-7

benzaldehyde

C

142505-43-9

(2-aminophenyl)thiomethyl isopropyl carbonate

Conditions
ConditionsYield
In benzene at 60℃; for 5h;A 17%
B 35%
C 53%
105-64-6

diisopropyl peroxydicarbonate

142505-40-6

N-(3-nitrophenylmethylene)-2-methylthiobenzenamine

A

22868-33-3

2-(3-nitrophenyl)benzothiazole

B

99-61-6

3-nitro-benzaldehyde

C

142505-43-9

(2-aminophenyl)thiomethyl isopropyl carbonate

D

142505-44-0

<(2-(3-nitrophenyl)methylenamino)phenyl>thiomethyl isopropyl carbonate

Conditions
ConditionsYield
With 2,6-di-tert-butylphenol In benzene at 60℃; for 5h;A 3%
B 13%
C 10%
D 50%
105-64-6

diisopropyl peroxydicarbonate

783-08-4

[4-(benzylideneamino)phenyl]methanol

A

128220-34-8

methyl 6-methoxy-2-phenylquinoline-4-carboxylate

B

85221-16-5

carbamic acid, (4-methoxyphenyl)-, 1-methylethyl ester

Conditions
ConditionsYield
With acrylic acid methyl ester In benzene at 60℃; for 4h;A 49%
B 14%
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  • propan-2-yl propan-2-yloxycarbonyloxy carbonate

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    Diisopropyl peroxydicarbonate

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    Molecular Formula: C4H8O4 Formula Weight: 120.10392

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Chemistry

Chemical Name: Diisopropyl peroxydicarbonate
IUPAC NAME: Propan-2-yl propan-2-yloxycarbonyloxy carbonate
CAS No.: 105-64-6
EINECS: 203-317-4
RTECS Class: Primary Irritant
Molecular Formula: C8H14O6
Molecular Weight: 206.19 g/mol
Melting Point: 12°C
Density: 1.138 g/cm3 
Flash Point: 79.1 °C
Boiling Point: 208 °C at 760 mmHg 
Sensitive: Heat sensitive.
Following is the structure of Diisopropyl perdicarbonate (105-64-6):


The chemical synonymous of Diisopropyl perdicarbonate (105-64-6) are Diisopropyl peroxydicarbonate ; Bisisopropyl peroxydicarbonate ; Isopropyl peroxydicarbonate ; Isopropyl peroxycarbonate ; Peroxydicarbonic acid, diisopropyl ester ; Isopropylpercarbonate ; Diisopropylperoxydicarbonat ; Diisopropyl peroxydiformate

Toxicity Data With Reference

1.    

eye-rbt 500 mg SEV

    IHFCAY    Industrial Hygiene Foundation of America, Chemical and Toxicological Series, Bulletin. 6 (1967),1.
2.    

orl-rat LD50:2140 mg/kg

    IHFCAY    Industrial Hygiene Foundation of America, Chemical and Toxicological Series, Bulletin. 6 (1967),1.
3.    

skn-rbt LD50:2025 mg/kg

    BSPII*    SPI Bulletin. (Society of the Plastics Industry, 250 Park Ave., New York, NY 10017) 1/75-19B .

Consensus Reports

Reported in EPA TSCA Inventory.

Safety Profile

Moderately toxic by ingestion and skin contact. A severe eye irritant. Very dangerous fire hazard. Dangerously unstable above 10°C. An impact- and heat-sensitive explosive. Solutions may spontaneously explode (the hazard increases with concentration). Storage in sealed containers may be dangerous. Explodes on contact with amines or potassium iodide. May explode on contact with organic matter. When heated to decomposition it emits acrid smoke and fumes. See also PEROXIDES, ORGANIC.
Attention:
1. Storage: Keep in a cool, dry, dark location in a tightly sealed container or cylinder. Keep away from incompatible materials, ignition sources and untrained individuals. Secure and label area. Protect containers/cylinders from physical damage.
2. Handling: All chemicals should be considered hazardous. Avoid direct physical contact. Use appropriate, approved safety equipment. Untrained individuals should not handle this chemical or its container. Handling should occur in a chemical fume hood.