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13734-28-6

Basic Information
CAS No.: 13734-28-6
Name: N-alpha-(tert-Butoxycarbonyl)-L-lysine
Article Data: 31
Molecular Structure:
Molecular Structure of 13734-28-6 (N-alpha-(tert-Butoxycarbonyl)-L-lysine)
Formula: C11H22N2O4
Molecular Weight: 246.307
Synonyms: N2-((1,1-Dimethylethoxy)carbonyl)-L-lysine;Boc-Lys-OH;(2S)-6-azaniumyl-2-(tert-butoxycarbonylamino)hexanoate;Boc-L-Lys-OH;N-tert-Butoxycarbonyl lysine;N-α-Boc-L-lysine;N-a-(tert.-butoxycarbonyl)-L-lysine;
EINECS: 237-303-4
Density: 1.113 g/cm3
Melting Point: ~205 °C
Boiling Point: 410.5 °C at 760 mmHg
Flash Point: 202 °C
Solubility: Soluble in water. Slightly soluble in methanol.
Appearance: white to off-white powder
Hazard Symbols: HarmfulXn
Risk Codes: 20/21/22-36/37/38
Safety: 24/25-36-26
PSA: 101.65000
LogP: 2.18450
Synthetic route
2389-45-9

Boc-Lys(Z)-OH

13734-28-6

Boc-Lys-OH

Conditions
ConditionsYield
With ammonium formate; palladium on activated charcoal In methanol for 0.0833333h; Ambient temperature;95%
With magnesium; hydrazinium monoformate In methanol at 25℃; for 0.5h;95%
With palladium on carbon; hydrogen In ethanol at 20℃; under 2172.08 Torr; for 0.5h; Inert atmosphere;78%
54613-99-9

Boc-(S)-Lys(2-Cl-Z)-OH

13734-28-6

Boc-Lys-OH

Conditions
ConditionsYield
With ammonium formate; palladium on activated charcoal In methanol at 20℃; for 0.166667h; Hydrogenolysis;95%
With magnesium; hydrazinium monoformate In methanol at 25℃; for 1.5h;94%
With hydrogen; palladium on activated charcoal In acetic acid at 20℃;
56-87-1

L-lysine

24424-99-5

di-tert-butyl dicarbonate

13734-28-6

Boc-Lys-OH

Conditions
ConditionsYield
With triethylamine In water; acetone at 25℃; for 4.5h;90%
With sodium hydrogencarbonate In water at 25℃; for 13h;89.5%
With sodium hydroxide In isopropyl alcohol Ambient temperature;76.5%
13734-29-7

Nα-tert-butoxycarbonyl-Nε-tosyl-L-lysine

13734-28-6

Boc-Lys-OH

Conditions
ConditionsYield
With 3-(4,8-dimethoxy-1-naphthyl)-propionic acid; ascorbic acid In ethanol for 2h; Irradiation;79%
77236-13-6

N-α-tert-Butyloxycarbonyl-N-ε-carbobenzoxy-L-lysine benzyl ester

A

2389-45-9

Boc-Lys(Z)-OH

B

13734-28-6

Boc-Lys-OH

Conditions
ConditionsYield
With bis(tri-n-butyltin)oxide In toluene at 70℃; for 36h;A 60%
B 10%
1070-19-5

N-(tert-butyloxycarbonyl) azide

1155-64-2

N6-[(benzyloxy)carbonyl]-L-lysine

13734-28-6

Boc-Lys-OH

Conditions
ConditionsYield
(i) aq. NaOH, dioxane, (ii) H2, Pd-C, aq. MeOH; Multistep reaction;
84624-27-1

Boc-Lys(Fmoc)-OH

13734-28-6

Boc-Lys-OH

Conditions
ConditionsYield
With piperidine; N,N-dimethyl-formamide for 0.05h;
104669-73-0

Nα-(tert-butoxycarbonyl)-Nε-(allyloxycarbonyl)-L-lysine

13734-28-6

Boc-Lys-OH

Conditions
ConditionsYield
With tri-n-butyl-tin hydride; bis-triphenylphosphine-palladium(II) chloride In dichloromethane Ambient temperature;95 % Spectr.
78981-72-3

α-<(tert-butyloxycarbonyl)lysyl>amido>benzyloxycarbonyl>-p'-nitroanilide

A

124-38-9

carbon dioxide

B

623-04-1

4-aminobenzenemethanol

C

13734-28-6

Boc-Lys-OH

D

100-01-6

4-nitro-aniline

Conditions
ConditionsYield
In water at 25℃; Product distribution; trypsin;
Boc-Lys(Z)-OResin

Boc-Lys(Z)-OResin

13734-28-6

Boc-Lys-OH

Conditions
ConditionsYield
With cyclohexa-1,4-diene; palladium diacetate In N,N-dimethyl-formamide at 30 - 40℃; for 3h; Yield given;
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  • Boc-L-Lys-OH

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Specification

The Boc-Lys-OH, with the CAS registry number 13734-28-6, is also known as N2-((1,1-Dimethylethoxy)carbonyl)-L-lysine. It belongs to the product categories of Amino Acids; Lysine [Lys, K]; Boc-Amino Acids and Derivative; Amino Acids (N-Protected); Biochemistry; Boc-Amino Acids; Boc-Amino Acid Series. Its EINECS registry number is 237-303-4. This chemical's molecular formula is C11H22N2O4 and molecular weight is 246.30338. Its IUPAC name is called 6-amino-2-[(2-methylpropan-2-yl)oxycarbonylamino]hexanoic acid. This chemical is white to off-white powder.

Physical properties of Boc-Lys-OH: (1)ACD/LogP: 0.74; (2)ACD/LogD (pH 5.5): -1.76; (3)ACD/LogD (pH 7.4): -1.76; (4)ACD/BCF (pH 5.5): 1; (5)ACD/BCF (pH 7.4): 1; (6)ACD/KOC (pH 5.5): 1; (7)ACD/KOC (pH 7.4): 1; (8)#H bond acceptors: 6; (9)#H bond donors: 4; (10)#Freely Rotating Bonds: 9; (11)Index of Refraction: 1.485; (12)Molar Refractivity: 63.4 cm3; (13)Molar Volume: 221.1 cm3; (14)Surface Tension: 42.8 dyne/cm; (15)Density: 1.113 g/cm3; (16)Flash Point: 202 °C; (17)Enthalpy of Vaporization: 72.72 kJ/mol; (18)Boiling Point: 410.5 °C at 760 mmHg; (19)Vapour Pressure: 6.91E-08 mmHg at 25°C.

When you are using this chemical, please be cautious about it as the following:
This chemical may cause damage to health. It is harmful by inhalation, in contact with skin and if swallowed. It is irritating to eyes, respiratory system and skin. In case of contact with eyes, you should rinse immediately with plenty of water and seek medical advice. Whenever you will contact it, please wear suitable protective clothing. Finally, you must avoid contacting it with skin and eyes.

You can still convert the following datas into molecular structure:
(1)Canonical SMILES: CC(C)(C)OC(=O)NC(CCCCN)C(=O)O
(2)InChI: InChI=1S/C11H22N2O4/c1-11(2,3)17-10(16)13-8(9(14)15)6-4-5-7-12/h8H,4-7,12H2,1-3H3,(H,13,16)(H,14,15)
(3)InChIKey: DQUHYEDEGRNAFO-UHFFFAOYSA-N