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172015-79-1

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Basic Information
CAS No.: 172015-79-1
Name: (1S–4R)-4-(2-amino-6-chloro-9H-purin-9-yl)-2-cyclopentene-1-methanol hydrochloride
Article Data: 5
Molecular Structure:
Molecular Structure of 172015-79-1 ((1S–4R)-4-(2-amino-6-chloro-9H-purin-9-yl)-2-cyclopentene-1-methanol hydrochloride)
Formula: C11H13Cl2N5O
Molecular Weight: 302.163
Synonyms: (1S-cis)-4-(2-Amino-6-chloro-9H-purin-9-yl)-2-cyclopentene-1-methanol Monohydrochloride;ZLD0252;V2106;(1S,4R)-4-(2-Amino-6-chloro-9H-purin-9-yl)-2-cyclopentene-1-methanol hydrochloride;((1S,4R)-4-(2-Amino-6-chloro-9H-purin-9-yl)cyclopent-2-en-1-yl)methanol hydrochloride;
Melting Point: 165-170?C
Boiling Point: 572oC at 760 mmHg
Flash Point: 299.7oC
PSA: 89.85000
LogP: 2.55460
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(1R,4S)-1-[(2-amino-6-chloro-5-formamido-4-pyrimidinyl)amino]-4-(hydroxymethyl)-2-cyclopentene

172015-79-1

((1S,4R)-4-(2-amino-6-chloro-9H-purin-9-yl)cyclopent-2-en-1-yl)methanol hydrochloride

Conditions
ConditionsYield
With hydrogenchloride; orthoformic acid triethyl ester In water for 4h; Cyclization;92%
With hydrogenchloride; orthoformic acid triethyl ester In water at 0 - 10℃; for 1h; Concentration; Temperature;76%
With hydrogenchloride; orthoformic acid triethyl ester In ethanol at 0 - 10℃; for 10h;72.2%
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orthoformic acid triethyl ester

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(1R,4S)-1-[(2-amino-6-chloro-5-formamido-4-pyrimidinyl)amino]-4-(hydroxymethyl)-2-cyclopentene

172015-79-1

((1S,4R)-4-(2-amino-6-chloro-9H-purin-9-yl)cyclopent-2-en-1-yl)methanol hydrochloride

Conditions
ConditionsYield
With hydrogenchloride In tetrahydrofuran; industrial methylated spirit; water at 0 - 25℃; Product distribution / selectivity;82%
With hydrogenchloride In industrial methylated spirit; water at 0 - 25℃; Product distribution / selectivity;81%
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(-)-2-azabicyclo[2.2.1]hept-5-en-3-one

172015-79-1

((1S,4R)-4-(2-amino-6-chloro-9H-purin-9-yl)cyclopent-2-en-1-yl)methanol hydrochloride

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: 1.264 g / tetrahydrofuran; H2O / 18 h / 20 - 60 °C
2: 90.5 percent / LiAlH4 / tetrahydrofuran / 19.5 h / 0 °C / Heating
3: 83 percent / Et3N / ethanol / 7 h / Heating
4: 92 percent / triethylorthoformate; HCl / H2O / 4 h
View Scheme
136522-35-5

(1R,4S)-1-amino-4-hydroxymethyl-2-cyclopentene

172015-79-1

((1S,4R)-4-(2-amino-6-chloro-9H-purin-9-yl)cyclopent-2-en-1-yl)methanol hydrochloride

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 83 percent / Et3N / ethanol / 7 h / Heating
2: 92 percent / triethylorthoformate; HCl / H2O / 4 h
View Scheme
171887-03-9

N-(2-amino-4,6-dichloropyrimidin-5-yl)formamide

172015-79-1

((1S,4R)-4-(2-amino-6-chloro-9H-purin-9-yl)cyclopent-2-en-1-yl)methanol hydrochloride

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 83 percent / Et3N / ethanol / 7 h / Heating
2: 92 percent / triethylorthoformate; HCl / H2O / 4 h
View Scheme
Multi-step reaction with 2 steps
1.1: sodium hydrogencarbonate / ethanol / 0.5 h / 20 °C / Inert atmosphere
1.2: 3 h / 75 - 80 °C / Inert atmosphere
2.1: orthoformic acid triethyl ester; hydrogenchloride / ethanol / 10 h / 0 - 10 °C
View Scheme
171887-02-8

2-amino-5-{[(dimethylamino)methylene]amino}-4,6-dichloropyrimidine

172015-79-1

((1S,4R)-4-(2-amino-6-chloro-9H-purin-9-yl)cyclopent-2-en-1-yl)methanol hydrochloride

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 72 percent / aq. phosphate buffer / 4 h / pH 3.2 / Heating
2: 83 percent / Et3N / ethanol / 7 h / Heating
3: 92 percent / triethylorthoformate; HCl / H2O / 4 h
View Scheme

(-)-(1S, 4R)-4-amino-2-cyclopentene-1-carboxylic acid methanesulfonate

172015-79-1

((1S,4R)-4-(2-amino-6-chloro-9H-purin-9-yl)cyclopent-2-en-1-yl)methanol hydrochloride

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 90.5 percent / LiAlH4 / tetrahydrofuran / 19.5 h / 0 °C / Heating
2: 83 percent / Et3N / ethanol / 7 h / Heating
3: 92 percent / triethylorthoformate; HCl / H2O / 4 h
View Scheme

(1S,4R)-4-amino-2-cyclopentene-1-methanol tartrate salt

116477-30-6

4,6-dichloro-2,5-diformamido-pyrimidine

172015-79-1

((1S,4R)-4-(2-amino-6-chloro-9H-purin-9-yl)cyclopent-2-en-1-yl)methanol hydrochloride

Conditions
ConditionsYield
Stage #1: (1S,4R)-4-amino-2-cyclopentene-1-methanol tartrate salt With sodium carbonate In ethanol for 0.5h;
Stage #2: 4,6-dichloro-2,5-diformamido-pyrimidine In ethanol for 3h; Heating / reflux;
Stage #3: With hydrogenchloride; orthoformic acid triethyl ester more than 3 stages;
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Cyclopropylamine

172015-79-1

((1S,4R)-4-(2-amino-6-chloro-9H-purin-9-yl)cyclopent-2-en-1-yl)methanol hydrochloride

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abacavir

Conditions
ConditionsYield
In methanol at 70℃; for 12h; Substitution;90%
Stage #1: (1S,cis)-4-(2-amino-6-chloro-9-H-purin-9-yl)-2-cyclopentene-1-methanol hydrochloride With triethylamine In water
Stage #2: Cyclopropylamine In water at 70 - 75℃; Concentration; Solvent; Temperature;		90%
In isopropyl alcohol at 90 - 95℃; for 12h; sealed reactor;
In ethanol at 25 - 78℃; for 6h;
With sodium carbonate In ethanol at 70 - 80℃;25 g
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pyrographite

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Cyclopropylamine

172015-79-1

((1S,4R)-4-(2-amino-6-chloro-9H-purin-9-yl)cyclopent-2-en-1-yl)methanol hydrochloride

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Conditions
ConditionsYield
With sodium hydroxide In acetone90%
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    China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:86-152-37804566

    Address:Evergrande Future City, intersection of Zhengkai Avenue and Sixteenth Street, Kaifeng Area, Henan Pilot Free Trade Zone

       Inquiry Now

  • (1S–4R)-4-(2-amino-6-chloro-9H-purin-9-yl)-2-cyclopentene-1-methanol hydrochloride

  • Casno:

    172015-79-1

    (1S–4R)-4-(2-amino-6-chloro-9H-purin-9-yl)-2-cyclopentene-1-methanol hydrochloride

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    1. Timely and efficient service to ensure communication with customers2. Produce products of different specifications and sizes according to your requirements.3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures sta

    Hebei Quanhe Biotechnology Co. LTD. is an enterprise specializing in the research and development, production and trade of pharmaceutical intermediates, apis and chemical raw mater

  •  Hebei Quanhe Biotechnology Co. LTD

    China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-0319-5919066

    Address:Haida Business Center, Xiangdu District

       Inquiry Now

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