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13159-52-9

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Basic Information
CAS No.: 13159-52-9
Name: 3-CHLORO-2-HYDROXYPROPYL METHACRYLATE
Article Data: 15
Molecular Structure:
Molecular Structure of 13159-52-9 (3-CHLORO-2-HYDROXYPROPYL METHACRYLATE)
Formula: C7H11 Cl O3
Molecular Weight: 178.616
Synonyms: Methacrylicacid, 3-chloro-2-hydroxypropyl ester (7CI,8CI); 1,2-Propanediol, 3-chloro-,1-methacrylate (8CI); 1-Chloro-3-methacryloxy-2-propanol;2-Hydroxy-3-chloropropyl methacrylate; 3-Chloro-2-hydroxyprop-1-ylmethacrylate; 3-Chloro-2-hydroxypropyl methacrylate; Noimer M; Topolene M; b-Hydroxy-g-chloropropyl methacrylate
Density: 1.177g/cm3
Boiling Point: 287.4°Cat760mmHg
Flash Point: 127.6°C
Hazard Symbols:
Risk Codes: 22-38-41-43
Safety:
Hazard Codes Xn
Risk Statements 22-38-41-43
Safety Statements 26-36
WGK Germany 3
PSA: 46.53000
LogP: 0.70540
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Synthetic route
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2,3-Epoxypropyl methacrylate

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3-chloro-2-hydroxypropyl methacrylate

Conditions
ConditionsYield
With quaternary ammonium chloride; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; water In acetonitrile for 0.5h; Heating;96%
With N-chloro-succinimide; triphenylphosphine In water; acetonitrile at 20℃; for 0.05h;95%
With N-chloro-succinimide; Silphos at 20℃; for 0.0833333h;94%
79-41-4

poly(methacrylic acid)

96-24-2

3-monochloro-1,2-propanediol

13159-52-9

3-chloro-2-hydroxypropyl methacrylate

Conditions
ConditionsYield
With toluene-4-sulfonic acid; hydroquinone
96-24-2

3-monochloro-1,2-propanediol

920-46-7

Methacryloyl chloride

13159-52-9

3-chloro-2-hydroxypropyl methacrylate

Conditions
ConditionsYield
With triethylamine; acetonitrile
79-41-4

poly(methacrylic acid)

106-89-8

epichlorohydrin

A

109573-57-1

2-Methyl-acrylic acid 2-chloro-1-hydroxymethyl-ethyl ester

B

13159-52-9

3-chloro-2-hydroxypropyl methacrylate

Conditions
ConditionsYield
Sn-P In benzene for 20h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
With chromium(lll) acetate for 80h; Kinetics; Solvent;
With diethylene glycol dimethyl ether; chromium(lll) acetate at 10℃; Kinetics; Temperature; Solvent; regioselective reaction;
...Expand
79-41-4

poly(methacrylic acid)

106-89-8

epichlorohydrin

13159-52-9

3-chloro-2-hydroxypropyl methacrylate

Conditions
ConditionsYield
With diethylene glycol dimethyl ether; chromium(lll) acetate at 80℃; Kinetics; Temperature; Solvent; regioselective reaction;
66545-45-7

N-(2,2,6,6-tetramethyl-4-piperidyl)-n-dodecylamine

13159-52-9

3-chloro-2-hydroxypropyl methacrylate

C28H54N2O3

Conditions
ConditionsYield
With potassium carbonate In acetonitrile for 24h; Reflux;98%
With potassium carbonate In acetonitrile for 24h; Reflux;
124-41-4

sodium methylate

13159-52-9

3-chloro-2-hydroxypropyl methacrylate

23056-15-7

3-methoxy-2-hydroxypropyl methacrylate

Conditions
ConditionsYield
With 10H-phenothiazine for 6h; Temperature; Reflux;79%
13159-52-9

3-chloro-2-hydroxypropyl methacrylate

2-bromo-3-chloropropyl methacrylate

Conditions
ConditionsYield
With tetraalkylammonium bromide; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone In acetonitrile for 0.5h; Heating;

sodium diselenide

13159-52-9

3-chloro-2-hydroxypropyl methacrylate

1352427-00-9

C14H22O6Se2

Conditions
ConditionsYield
In ethanol; water at 20℃; for 3h;

C35H52N3P(2+)*2Br(1-)

13159-52-9

3-chloro-2-hydroxypropyl methacrylate

C42H62N3O3P(2+)*2Br(1-)

Conditions
ConditionsYield
With potassium carbonate In acetonitrile for 24h; Reflux;
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