Name: DIIODOSILANE
SKU: 13760-02-6

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Basic Information

Molecular Structure:
CAS No.:	13760-02-6
Name:	DIIODOSILANE
Article Data:	10

Formula:	H₂I₂Si
Molecular Weight:	283.91
Synonyms:	Diiodosilane;
Density:	2.834 g/mL at 25 °C(lit.)
Melting Point:	-1°C
Boiling Point:	153.7 °C at 760 mmHg
Flash Point:	101 °F
Appearance:	Clear liquid
Hazard Symbols:	C
Risk Codes:	10-14-20/21/22-34
Safety:	16-26-27-28-36/37/39-45
PSA:	0.00000
LogP:	0.85520

Synthetic route

: 4109-96-0
Dichlorosilane

: lithium iodide

: 13760-02-6
diiodosilane

Conditions

Conditions	Yield
In pentane at -70 - 35℃; for 16h; Temperature; Solvent; Inert atmosphere; Large scale;	77%
at 40℃; under 1277.21 - 2311.54 Torr; for 0.08h; Temperature;	45.3 g

: 12185-10-3
phosphorous

: 13598-42-0
iodosilane

A: 13760-02-6
diiodosilane

B: 128166-50-7
P(SiH3)I2

C: 7440-21-3
monosilane

Conditions

Conditions	Yield
In neat (no solvent) byproducts: H2; heating in evacuated, sealed tube to 100°C;;

...Expand

: 12185-10-3
phosphorus

: 13598-42-0
iodosilane

A: 13760-02-6
diiodosilane

B: 128166-50-7
P(SiH3)I2

C: 7440-21-3
monosilane

Conditions

Conditions	Yield
byproducts: H2; at 100°C;

...Expand

: 12185-10-3
phosphorus

: 13598-42-0
iodosilane

A: 13760-02-6
diiodosilane

B: Si2H4

C: P(SiH3)4I

D: 7803-51-2
phosphan

Conditions

Conditions	Yield
byproducts: H2; at 20°C;	A <1 B n/a C n/a D n/a

...Expand

: 10034-85-2
hydrogen iodide

: 7440-21-3
monosilane

A: 13760-02-6
diiodosilane

B: 13465-72-0
triiodo silane

C: 13465-84-4
silicon tetraiodide

D: 13598-42-0
iodosilane

Conditions

Conditions	Yield
aluminium(III) iodide In neat (no solvent) reaction at 80°C and 500 Torr;; fractional distillation and condensation;;
aluminium(III) iodide In neat (no solvent) reaction at 80°C and 500 Torr;; fractional distillation and condensation;;

...Expand

: 775-12-2
diphenylsilane

: 10034-85-2
hydrogen iodide

: 13760-02-6
diiodosilane

Conditions

Conditions	Yield
In not given according to Fritz, G., Kummer D., Chem. Ber., 94 (1961) p. 1143; at -40°C;

: 4109-96-0
Dichlorosilane

: lithium iodide

A: 13760-02-6
diiodosilane

B: 21479-74-3
SiH2ClI

Conditions

Conditions	Yield
In toluene at 20 - 29℃; for 18h; Temperature; Solvent;

...Expand

: 13760-02-6
diiodosilane

: 870-61-1
bis(trifluoromethylseleno)mercury

: 69641-88-9
bis(trifluoromethylseleno)silane

Conditions

Conditions	Yield
In decalin stirring, 20°C, 1 h;	78%

: 13760-02-6
diiodosilane

: 2S-benzyloxymethyl-4R-acetoxy-1,3 dioxolane

: 154459-77-5
2S-benzyloxymethyl-4S acetoxy-1,3 dioxolane

A: 2S-Benzyloxymethyl-4R-iodo-1,3-dioxolane

B: 299412-06-9
2S-benzyloxymethyl-4S-iodo-1,3 dioxolane

Conditions

Conditions	Yield
In dichloromethane; toluene

...Expand

: 13760-02-6
diiodosilane

: mercury

: mercury(I) iodide

Conditions

Conditions	Yield
In neat (no solvent) byproducts: SiH4, Si2H6, H2; at ambient temp.;;
In neat (no solvent) byproducts: SiH4, Si2H6, H2; at ambient temp.;;

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Specification

The Silane, diiodo-(7CI,8CI,9CI) is an organic compound with the formula H₂I₂Si. The systematic name of this chemical is diiodosilane. With the CAS registry number 13760-02-6, it is also named as silane, diiodo-. The product's categories are Protecting and Derivatizing Reagents; Protection and Derivatization; Silicon-Based.

Physical properties about Silane, diiodo-(7CI,8CI,9CI) are: (1)Boiling Point: 153.7 °C at 760 mmHg ; (2)Vapour Pressure: 4.21 mmHg at 25°C.

When you are using this chemical, please be cautious about it as the following:
It is flammable and harmful by inhalation, in contact with skin and if swallowed. After contact with skin, wash immediately with plenty of ... (to be specified by the manufacturer). Please keep away from sources of ignition - No smoking and take off immediately all contaminated clothing. In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. Besides, this chemical reacts violently with water and can cause burns. When you are using it, wear suitable gloves and eye/face protection. In case of accident or if you feel unwell seek medical advice immediately (show the label where possible).

You can still convert the following datas into molecular structure:
(1)SMILES: I[SiH2]I
(2)InChI: InChI=1/H2I2Si/c1-3-2/h3H2
(3)InChIKey: AIHCVGFMFDEUMO-UHFFFAOYAW
(4)Std. InChI: InChI=1S/H2I2Si/c1-3-2/h3H2
(5)Std. InChIKey: AIHCVGFMFDEUMO-UHFFFAOYSA-N