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Basic Information
CAS No.: 1440-00-2
Name: 1,3-Benzenediol, 4,4'-[6-(4-methoxyphenyl)-1,3,5-triazine-2,4-diyl]bis-
Article Data: 11
Molecular Structure:
Molecular Structure of 1440-00-2 (1,3-Benzenediol, 4,4'-[6-(4-methoxyphenyl)-1,3,5-triazine-2,4-diyl]bis-)
Formula: C22H17N3O5
Molecular Weight: 403.394
Density: 1.427g/cm3
Melting Point: >360 °C
Boiling Point: 755.6oC at 760 mmHg
Flash Point: 410.8oC
PSA: 128.30000
LogP: 1.43860
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4-[4-(2,4-dihydroxyphenyl)-6-(4-methoxyphenyl)-1,3,5-triazin-2-yl]benzene-1,3-diol

Conditions
ConditionsYield
With aluminum (III) chloride; 1-methyl-3-propyl-1H-imidazolium chloride at 75℃; for 8h; Reagent/catalyst; Temperature;96.1%
With aluminum (III) chloride; silica gel In sulfolane at 60 - 80℃; for 10h; Solvent; Temperature; Reagent/catalyst;86%
Stage #1: 2,4-dichloro-6-(4-methoxy-phenyl)-[1,3,5]triazine With aluminum (III) chloride In chlorobenzene at 25℃; for 0.5h; Inert atmosphere;
Stage #2: recorcinol at 85℃; for 5h;		84%
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2,4-dichloro-6-(4-methoxy-phenyl)-[1,3,5]triazine

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recorcinol

A

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1440-00-2

4-[4-(2,4-dihydroxyphenyl)-6-(4-methoxyphenyl)-1,3,5-triazin-2-yl]benzene-1,3-diol

Conditions
ConditionsYield
aluminium chloride In sulfolane; methanol; 5,5-dimethyl-1,3-cyclohexadiene
...Expand
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4-methoxyphenyl magnesium bromide

1440-00-2

4-[4-(2,4-dihydroxyphenyl)-6-(4-methoxyphenyl)-1,3,5-triazin-2-yl]benzene-1,3-diol

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: tetrahydrofuran / 10 h / 0 - 45 °C / Inert atmosphere
2.1: aluminum (III) chloride / chlorobenzene / 0.5 h / 25 °C / Inert atmosphere
2.2: 5 h / 85 °C
View Scheme
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1,3,5-trichloro-2,4,6-triazine

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4-[4-(2,4-dihydroxyphenyl)-6-(4-methoxyphenyl)-1,3,5-triazin-2-yl]benzene-1,3-diol

Conditions
ConditionsYield
Stage #1: 1,3,5-trichloro-2,4,6-triazine; methoxybenzene With aluminum (III) chloride In sulfolane at 50 - 60℃; for 2h;
Stage #2: recorcinol In sulfolane at 40 - 50℃; for 4h; Solvent;		142 g
Stage #1: 1,3,5-trichloro-2,4,6-triazine; methoxybenzene With aluminum (III) chloride In sulfolane at 50 - 60℃; for 2h;
Stage #2: recorcinol In sulfolane at 40 - 50℃; for 4h;		320 g
Stage #1: 1,3,5-trichloro-2,4,6-triazine; recorcinol With aluminum (III) chloride In sulfolane at 50 - 60℃; for 2h;
Stage #2: methoxybenzene In sulfolane at 40 - 50℃; for 4h;		318 g
...Expand
100-66-3

methoxybenzene

1440-00-2

4-[4-(2,4-dihydroxyphenyl)-6-(4-methoxyphenyl)-1,3,5-triazin-2-yl]benzene-1,3-diol

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: aluminum (III) chloride / sulfolane / 40 - 60 °C
2: aluminum (III) chloride / sulfolane / 5 h / 40 - 50 °C
View Scheme
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glycidyl isopropyl ether

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ethyltriphenylphosphonium bromide

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4-[4-(2,4-dihydroxyphenyl)-6-(4-methoxyphenyl)-1,3,5-triazin-2-yl]benzene-1,3-diol

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2,4-bis{[4-(3-(2-propyloxy)-2-hydroxypropyloxy)-2-hydroxyphenyl]}-6-(4-methoxyphenyl)-1,3,5-triazine

Conditions
ConditionsYield
In N-methyl-acetamide; 5,5-dimethyl-1,3-cyclohexadiene; acetone; toluene
...Expand
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4-[4-(2,4-dihydroxyphenyl)-6-(4-methoxyphenyl)-1,3,5-triazin-2-yl]benzene-1,3-diol

2,4-bis-[{(4-(3-sulfonato)-2-hydroxypropyloxy)-2-hydroxy}phenyl]-6-(4-methoxyphenyl)-1,3,5-triazine sodium salt

Conditions
ConditionsYield
With sodium hydroxide In 2-methoxy-ethanol; acetone
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4-[4-(2,4-dihydroxyphenyl)-6-(4-methoxyphenyl)-1,3,5-triazin-2-yl]benzene-1,3-diol

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Conditions
ConditionsYield
With sodium carbonate In N,N-dimethyl-formamide at 100 - 143℃; for 7h; pH=7; Reagent/catalyst; Temperature;
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2-ethylhexyl bromide

1440-00-2

4-[4-(2,4-dihydroxyphenyl)-6-(4-methoxyphenyl)-1,3,5-triazin-2-yl]benzene-1,3-diol

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Conditions
ConditionsYield
With sodium carbonate In N,N-dimethyl-formamide at 125℃;
With sodium carbonate In N,N-dimethyl-formamide at 125℃;160 g
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4-[4-(2,4-dihydroxyphenyl)-6-(4-methoxyphenyl)-1,3,5-triazin-2-yl]benzene-1,3-diol

2,4-bis((4-(ethyl-hexyloxy)-2-hydroxy)-phenyl)-6-(4-methoxyphenyl)-1,3,5-triazine

Conditions
ConditionsYield
With sodium hydroxide In N,N-dimethyl-formamide at 70℃;
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