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Basic Information
| CAS No.: | 13159-52-9 | ||||||||
|---|---|---|---|---|---|---|---|---|---|
| Name: | 3-CHLORO-2-HYDROXYPROPYL METHACRYLATE | ||||||||
| Molecular Structure: | |||||||||
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| Formula: | C7H11 Cl O3 | ||||||||
| Molecular Weight: | 178.616 | ||||||||
| Synonyms: | Methacrylicacid, 3-chloro-2-hydroxypropyl ester (7CI,8CI); 1,2-Propanediol, 3-chloro-,1-methacrylate (8CI); 1-Chloro-3-methacryloxy-2-propanol;2-Hydroxy-3-chloropropyl methacrylate; 3-Chloro-2-hydroxyprop-1-ylmethacrylate; 3-Chloro-2-hydroxypropyl methacrylate; Noimer M; Topolene M; b-Hydroxy-g-chloropropyl methacrylate | ||||||||
| Density: | 1.177g/cm3 | ||||||||
| Boiling Point: | 287.4°Cat760mmHg | ||||||||
| Flash Point: | 127.6°C | ||||||||
| Hazard Symbols: |
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| Risk Codes: | 22-38-41-43 | ||||||||
| Safety: |
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| PSA: | 46.53000 | ||||||||
| LogP: | 0.70540 | ||||||||
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Synthetic route
- 106-91-2
2,3-Epoxypropyl methacrylate
- 13159-52-9
3-chloro-2-hydroxypropyl methacrylate
Conditions
| Conditions | Yield |
|---|---|
| With quaternary ammonium chloride; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; water In acetonitrile for 0.5h; Heating; | 96% |
| With N-chloro-succinimide; triphenylphosphine In water; acetonitrile at 20℃; for 0.05h; | 95% |
| With N-chloro-succinimide; Silphos at 20℃; for 0.0833333h; | 94% |
- 79-41-4
poly(methacrylic acid)
- 96-24-2
3-monochloro-1,2-propanediol
- 13159-52-9
3-chloro-2-hydroxypropyl methacrylate
Conditions
| Conditions | Yield |
|---|---|
| With toluene-4-sulfonic acid; hydroquinone |
- 96-24-2
3-monochloro-1,2-propanediol
- 920-46-7
Methacryloyl chloride
- 13159-52-9
3-chloro-2-hydroxypropyl methacrylate
Conditions
| Conditions | Yield |
|---|---|
| With triethylamine; acetonitrile |
- 79-41-4
poly(methacrylic acid)
- 106-89-8
epichlorohydrin
A
- 109573-57-1
2-Methyl-acrylic acid 2-chloro-1-hydroxymethyl-ethyl ester
B
- 13159-52-9
3-chloro-2-hydroxypropyl methacrylate
Conditions
| Conditions | Yield |
|---|---|
| Sn-P In benzene for 20h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts; | |
| With chromium(lll) acetate for 80h; Kinetics; Solvent; | |
| With diethylene glycol dimethyl ether; chromium(lll) acetate at 10℃; Kinetics; Temperature; Solvent; regioselective reaction; |
...Expand
Conditions
| Conditions | Yield |
|---|---|
| With diethylene glycol dimethyl ether; chromium(lll) acetate at 80℃; Kinetics; Temperature; Solvent; regioselective reaction; |
- 66545-45-7
N-(2,2,6,6-tetramethyl-4-piperidyl)-n-dodecylamine
- 13159-52-9
3-chloro-2-hydroxypropyl methacrylate
Conditions
| Conditions | Yield |
|---|---|
| With potassium carbonate In acetonitrile for 24h; Reflux; | 98% |
| With potassium carbonate In acetonitrile for 24h; Reflux; |
- 124-41-4
sodium methylate
- 13159-52-9
3-chloro-2-hydroxypropyl methacrylate
- 23056-15-7
3-methoxy-2-hydroxypropyl methacrylate
Conditions
| Conditions | Yield |
|---|---|
| With 10H-phenothiazine for 6h; Temperature; Reflux; | 79% |
- 13159-52-9
3-chloro-2-hydroxypropyl methacrylate
Conditions
| Conditions | Yield |
|---|---|
| With tetraalkylammonium bromide; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone In acetonitrile for 0.5h; Heating; |
Conditions
| Conditions | Yield |
|---|---|
| In ethanol; water at 20℃; for 3h; |
Conditions
| Conditions | Yield |
|---|---|
| With potassium carbonate In acetonitrile for 24h; Reflux; |
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3-CHLORO-2-HYDROXYPROPYL METHACRYLATE
