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1569-01-3

Basic Information
CAS No.: 1569-01-3
Name: 1-PROPOXY-2-PROPANOL
Article Data: 22
Molecular Structure:
Molecular Structure of 1569-01-3 (1-PROPOXY-2-PROPANOL)
Formula: C6H14 O2
Molecular Weight: 118.176
Synonyms: 1,2-Propyleneglycol 1-propyl ether; 1-Propoxy-2-propanol; Arcosolv PNP
EINECS: 250-069-8
Density: 0.885 g/mL at 25 °C(lit.)
Melting Point: -80 C
Boiling Point: 140 - 160 C
Flash Point: 48 C
Solubility: miscible
Appearance: clear liquid
Hazard Symbols: UN NO.
Risk Codes: R10; R36/37/38
Transport Information: HAZARD
PSA: 29.46000
LogP: 0.79380
Synthetic route
71-23-8

propan-1-ol

75-56-9, 16033-71-9

methyloxirane

1569-01-3

1-(1-propyloxy)propan-2-ol

Conditions
ConditionsYield
With Al2O3/MgO composite at 120℃; Inert atmosphere;34.4%
With KAcMIMOH at 60℃; for 4h;
With hematite at 160℃; for 8h; Autoclave;
71-23-8

propan-1-ol

75-56-9, 16033-71-9

methyloxirane

A

10215-30-2

2-propoxy-1-propanol

B

1569-01-3

1-(1-propyloxy)propan-2-ol

Conditions
ConditionsYield
at 100 - 200℃;
at 180 - 205℃;
With sulfuric acid Yield given. Yields of byproduct given;
6819-41-6

sodium n-propoxide

75-56-9, 16033-71-9

methyloxirane

1569-01-3

1-(1-propyloxy)propan-2-ol

106-92-3

Allyl glycidyl ether

A

3126-95-2

3-Propoxy-1,2-epoxypropan

B

1569-01-3

1-(1-propyloxy)propan-2-ol

Conditions
ConditionsYield
With hydrogen; 5percent Pd/C(en) In tetrahydrofuran at 20℃; for 2.5h; Catalytic hydrogenation; Title compound not separated from byproducts.;
57-55-6

propylene glycol

A

71-23-8

propan-1-ol

B

111-43-3

Dipropyl ether

C

10215-30-2

2-propoxy-1-propanol

D

1569-01-3

1-(1-propyloxy)propan-2-ol

Conditions
ConditionsYield
With trifluorormethanesulfonic acid; hydrogen; [{CpRu(CO)2}2(μ-H)](+)*OTf(-); cyclopenta-1,3-diene In sulfolane at 110℃; under 39003.1 Torr; for 30h; Product distribution;A 54 % Chromat.
B 15 % Chromat.
C n/a
D n/a
57-55-6

propylene glycol

A

71-23-8

propan-1-ol

B

4359-46-0

2-ethyl-4-methyl-1,3-dioxolane

C

111-43-3

Dipropyl ether

D

10215-30-2

2-propoxy-1-propanol

E

1569-01-3

1-(1-propyloxy)propan-2-ol

F

123-38-6

propionaldehyde

Conditions
ConditionsYield
With bis(dicarbonyl)(μ-hydrido)(pentamethylcyclopentadiene)ruthenium trifluoromethanesulfonate; trifluorormethanesulfonic acid; hydrogen In sulfolane at 110℃; under 38787.1 Torr; for 30h; Mechanism; Kinetics; Solvent; Pressure; Concentration; Temperature; Time; regioselective reaction;A 54 %Chromat.
B n/a
C n/a
D n/a
E n/a
F n/a
57-55-6

propylene glycol

A

71-23-8

propan-1-ol

B

106-36-5

propyl propionate

C

74-98-6

propane

D

10215-30-2

2-propoxy-1-propanol

E

1569-01-3

1-(1-propyloxy)propan-2-ol

F

802294-64-0

propionic acid

G

108-67-8

1,3,5-trimethyl-benzene

Conditions
ConditionsYield
With [C6H3-2,6-(OP(tBu)2)2]IrH2; trifluorormethanesulfonic acid; hydrogen In 1,4-dioxane at 125℃; under 5171.62 Torr; Autoclave;

1-propoxy-2-propanyl formate

A

64-18-6

formic acid

B

1569-01-3

1-(1-propyloxy)propan-2-ol

Conditions
ConditionsYield
With water at 80℃; for 24h; Equilibrium constant; Sealed tube;
1569-01-3

1-(1-propyloxy)propan-2-ol

1056233-21-6

N’-(5-bromo-6-hydroxy-2-methyl-3-pyridyl)-N-ethyl-N-methyl-formamidine

N’-[5-bromo-2-methyl-6-[1-methyl-2-propoxy-ethoxy]-3-pyridyl]-N-ethyl-N-methyl-formamidine

Conditions
ConditionsYield
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 20 - 40℃; for 1.66667h; Inert atmosphere;95%
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 20℃; for 1.5h; Inert atmosphere;95%
67-56-1

methanol

1569-01-3

1-(1-propyloxy)propan-2-ol

1-propoxy-2-propanyl formate

Conditions
ConditionsYield
With [bis({2‐[bis(propan‐2‐yl)phosphanyl]ethyl})amine](borohydride)(carbonyl)(hydride)iron(II); methacrylic acid methyl ester In toluene at 140℃; under 13689.1 Torr; for 4h; Autoclave; Inert atmosphere;71%
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    Product Name: 1-PROPOXY-2-PROPANOL MF: C6H14O2 MW: 118.17 EINECS: 216-372-4 Mol File: 1569-01-3.mol 1-PROPOXY-2-PROPANOL Structure 1-PROPOXY-2-PROPANOL Chemical Properties Melting point -80°C Boiling point 140-160 °C(

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Chemistry

Synonyms: PNP;2-Propanol, 1-propoxy-;PROPYLENE GLYCOL PROPYL ETHER;PROPYLENE GLYCOL MONOPROPYL ETHER;PROPYLENE GLYCOL NORMAL PROPYL ETHER;ethermonopropyliquenormaldupropyleneglycol ;1-propoxy-2-propano;1-propoxy-propan-2-ol;
The Molecular formula of 1-PROPOXY-2-PROPANOL(1569-01-3): C6H14O2
The Molecular Weight of 1-PROPOXY-2-PROPANOL(1569-01-3): 118.17
Molecular Structure : 
EINECS: 216-372-4
Boiling point: 140-160 °C(lit.)
Flash point: 119 °F
density: 0.885 g/mL at 25 °C(lit.)
refractive index: n20/D 1.411(lit.)

Toxicity Data With Reference

1.   

skn-rbt 500 mg

   VHTODE    Veterinary and Human Toxicology. 30 (1988),126.
2.   

eye-rbt 100 mg MOD

   VHTODE    Veterinary and Human Toxicology. 30 (1988),126.
3.   

orl-rat LD50:2504 mg/kg

   VHTODE    Veterinary and Human Toxicology. 30 (1988),126.
4.   

skn-rbt LD50:3550 mg/kg

   38MKAJ    Pattys Industrial Hygiene and Toxicology. 2C (1982),3983.

Consensus Reports

Reported in EPA TSCA Inventory.

Safety Profile

Moderately toxic by ingestion and skin contact. A skin and eye irritant. When heated to decomposition it emits acrid smoke and irritating fumes.
The Hazard Codes of 1-PROPOXY-2-PROPANOL(1569-01-3):   Xi
The Risk Statements information of 1-PROPOXY-2-PROPANOL(1569-01-3):
10:  Flammable 
36/37/38:  Irritating to eyes, respiratory system and skin 
The Safety Statements information of 1-PROPOXY-2-PROPANOL(1569-01-3):
16:  Keep away from sources of ignition - No smoking 
26:  In case of contact with eyes, rinse immediately with plenty of water and seek medical advice  
36:  Wear suitable protective clothing 
RIDADR: UN 3271 3/PG 3