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161596-47-0

Basic Information
CAS No.: 161596-47-0
Name: 1H-Isoindole-1,3(2H)-dione,2-[(2S)-2-oxiranylmethyl]-
Molecular Structure:
Molecular Structure of 161596-47-0 (1H-Isoindole-1,3(2H)-dione,2-[(2S)-2-oxiranylmethyl]-)
Formula: C11H9NO3
Molecular Weight: 203.19
Synonyms: 1H-Isoindole-1,3(2H)-dione,2-(oxiranylmethyl)-, (S)-;1H-Isoindole-1,3(2H)-dione, 2-[(2S)-oxiranylmethyl]-(9CI);(S)-2-(Oxiran-2-ylmethyl)-1H-isoindole-1,3(2H)-dione;(S)-N-(2,3-Epoxypropan-1-yl)phthalimide;N-((2S)-Oxiran-2-ylmethyl)phthalimide;N-(S)-Glycidylphthalimide;
EINECS: 1308068-626-2
Density: 1.446 g/cm3
Melting Point: 102 °C
Boiling Point: 347.4 °C at 760 mmHg
Flash Point: 163.9 °C
Solubility:
Appearance:
Hazard Symbols: IrritantXi
Risk Codes: 41
Safety: 26-39
Transport Information:
PSA: 49.91000
LogP: 0.61930
Synthetic route
148857-42-5

2-((S)-3-chloro-2-hydroxypropyl)isoindoline-1,3-dione

161596-47-0

(S)-N-glycidylphthalimide

Conditions
ConditionsYield
With sodium carbonate In 5,5-dimethyl-1,3-cyclohexadiene for 4h; Reflux; Green chemistry;94%
With sodium carbonate In 5,5-dimethyl-1,3-cyclohexadiene for 4h; Reflux;89%
With potassium phosphate In 1,2-dichloro-ethane at 80℃; for 14h; Product distribution / selectivity;n/a
40137-25-5

1H-isoindole-1,3(2H)-dione, 2-[[(4S)-2,2-dimethyl-1,3-dioxolan-4-yl]methyl]

161596-47-0

(S)-N-glycidylphthalimide

Conditions
ConditionsYield
Stage #1: 1H-isoindole-1,3(2H)-dione, 2-[[(4S)-2,2-dimethyl-1,3-dioxolan-4-yl]methyl] With hydrogen bromide In 1,2-dichloro-ethane at 10 - 15℃; for 4h;
Stage #2: With sodium methylate In methanol at 0 - 15℃; for 3h;
93.6%
Multi-step reaction with 4 steps
1: hydrogenchloride / water / 2 h / 60 - 67 °C / Industrial scale
2: pyridinium p-toluenesulfonate / toluene / 0.25 h / 30 - 50 °C / Industrial scale
3: chloro-trimethyl-silane / toluene / 2.5 h / 30 °C
4: sodium methylate / methanol / 20 h / 30 °C
View Scheme
Multi-step reaction with 4 steps
1: hydrogenchloride / water / 2 h / 60 - 67 °C / Industrial scale
2: pyridinium p-toluenesulfonate / toluene / 3 h / Dean-Stark; Reflux; Industrial scale
3: N-Bromosuccinimide / 1,2-dichloro-ethane / 1.33 h / 12 - 22 °C / Industrial scale
4: sodium methylate / toluene; methanol / 5.17 h / 9 - 22 °C / Industrial scale
View Scheme
136918-14-4

phthalimide

60456-23-7

(S)-oxiranemethanol

161596-47-0

(S)-N-glycidylphthalimide

Conditions
ConditionsYield
With triphenylphosphine; diethylazodicarboxylate In tetrahydrofuran at 0 - 20℃;91%
With triphenylphosphine; diethylazodicarboxylate In tetrahydrofuran at 0 - 20℃;91%
With triphenylphosphine; diethylazodicarboxylate In tetrahydrofuran at 20 - 25℃; for 18h;80%
136918-14-4

phthalimide

51594-55-9

(R)-(-)-epichlorohydrin

161596-47-0

(S)-N-glycidylphthalimide

Conditions
ConditionsYield
With benzyltrimethylammonium chloride In isopropyl alcohol at 40℃; for 22h;90%
With potassium tert-butylate; benzyltrimethylammonium chloride; sodium carbonate In tetrahydrofuran at 50℃; for 39h;81%
With benzyltrimethylammonium chloride; sodium hydrogencarbonate In isopropyl alcohol at 20℃; for 25h;80%

C15H17NO4

161596-47-0

(S)-N-glycidylphthalimide

Conditions
ConditionsYield
Stage #1: C15H17NO4 With hydrogenchloride In dichloromethane; water at 10 - 15℃; for 4h;
Stage #2: With sodium methylate In methanol at 0 - 15℃; for 3h; Reagent/catalyst;
89.7%

C17H21NO4

161596-47-0

(S)-N-glycidylphthalimide

Conditions
ConditionsYield
Stage #1: C17H21NO4 With hydrogen iodide In chloroform at 10 - 15℃; for 4h;
Stage #2: With sodium ethanolate In ethanol at 0 - 15℃; for 3h;
85.9%
51594-55-9

(R)-(-)-epichlorohydrin

1074-82-4

potassium phtalimide

161596-47-0

(S)-N-glycidylphthalimide

Conditions
ConditionsYield
With benzyltrimethylammonium chloride In isopropyl alcohol at 10℃; for 46h;83%
With benzyltrimethylammonium chloride In tetrahydrofuran at 50℃; for 44h;74%
With benzyltrimethylammonium chloride In methanol at 20℃; for 15h;68%
136918-14-4

phthalimide

51594-55-9

(R)-(-)-epichlorohydrin

A

161596-47-0

(S)-N-glycidylphthalimide

B

148857-42-5

2-((S)-3-chloro-2-hydroxypropyl)isoindoline-1,3-dione

Conditions
ConditionsYield
With potassium fluoride on basic alumina In 2-methyltetrahydrofuran for 3h; Inert atmosphere; Reflux; stereospecific reaction;A 10%
B 83%
67843-74-7

(S)-epichlorohydrin

1074-82-4

potassium phtalimide

161596-47-0

(S)-N-glycidylphthalimide

Conditions
ConditionsYield
at 70℃; for 1h; Temperature;83%
With N-benzyl-N,N,N-triethylammonium chloride; potassium iodide In isopropyl alcohol at 28℃; for 72h; Reagent/catalyst; Temperature; Solvent;88.1 g

1H-isoindole-1,3(2H)-dione, 2-[2-(benzoyloxy)-3-bromopropyl]

161596-47-0

(S)-N-glycidylphthalimide

Conditions
ConditionsYield
With sodium methylate In methanol; toluene at 9 - 22℃; for 5.16667h; Industrial scale;80.8%
136918-14-4

phthalimide

67843-74-7

(S)-epichlorohydrin

161596-47-0

(S)-N-glycidylphthalimide

Conditions
ConditionsYield
Stage #1: phthalimide; (S)-epichlorohydrin With methylamine In isopropyl alcohol at 60℃; for 5h;
Stage #2: With sodium methylate In methanol; isopropyl alcohol at 10 - 30℃; Solvent; Reagent/catalyst;
77.5%
Stage #1: phthalimide; (S)-epichlorohydrin With N-benzyl-N,N,N-triethylammonium chloride; sodium carbonate In isopropyl alcohol at 20 - 40℃;
Stage #2: With potassium tert-butylate In isopropyl alcohol at 5 - 10℃;
With sodium acetate In isopropyl alcohol at 65 - 70℃;5 g
With 1-hexylamine hydrochloride; potassium tert-butylate; potassium iodide In isopropyl alcohol at 28℃; for 72h;84.5 g
136918-14-4

phthalimide

57044-25-4

(R)-oxiranemethanol

161596-47-0

(S)-N-glycidylphthalimide

Conditions
ConditionsYield
With triphenylphosphine; diethylazodicarboxylate In tetrahydrofuran at 20℃; for 4h;53%
51594-55-9

(R)-(-)-epichlorohydrin

1074-82-4

potassium phtalimide

A

181140-34-1

(-)-2-[(2R)-oxiran-2-ylmethyl]-1H-isoindole-1,3(2H)-dione

B

161596-47-0

(S)-N-glycidylphthalimide

Conditions
ConditionsYield
With benzyltrimethylammonium chloride In DMF (N,N-dimethyl-formamide) at 20℃; for 16h;
19667-37-9, 34839-11-7, 148857-42-5, 148857-44-7

2-(3-chloro-2-hydroxypropyl)-1H-isoindole-1,3(2H)-dione

161596-47-0

(S)-N-glycidylphthalimide

Conditions
ConditionsYield
With potassium carbonate In toluene Reflux;n/a
In tetrahydrofuran; water
879507-96-7

(S)-2-(2-acetoxy-3-bromo-propyl)-isoindole-1,3-dione

161596-47-0

(S)-N-glycidylphthalimide

Conditions
ConditionsYield
With potassium carbonate In methanol at 0℃; for 1h;
136918-14-4

phthalimide

113826-06-5

(R)-glycidyl tosylate

161596-47-0

(S)-N-glycidylphthalimide

Conditions
ConditionsYield
With tetrabutylammomium bromide; potassium carbonate In acetone at 35 - 60℃; for 12h;
With tetrabutylammomium bromide; potassium carbonate In acetone at 25 - 60℃; for 12h;
136918-14-4

phthalimide

161596-47-0

(S)-N-glycidylphthalimide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: aluminum oxide / 1-methyl-pyrrolidin-2-one / 64 - 68 °C
1.2: 0.5 h
2.1: potassium carbonate / toluene / Reflux
View Scheme
Multi-step reaction with 2 steps
1.1: aluminum oxide / 1-methyl-pyrrolidin-2-one / 64 - 68 °C
1.2: 0.5 h
2.1: potassium carbonate / toluene / Reflux
View Scheme
Multi-step reaction with 2 steps
1.1: aluminum oxide / 1-methyl-pyrrolidin-2-one / 64 - 68 °C
1.2: 0.5 h
2.1: potassium carbonate / toluene / Reflux
View Scheme
136918-14-4

phthalimide

67843-74-7

(S)-epichlorohydrin

A

19667-37-9, 34839-11-7, 148857-42-5, 148857-44-7

2-(3-chloro-2-hydroxypropyl)-1H-isoindole-1,3(2H)-dione

B

161596-47-0

(S)-N-glycidylphthalimide

Conditions
ConditionsYield
With aluminum oxide In 1-methyl-pyrrolidin-2-one at 64 - 68℃;
1074-82-4

potassium phtalimide

161596-47-0

(S)-N-glycidylphthalimide

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: N-benzyl-N,N,N-triethylammonium chloride / N,N-dimethyl-formamide / 6 h / 100 - 120 °C / Industrial scale
2: pyridinium p-toluenesulfonate / toluene / 3 h / Dean-Stark; Reflux; Industrial scale
3: N-Bromosuccinimide / 1,2-dichloro-ethane / 1.33 h / 12 - 22 °C / Industrial scale
4: sodium methylate / toluene; methanol / 5.17 h / 9 - 22 °C / Industrial scale
View Scheme
Multi-step reaction with 4 steps
1: N-benzyl-N,N,N-triethylammonium chloride / N,N-dimethyl-formamide / 6 h / 100 - 120 °C / Industrial scale
2: pyridinium p-toluenesulfonate / toluene / 0.25 h / 30 - 50 °C / Industrial scale
3: chloro-trimethyl-silane / toluene / 2.5 h / 30 °C
4: sodium methylate / methanol / 20 h / 30 °C
View Scheme
Multi-step reaction with 2 steps
1.1: potassium iodide / N,N-dimethyl-formamide / 4 h / 80 - 85 °C
2.1: hydrogen bromide / 1,2-dichloro-ethane / 4 h / 10 - 15 °C
2.2: 3 h / 0 - 15 °C
View Scheme
879507-95-6

(S)-2-(2-methoxy-2-methyl-[1,3]dioxolane-4-ylmethyl)-isoindole-1,3-dione

161596-47-0

(S)-N-glycidylphthalimide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: chloro-trimethyl-silane / toluene / 2.5 h / 30 °C
2: sodium methylate / methanol / 20 h / 30 °C
View Scheme

(S)-2-phthalimido-1-(chloromethyl)ethyl acetate

161596-47-0

(S)-N-glycidylphthalimide

Conditions
ConditionsYield
With sodium methylate In methanol at 30℃; for 20h;65.6 kg

1H-isoindole-1,3(2H)-dione, 2-[[(4S)-2-phenyl-1,3-dioxolan-4-yl]methyl]

161596-47-0

(S)-N-glycidylphthalimide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: N-Bromosuccinimide / 1,2-dichloro-ethane / 1.33 h / 12 - 22 °C / Industrial scale
2: sodium methylate / toluene; methanol / 5.17 h / 9 - 22 °C / Industrial scale
View Scheme
119835-88-0

1H-isoindole-1,3(2H)-dione, 2-[(2S)-2,3-dihydroxypropyl]

161596-47-0

(S)-N-glycidylphthalimide

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: pyridinium p-toluenesulfonate / toluene / 3 h / Dean-Stark; Reflux; Industrial scale
2: N-Bromosuccinimide / 1,2-dichloro-ethane / 1.33 h / 12 - 22 °C / Industrial scale
3: sodium methylate / toluene; methanol / 5.17 h / 9 - 22 °C / Industrial scale
View Scheme
Multi-step reaction with 3 steps
1: pyridinium p-toluenesulfonate / toluene / 0.25 h / 30 - 50 °C / Industrial scale
2: chloro-trimethyl-silane / toluene / 2.5 h / 30 °C
3: sodium methylate / methanol / 20 h / 30 °C
View Scheme
5455-98-1

2-oxiranylmethylisoindole-1,3-dione

A

181140-34-1

(-)-2-[(2R)-oxiran-2-ylmethyl]-1H-isoindole-1,3(2H)-dione

B

161596-47-0

(S)-N-glycidylphthalimide

Conditions
ConditionsYield
With Cu metal organic framework based on (R)-3,3′-bis(6-carboxy-2-naphthyl)-2,2′-dihydroxy-1,1′-binaphthyl*silica packed stainless steel column (10 cm long × 4.0 mm i.d.) In ethanol; hexane at 25℃; Resolution of racemate;

2-((S)-3-bromo-2-hydroxypropyl)isoindoline-1,3-dione

161596-47-0

(S)-N-glycidylphthalimide

Conditions
ConditionsYield
With sodium methylate In methanol; toluene at 5℃; for 0.75h;34.1 g

2-((S)-3-p-toluenesulfonyloxy-2-hydroxypropyl)isoindoline-1,3-dione

161596-47-0

(S)-N-glycidylphthalimide

Conditions
ConditionsYield
With sodium methylate In methanol; toluene at -5 - 20℃; for 1.25h;35.8 g
71026-66-9

N-(tert-butoxycarbonyl)-1,4-phenylenediamine

161596-47-0

(S)-N-glycidylphthalimide

1082937-55-0

C22H25N3O5

Conditions
ConditionsYield
In isopropyl alcohol for 16h; Reflux;100%
In isopropyl alcohol for 16h; Reflux;100%
In isopropyl alcohol for 16h; Heating / reflux;100%
54879-88-8

N-benzyl-2,2-dimethoxyethylamine

161596-47-0

(S)-N-glycidylphthalimide

1374982-07-6

(R)-2-{3-[benzyl-(2,2-dimethoxyethyl)amino]-2-hydroxypropyl}-1H-isoindole-1,3(2H)-dione

Conditions
ConditionsYield
In ethanol for 20h; Inert atmosphere; Reflux;100%
161596-47-0

(S)-N-glycidylphthalimide

2-((R)-3-Azido-2-hydroxy-propyl)-isoindole-1,3-dione

Conditions
ConditionsYield
With sodium azide; ammonium chloride In N,N-dimethyl-formamide at 80℃; for 1h;100%
With sodium azide; ammonium chloride In N,N-dimethyl-formamide at 80℃;100%
224323-51-7

3-fluoro-4-(morpholin-4-yl)-phenyl isocyanate

161596-47-0

(S)-N-glycidylphthalimide

168828-89-5

2-({(5S)-2-oxo-3-[(4-morpholino-3-fluorophenyl)]-4,5-dihydro-1,3-oxazole-5-yl}methyl)-isoindole-1,3-dione

Conditions
ConditionsYield
With lithium bromide at 120℃; for 4h; Temperature; Solvent;96.51%
With lithium bromide In N,N-dimethyl-formamide at 60℃; for 4h; Reagent/catalyst; Solvent;90.11%
1325210-64-7

4-(4-isocyanatophenyl)morpholin-3-one

161596-47-0

(S)-N-glycidylphthalimide

446292-08-6

2-({(5S)-2-oxo-3-[4-(3-oxo-4-morpholinyl)phenyl]-1,3-oxazolidin-5-yl}methyl)-1H-isoindole-1,3(2H)-dione

Conditions
ConditionsYield
With 3-methyl-1-butyl acetate; magnesium chloride at 120℃; for 4h; Solvent; Reagent/catalyst; Temperature;95.5%
With lithium iodide In chlorobenzene at 115℃; for 4h; Reagent/catalyst; Solvent; Temperature;94.09%
161596-47-0

(S)-N-glycidylphthalimide

438056-69-0

4-(4-aminophenyl)morpholin-3-one

446292-07-5

2-((2R)-2-hydroxy-3-{[4-(3-oxo-4-morpholinyl)phenyl]amino}propyl)-1H-isoindole-1,3(2H)-dione

Conditions
ConditionsYield
In ethanol; water at 20℃; for 15h; Solvent; Temperature;95%
In ethanol; water for 27h; Heating;92%
In methanol; water at 65 - 70℃; for 32h;92%
161596-47-0

(S)-N-glycidylphthalimide

438056-69-0

4-(4-aminophenyl)morpholin-3-one

2-((2R)-2-hydroxy-3-{[4-(3-oxomorpholin-4-yl)phenyl]amino}propyl)-1H-isoindole-1,3(2H)-dione

Conditions
ConditionsYield
In water; toluene at 30 - 85℃; Solvent; Temperature;94.6%
93246-53-8

3-fluoro-4-(morpholinyl)aniline

161596-47-0

(S)-N-glycidylphthalimide

874340-08-6

N-[3-phthalimido-2-(R)-hydroxypropyl]-3-fluoro-4-(4-morpholinyl)aniline

Conditions
ConditionsYield
In ethanol; water at 80℃; for 14h;94.4%
In N,N-dimethyl-formamide for 5h; Product distribution / selectivity; Heating / reflux;
In N,N-dimethyl-formamide
122-80-5

N-acetyl-p-phenylenediamine

161596-47-0

(S)-N-glycidylphthalimide

C19H19N3O4

Conditions
ConditionsYield
In isopropyl alcohol for 16h; Reflux;93.8%
161596-47-0

(S)-N-glycidylphthalimide

148857-42-5

2-((S)-3-chloro-2-hydroxypropyl)isoindoline-1,3-dione

Conditions
ConditionsYield
Stage #1: (S)-N-glycidylphthalimide With Chloroiodomethane In 2-methyltetrahydrofuran at -78℃; for 0.0333333h;
Stage #2: With methyllithium In 2-methyltetrahydrofuran; diethyl ether at -78℃; for 1h; Solvent; Reagent/catalyst; Temperature; enantioselective reaction;
93%
With C25H21OP; trichloroacetonitrile In water; N,N-dimethyl-formamide at 25℃; for 6h; Inert atmosphere; Irradiation;78%
100-01-6

4-nitro-aniline

161596-47-0

(S)-N-glycidylphthalimide

C17H15N3O5

Conditions
ConditionsYield
In ethanol at 50℃; Solvent; Temperature;91%
161596-47-0

(S)-N-glycidylphthalimide

C11H10INO3

Conditions
ConditionsYield
Stage #1: (S)-N-glycidylphthalimide With diiodomethane In 2-methyltetrahydrofuran at -78℃; for 0.0333333h;
Stage #2: With methyllithium In 2-methyltetrahydrofuran; diethyl ether at -78℃; for 1h; enantioselective reaction;
91%
93246-53-8

3-fluoro-4-(morpholinyl)aniline

161596-47-0

(S)-N-glycidylphthalimide

C21H22FN3O4

Conditions
ConditionsYield
In ethanol at 60℃; for 16h; Temperature; Inert atmosphere;90.09%
161596-47-0

(S)-N-glycidylphthalimide

2-((S)-3-bromo-2-hydroxypropyl)isoindoline-1,3-dione

Conditions
ConditionsYield
Stage #1: (S)-N-glycidylphthalimide With iodobromomethane In 2-methyltetrahydrofuran at -78℃; for 0.0333333h;
Stage #2: With methyllithium In 2-methyltetrahydrofuran; diethyl ether at -78℃; for 1h; enantioselective reaction;
89%

C10H8(2)H4N2O2

161596-47-0

(S)-N-glycidylphthalimide

C21H17(2)H4N3O5

Conditions
ConditionsYield
In ethanol; water at 0℃; for 32h; Reflux;88%
75-86-5

2-hydroxy-2-methylpropanenitrile

161596-47-0

(S)-N-glycidylphthalimide

929281-94-7

(S)-4-(1,3-dioxoisoindol-2-yl)-3-hydroxybutyronitrile

Conditions
ConditionsYield
With triethylamine In tetrahydrofuran at 75℃;87%
103-71-9

phenyl isocyanate

161596-47-0

(S)-N-glycidylphthalimide

(S)-2-((2-oxo-3-phenyloxazolidin-5-yl)methyl)isoindoline-1,3-dione

Conditions
ConditionsYield
With (2-hydroxy-5-methylphenyl)triphenylphosphonium iodide In chlorobenzene at 100℃; for 6h; Inert atmosphere;87%
212325-40-1

methyl (3-fluoro-4-morpholinophenyl)carbamate

161596-47-0

(S)-N-glycidylphthalimide

168828-89-5

2-({(5S)-2-oxo-3-[(4-morpholino-3-fluorophenyl)]-4,5-dihydro-1,3-oxazole-5-yl}methyl)-isoindole-1,3-dione

Conditions
ConditionsYield
With lithium tert-butoxide In N,N-dimethyl-formamide at 25 - 85℃; Temperature; Solvent; Reagent/catalyst;85%
With lithium tert-butoxide In ethyl acetate at 25 - 75℃; Solvent; Temperature; Reagent/catalyst;70%
161596-47-0

(S)-N-glycidylphthalimide

540-37-4

p-aminoiodobenzene

(R)-2-(2-hydroxy-3-((4-iodophenyl)amino)propyl)isoindolin-1,3-one

Conditions
ConditionsYield
In ethanol; water at 100℃; for 12h;84.9%

C24H26N2O3

161596-47-0

(S)-N-glycidylphthalimide

C35H35N3O6

Conditions
ConditionsYield
In methanol; ethanol at 75℃; for 48h; Temperature; Solvent;84.7%
161596-47-0

(S)-N-glycidylphthalimide

873-74-5

4-Aminobenzonitrile

1261131-68-3

4-(3-(1,3-dioxoisoindolin-2-yl)-2-hydroxypropylamino)benzonitrile

Conditions
ConditionsYield
at 105℃; for 13h;84%
With magnesium(II) perchlorate In 1,4-dioxane for 10h; Reflux;78%
161596-47-0

(S)-N-glycidylphthalimide

103-49-1

dibenzylamine

1357474-57-7

2-[(2R)-3-(dibenzylamino)-2-hydroxy-propyl]isoindoline-1,3-dione

Conditions
ConditionsYield
In isopropyl alcohol at 0℃; for 9h; Reflux; Inert atmosphere; regioselective reaction;84%
168828-81-7, 1027135-00-7

benzyl 3-fluoro-4-(4-morpholinyl)phenylcarbamate

161596-47-0

(S)-N-glycidylphthalimide

168828-89-5

2-({(5S)-2-oxo-3-[(4-morpholino-3-fluorophenyl)]-4,5-dihydro-1,3-oxazole-5-yl}methyl)-isoindole-1,3-dione

Conditions
ConditionsYield
Stage #1: benzyl 3-fluoro-4-(4-morpholinyl)phenylcarbamate With lithium tert-butoxide In tetrahydrofuran; N,N-dimethyl-formamide at 5℃; for 0.5h; Inert atmosphere;
Stage #2: (S)-N-glycidylphthalimide In tetrahydrofuran; N,N-dimethyl-formamide at 5 - 20℃; for 24h; Reagent/catalyst; Temperature; Inert atmosphere;
84%

7-fluoro-1-(piperazin-1-yl)isoquinoline

161596-47-0

(S)-N-glycidylphthalimide

2-[(2R)-3-[4-(7-fluoroisoquinolin-1-yl)piperazin-1-yl]-2-hydroxypropyl]-2,3-dihydro-1H-isoindole-1,3-dione

Conditions
ConditionsYield
In acetonitrile at 70℃; for 6h;84%
Downstream Products
168828-89-5
446292-07-5
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    161596-47-0

    Rivaroxaban Intermediate 3

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    Business Type:Lab/Research institutions

    Tel:+86-0512-62959601 skype:aimmezhang

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    161596-47-0

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  • (S)-(+)-GLYCIDYL PHTHALIMIDE

  • Casno:

    161596-47-0

    (S)-(+)-GLYCIDYL PHTHALIMIDE

    Min.Order: 1 Gram

    FOB Price:  USD $ 0.0-0.0/Gram

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    Hangzhou ZeErRui Chemical Co., Ltd. located in Lingang industrial areas, our plant covers an area of 6000 square meters.ZeErRui dedicated to the development, production and marketi

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  • (S)-(+)-glycidyl phthalimide

  • Casno:

    161596-47-0

    (S)-(+)-glycidyl phthalimide

    Min.Order: 100 Gram

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    Appearance:white or light yellow crystalline powder Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for research and industrial manufacture. Transportation:By

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Specification

The (S)-2-Oxiranylmethyl-isoindole-1,3-dione is an organic compound with the formula C11H9NO3. The systematic name of this chemical is 2-(oxiran-2-ylmethyl)-1H-isoindole-1,3(2H)-dione . With the CAS registry number 161596-47-0, it is also named as 1H-Isoindole-1,3(2H)-dione, 2-(oxiranylmethyl)-. The product's categories are N-Substituted Maleimides, Succinimides & Phthalimides; N-Substituted Phthalimides; Oxiranes; Simple 3-Membered Ring Compounds.

Physical properties about (S)-2-Oxiranylmethyl-isoindole-1,3-dione are: (1)ACD/LogP: 1.60; (2)ACD/LogD (pH 5.5): 1.6; (3)ACD/LogD (pH 7.4): 1.6; (4)ACD/BCF (pH 5.5): 9.76; (5)ACD/BCF (pH 7.4): 9.76; (6)ACD/KOC (pH 5.5): 177.71; (7)ACD/KOC (pH 7.4): 177.71; (8)#H bond acceptors: 4; (9)#Freely Rotating Bonds: 2; (10)Polar Surface Area: 49.91 Å2; (11)Index of Refraction: 1.648; (12)Molar Refractivity: 51.16 cm3; (13)Molar Volume: 140.4 cm3; (14)Polarizability: 20.28×10-24cm3; (15)Surface Tension: 64.5 dyne/cm; (16)Density: 1.446 g/cm3; (17)Flash Point: 163.9 °C; (18)Enthalpy of Vaporization: 59.17 kJ/mol; (19)Boiling Point: 347.4 °C at 760 mmHg; (20)Vapour Pressure: 5.38E-05 mmHg at 25°C.

When you are using this chemical, please be cautious about it as the following:
This chemical is risk of serious damage to eyes. When you are using it, wear eye/face protection. In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.

You can still convert the following datas into molecular structure:
(1)SMILES: O=C1c3c(C(=O)N1CC2OC2)cccc3
(2)InChI: InChI=1/C11H9NO3/c13-10-8-3-1-2-4-9(8)11(14)12(10)5-7-6-15-7/h1-4,7H,5-6H2
(3)InChIKey: DUILGEYLVHGSEE-UHFFFAOYAO
(4)Std. InChI: InChI=1S/C11H9NO3/c13-10-8-3-1-2-4-9(8)11(14)12(10)5-7-6-15-7/h1-4,7H,5-6H2
(5)Std. InChIKey: DUILGEYLVHGSEE-UHFFFAOYSA-N

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