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| CAS No.: | 17825-58-0 |
|---|---|
| Name: | 2,3-Diphenylcycloprop-2-ene-1-carboxylic acid |
| Molecular Structure: | |
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|
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| Formula: | C16H12 O2 |
| Molecular Weight: | 236.27 |
| Synonyms: | 1,2-Diphenylcyclopropene-3-carboxylicacid; 2,3-Diphenyl-2-cyclopropene-1-carboxylic acid; 2,3-Diphenyl-2-cyclopropenecarboxylicacid; NSC 406044 |
| Density: | 1.29g/cm3 |
| Melting Point: | 209.5-211.5 °C |
| Boiling Point: | 394.1°Cat760mmHg |
| Flash Point: | 181.9°C |
| PSA: | 37.30000 |
| LogP: | 3.31180 |
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- 7382-06-1
ethyl 2,3-diphenylcycloprop-2-enecarboxylate
- 17825-58-0
2,3-diphenylcycloprop-2-enecarboxylic acid
| Conditions | Yield |
|---|---|
| With potassium hydroxide In tetrahydrofuran; methanol; water at 20℃; for 48h; Hydrolysis; | 95% |
| Stage #1: ethyl 2,3-diphenylcycloprop-2-enecarboxylate With water; potassium hydroxide In methanol at 20℃; for 48h; Stage #2: With hydrogenchloride In water pH=1; | 93% |
- 623-73-4
diazoacetic acid ethyl ester
- 501-65-5
diphenyl acetylene
- 17825-58-0
2,3-diphenylcycloprop-2-enecarboxylic acid
| Conditions | Yield |
|---|---|
| (i) Cu, (heating), (ii) KOH; Multistep reaction; |
- 501-65-5
diphenyl acetylene
- 17825-58-0
2,3-diphenylcycloprop-2-enecarboxylic acid
| Conditions | Yield |
|---|---|
| Multi-step reaction with 2 steps 1: 56 percent / Cu-bronze 2: 95 percent / KOH / tetrahydrofuran; methanol; H2O / 48 h / 20 °C View Scheme |
- 501-65-5
diphenyl acetylene
- 17825-58-0
2,3-diphenylcycloprop-2-enecarboxylic acid
| Conditions | Yield |
|---|---|
| Multi-step reaction with 2 steps 1: rhodium acetate dimer / CH2Cl2 / 35 °C 2: KOH / methanol / 4 h / Heating View Scheme |
- 501-65-5
diphenyl acetylene
- 17825-58-0
2,3-diphenylcycloprop-2-enecarboxylic acid
| Conditions | Yield |
|---|---|
| Multi-step reaction with 2 steps 1: Cu / 0.25 h / 105 °C 2: KOH / methanol; H2O / 1 h / Heating View Scheme |
- 17825-58-0
2,3-diphenylcycloprop-2-enecarboxylic acid
- 100-39-0
benzyl bromide
- 99838-01-4
2,3-Diphenyl-cycloprop-2-enecarboxylic acid benzyl ester
| Conditions | Yield |
|---|---|
| With N(Et)4(1+)*(2-pyrrolidone-anion) In N,N-dimethyl-formamide for 1h; Ambient temperature; | 99% |
- 17825-58-0
2,3-diphenylcycloprop-2-enecarboxylic acid
- 6415-58-3
2,3-diphenyl-2-cyclopropene-1-carbonyl chloride
| Conditions | Yield |
|---|---|
| With oxalyl dichloride In chloroform for 48h; Ambient temperature; further reagent: SOCl2; | 92% |
| With thionyl chloride | 90% |
| With thionyl chloride |
- 524-38-9
N-hydroxyphthalimide
- 17825-58-0
2,3-diphenylcycloprop-2-enecarboxylic acid
- 234075-38-8
N-(2,3-diphenyl-2-cyclopropenylcarbonyloxy)phthalimide
| Conditions | Yield |
|---|---|
| With dmap; dicyclohexyl-carbodiimide Substitution; | 87% |
- 17825-58-0
2,3-diphenylcycloprop-2-enecarboxylic acid
| Conditions | Yield |
|---|---|
| Stage #1: 2,3-diphenylcycloprop-2-enecarboxylic acid Stage #2: With ammonia | 86% |
- 186581-53-3, 908094-01-9
diazomethane
- 17825-58-0
2,3-diphenylcycloprop-2-enecarboxylic acid
| Conditions | Yield |
|---|---|
| In diethyl ether at -10℃; for 480h; | A 14% B 73% |
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