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Basic Information
CAS No.: 13220-33-2
Name: 1-Methyl-3-pyrrolidinol
Article Data: 13
Molecular Structure:
Molecular Structure of 13220-33-2 (1-Methyl-3-pyrrolidinol)
Formula: C5H11NO
Molecular Weight: 101.148
Synonyms: 1-Methyl-3-pyrrolidinol;N-Methyl-3-hydroxypyrrolidine;N-Methyl-3-pyrrolidinol;NSC 89279;
EINECS: 236-189-3
Density: 1.045 g/cm3
Boiling Point: 192.2 °C at 760 mmHg
Flash Point: 70.6 °C
Appearance: Colorless or light yellow liquid
Hazard Symbols: IrritantXi
Risk Codes: 36/37/38
Safety: 26-36/37/39
PSA: 23.47000
LogP: -0.37930
Synthetic route
19398-47-1

1,4-dibromo-2-butanol

74-89-5

methylamine

A

13220-33-2

1-methyl-3-pyrrolidinol

B

1404453-61-7

1,4-bis(methylamino)butan-2-ol

Conditions
ConditionsYield
In water at 100℃; for 16h; Inert atmosphere;A 98%
B 0.9 g
2419-74-1

1,4-dichlorobutan-2-ol

74-89-5

methylamine

13220-33-2

1-methyl-3-pyrrolidinol

Conditions
ConditionsYield
In water at 10 - 120℃; under 7500.75 Torr; for 10h; Temperature; Pressure; Autoclave; Sealed tube;64.8%

4-methylamino-3-hydroxybutyronitrile

13220-33-2

1-methyl-3-pyrrolidinol

Conditions
ConditionsYield
56%
CH3 NH2

CH3 NH2

19398-47-1

1,4-dibromo-2-butanol

13220-33-2

1-methyl-3-pyrrolidinol

Conditions
ConditionsYield
25%
14891-10-2

ethyl-3-oxo-1-pyrrolidinecarboxylate

13220-33-2

1-methyl-3-pyrrolidinol

Conditions
ConditionsYield
With lithium aluminium tetrahydride
19398-47-1

1,4-dibromo-2-butanol

74-89-5

methylamine

13220-33-2

1-methyl-3-pyrrolidinol

Conditions
ConditionsYield
With ethanol at 125 - 130℃;
554-15-4

1-methyl-2,5-dihydro-pyrrole

13220-33-2

1-methyl-3-pyrrolidinol

Conditions
ConditionsYield
With sodium hydroxide; dimethylsulfide borane complex; dihydrogen peroxide Product distribution; var. hydroborating agents, olefin to hydroborating agent ratios, and times; other N-substituted-3-pyrrolines;
1.1-dimethyl-3-oxy-pyrrolidinium chloride

1.1-dimethyl-3-oxy-pyrrolidinium chloride

13220-33-2

1-methyl-3-pyrrolidinol

14891-10-2

ethyl-3-oxo-1-pyrrolidinecarboxylate

60-29-7

diethyl ether

lithium alanate

lithium alanate

13220-33-2

1-methyl-3-pyrrolidinol

40499-83-0

pyrrolidin-3-ol

50-00-0

formaldehyd

13220-33-2

1-methyl-3-pyrrolidinol

Conditions
ConditionsYield
With sodium tris(acetoxy)borohydride; acetic acid In tetrahydrofuran
Downstream Products
68165-06-0
13118-11-1
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  • 1-Methyl-3-pyrrolidinol

  • Casno:

    13220-33-2

    1-Methyl-3-pyrrolidinol

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  • 1-Methyl-3-pyrrolidinol

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    13220-33-2

    1-Methyl-3-pyrrolidinol

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Chemistry

IUPAC Name: 1-methylpyrrolidin-3-ol 
Empirical Formula: C5H11NO
Molecular Weight: 101.1469g/mol
EINECS: 236-189-3 
Structure of 3-Pyrrolidinol,1-methyl- (CAS NO.13220-33-2):

Index of Refraction: 1.496
Molar Refractivity: 28.31 cm3
Molar Volume: 96.7 cm3
Polarizability: 11.22×10-24cm3
Surface Tension: 39 dyne/cm
Density: 1.045 g/cm3
Flash Point: 70.6 °C
Enthalpy of Vaporization: 49.85 kJ/mol
Boiling Point: 192.2 °C at 760 mmHg
Vapour Pressure: 0.132 mmHg at 25°C 
Chemical Properties: Clear colorless to pale yellow liquid
Product Categories: Heterocyclic Compounds;Heterocycles;Building Blocks;Heterocyclic Building Blocks;Pyrrolidines 
Canonical SMILES: CN1CCC(C1)O
InChI: InChI=1S/C5H11NO/c1-6-3-2-5(7)4-6/h5,7H,2-4H2,1H3
InChIKey: FLVFPAIGVBQGET-UHFFFAOYSA-N

Safety Profile

Hazard Codes: IrritantXi
Risk Statements: 36/37/38
R36/37/38:Irritating to eyes, respiratory system and skin.
Safety Statements: 26-36/37/39
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. 
S36/37/39:Wear suitable protective clothing, gloves and eye/face protection.
WGK Germany: 3

Specification

  3-Pyrrolidinol,1-methyl- , its cas register number is 13220-33-2. It also can be called 1-Methyl-3-pyrrolidinol ; EINECS 236-189-3 ; NSC 89279 . 3-Pyrrolidinol,1-methyl- (CAS NO.13220-33-2) is irritating to eyes, respiratory system and skin. In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.