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2-Cyclopropene-1-carboxylicacid, 2,3-diphenyl-
Cas No: 17825-58-0
USD $ 3.0-3.0 / Kilogram 1 Kilogram 1-100 Metric Ton/Month Dayang Chem (Hangzhou) Co.,Ltd. Contact Supplier
Best quality with fast delivery17825-58-0
Cas No: 17825-58-0
USD $ 367.0-724.0 / Kilogram 1 Kilogram 10000 Metric Ton/Month Baoji Guokang Healthchem co.,ltd Contact Supplier
2-Cyclopropene-1-carboxylicacid, 2,3-diphenyl-
Cas No: 17825-58-0
No Data No Data 5 Hangzhou J&H Chemical Co., Ltd. Contact Supplier
17825-58-0 2-Cyclopropene-1-carboxylicacid, 2,3-diphenyl-
Cas No: 17825-58-0
USD $ 5000.0-5000.0 / Metric Ton 1 Metric Ton 1 Metric Ton/Day Henan Tianfu Chemical Co., Ltd. Contact Supplier
2-Cyclopropene-1-carboxylicacid, 2,3-diphenyl- cas 17825-58-0
Cas No: 17825-58-0
No Data No Data No Data Hangzhou Fandachem Co.,Ltd Contact Supplier
2,3-Diphenylcycloprop-2-ene-1-carboxylic acid
Cas No: 17825-58-0
No Data No Data No Data Angene International Limited Contact Supplier

17825-58-0 Usage

InChI:InChI=1/C16H12O2/c17-16(18)15-13(11-7-3-1-4-8-11)14(15)12-9-5-2-6-10-12/h1-10,15H,(H,17,18)

17825-58-0SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 12, 2017

Revision Date: Aug 12, 2017

1.Identification

1.1 GHS Product identifier

Product name 2,3-diphenylcycloprop-2-ene-1-carboxylic acid

1.2 Other means of identification

Product number -
Other names 2,3-Diphenyl-2-cyclopropene-1-carboxylic acid

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:17825-58-0 SDS

17825-58-0Synthetic route

ethyl 2,3-diphenylcycloprop-2-enecarboxylate
7382-06-1

ethyl 2,3-diphenylcycloprop-2-enecarboxylate

2,3-diphenylcycloprop-2-enecarboxylic acid
17825-58-0

2,3-diphenylcycloprop-2-enecarboxylic acid

Conditions
ConditionsYield
With potassium hydroxide In tetrahydrofuran; methanol; water at 20℃; for 48h; Hydrolysis;95%
Stage #1: ethyl 2,3-diphenylcycloprop-2-enecarboxylate With water; potassium hydroxide In methanol at 20℃; for 48h;
Stage #2: With hydrogenchloride In water pH=1;
93%
diazoacetic acid ethyl ester
623-73-4

diazoacetic acid ethyl ester

diphenyl acetylene
501-65-5

diphenyl acetylene

2,3-diphenylcycloprop-2-enecarboxylic acid
17825-58-0

2,3-diphenylcycloprop-2-enecarboxylic acid

Conditions
ConditionsYield
(i) Cu, (heating), (ii) KOH; Multistep reaction;
diphenyl acetylene
501-65-5

diphenyl acetylene

bis(1,3,2-dioxaborol-2-yl)dicobaltatetrahedrane

bis(1,3,2-dioxaborol-2-yl)dicobaltatetrahedrane

2,3-diphenylcycloprop-2-enecarboxylic acid
17825-58-0

2,3-diphenylcycloprop-2-enecarboxylic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 56 percent / Cu-bronze
2: 95 percent / KOH / tetrahydrofuran; methanol; H2O / 48 h / 20 °C
View Scheme
diphenyl acetylene
501-65-5

diphenyl acetylene

thiocyanato

thiocyanato

2,3-diphenylcycloprop-2-enecarboxylic acid
17825-58-0

2,3-diphenylcycloprop-2-enecarboxylic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: rhodium acetate dimer / CH2Cl2 / 35 °C
2: KOH / methanol / 4 h / Heating
View Scheme
diphenyl acetylene
501-65-5

diphenyl acetylene

2,3-diphenylcycloprop-2-enecarboxylic acid
17825-58-0

2,3-diphenylcycloprop-2-enecarboxylic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: Cu / 0.25 h / 105 °C
2: KOH / methanol; H2O / 1 h / Heating
View Scheme
2,3-diphenylcycloprop-2-enecarboxylic acid
17825-58-0

2,3-diphenylcycloprop-2-enecarboxylic acid

benzyl bromide
100-39-0

benzyl bromide

2,3-Diphenyl-cycloprop-2-enecarboxylic acid benzyl ester
99838-01-4

2,3-Diphenyl-cycloprop-2-enecarboxylic acid benzyl ester

Conditions
ConditionsYield
With N(Et)4(1+)*(2-pyrrolidone-anion) In N,N-dimethyl-formamide for 1h; Ambient temperature;99%
2,3-diphenylcycloprop-2-enecarboxylic acid
17825-58-0

2,3-diphenylcycloprop-2-enecarboxylic acid

2,3-diphenyl-2-cyclopropene-1-carbonyl chloride
6415-58-3

2,3-diphenyl-2-cyclopropene-1-carbonyl chloride

Conditions
ConditionsYield
With oxalyl dichloride In chloroform for 48h; Ambient temperature; further reagent: SOCl2;92%
With thionyl chloride90%
With thionyl chloride
N-hydroxyphthalimide
524-38-9

N-hydroxyphthalimide

2,3-diphenylcycloprop-2-enecarboxylic acid
17825-58-0

2,3-diphenylcycloprop-2-enecarboxylic acid

N-(2,3-diphenyl-2-cyclopropenylcarbonyloxy)phthalimide
234075-38-8

N-(2,3-diphenyl-2-cyclopropenylcarbonyloxy)phthalimide

Conditions
ConditionsYield
With dmap; dicyclohexyl-carbodiimide Substitution;87%
2,3-diphenylcycloprop-2-enecarboxylic acid
17825-58-0

2,3-diphenylcycloprop-2-enecarboxylic acid

N-(2,3-diphenylcycloprop-2-enyl)urea

N-(2,3-diphenylcycloprop-2-enyl)urea

Conditions
ConditionsYield
Stage #1: 2,3-diphenylcycloprop-2-enecarboxylic acid
Stage #2: With ammonia
86%
2,3-diphenylcycloprop-2-enecarboxylic acid
17825-58-0

2,3-diphenylcycloprop-2-enecarboxylic acid

methyl 1,5-diphenyl-2,3-diazabicyclo[3.1.0]hex-2-ene-endo-6-carboxylate

methyl 1,5-diphenyl-2,3-diazabicyclo[3.1.0]hex-2-ene-endo-6-carboxylate

methyl 1,5-diphenyl-2,3-diazabicyclo[3.1.0]hex-2-ene-exo-6-carboxylate

methyl 1,5-diphenyl-2,3-diazabicyclo[3.1.0]hex-2-ene-exo-6-carboxylate

Conditions
ConditionsYield
In diethyl ether at -10℃; for 480h;A 14%
B 73%
2,3-diphenylcycloprop-2-enecarboxylic acid
17825-58-0

2,3-diphenylcycloprop-2-enecarboxylic acid

1-oxo-2-(1-pyrrolin-1-ylium)-1H-indene-3-olat
15365-97-6, 109159-92-4

1-oxo-2-(1-pyrrolin-1-ylium)-1H-indene-3-olat

(±)-1′,3′-dioxo-1a,6b-diphenyl-1a,1′,3′,4,5,6,6a,6b-octahydro-1H-spiro[cyclopropa[a]pyrro-lizine-2,2′-indene]-1-carboxylic acid

(±)-1′,3′-dioxo-1a,6b-diphenyl-1a,1′,3′,4,5,6,6a,6b-octahydro-1H-spiro[cyclopropa[a]pyrro-lizine-2,2′-indene]-1-carboxylic acid

Conditions
ConditionsYield
In methanol at 25℃; for 10h; diastereoselective reaction;71%
L-leucine
61-90-5

L-leucine

indan-1,2,3-trione hydrate
485-47-2

indan-1,2,3-trione hydrate

2,3-diphenylcycloprop-2-enecarboxylic acid
17825-58-0

2,3-diphenylcycloprop-2-enecarboxylic acid

(±)-(1R,4R,5S,6R)-4-isobutyl-1',3'-dioxo-1,5-diphenyl-1',3'-dihydro-3-azaspiro[bicyclo[3.1.0]hexane-2,2'-indene]-6-carboxylic acid

(±)-(1R,4R,5S,6R)-4-isobutyl-1',3'-dioxo-1,5-diphenyl-1',3'-dihydro-3-azaspiro[bicyclo[3.1.0]hexane-2,2'-indene]-6-carboxylic acid

Conditions
ConditionsYield
In methanol; water for 10h; Reflux; diastereoselective reaction;68%
glycylglycine
556-50-3

glycylglycine

indan-1,2,3-trione hydrate
485-47-2

indan-1,2,3-trione hydrate

2,3-diphenylcycloprop-2-enecarboxylic acid
17825-58-0

2,3-diphenylcycloprop-2-enecarboxylic acid

(±)-(1R,4S,5S,6R)-4-[(carboxymethyl)carbamoyl]-1',3'-dioxo-1,5-diphenyl-1',3'-dihydro-3-azaspiro[bicyclo[3.1.0]hexane-2,2'-indene]-6-carboxylic acid

(±)-(1R,4S,5S,6R)-4-[(carboxymethyl)carbamoyl]-1',3'-dioxo-1,5-diphenyl-1',3'-dihydro-3-azaspiro[bicyclo[3.1.0]hexane-2,2'-indene]-6-carboxylic acid

Conditions
ConditionsYield
With acetic acid In methanol; water for 12h; Reflux; diastereoselective reaction;63%
indan-1,2,3-trione hydrate
485-47-2

indan-1,2,3-trione hydrate

2,3-diphenylcycloprop-2-enecarboxylic acid
17825-58-0

2,3-diphenylcycloprop-2-enecarboxylic acid

phenylglycin
2835-06-5

phenylglycin

(±)-(1R,4R,5S,6R)-1',3'-dioxo-1,4,5-triphenyl-1',3'-dihydro-3-azaspiro[bicyclo[3.1.0]hexane-2,2'-inden]-6-carboxylic acid

(±)-(1R,4R,5S,6R)-1',3'-dioxo-1,4,5-triphenyl-1',3'-dihydro-3-azaspiro[bicyclo[3.1.0]hexane-2,2'-inden]-6-carboxylic acid

Conditions
ConditionsYield
In methanol; water for 10h; Reflux; diastereoselective reaction;61%
2,3-diphenylcycloprop-2-enecarboxylic acid
17825-58-0

2,3-diphenylcycloprop-2-enecarboxylic acid

1,2-dophenylcyclopropenylim perchlorate
37647-36-2

1,2-dophenylcyclopropenylim perchlorate

Conditions
ConditionsYield
With perchloric acid; acetic anhydride In water at 0℃;59%
With perchloric acid; acetic anhydride at 0℃; Inert atmosphere;59%
With perchloric acid; acetic anhydride
2-amino-hexanoic acid
616-06-8

2-amino-hexanoic acid

indan-1,2,3-trione hydrate
485-47-2

indan-1,2,3-trione hydrate

2,3-diphenylcycloprop-2-enecarboxylic acid
17825-58-0

2,3-diphenylcycloprop-2-enecarboxylic acid

(±)-(1R,4R,5S,6R)-4-butyl-1',3'-dioxo-1,5-diphenyl-1',3'-dihydro-3-azaspiro[bicyclo[3.1.0]hexane-2,2'-indene]-6-carboxylic acid

(±)-(1R,4R,5S,6R)-4-butyl-1',3'-dioxo-1,5-diphenyl-1',3'-dihydro-3-azaspiro[bicyclo[3.1.0]hexane-2,2'-indene]-6-carboxylic acid

Conditions
ConditionsYield
In methanol; water for 10h; Reflux; diastereoselective reaction;51%
glycine-glycine-glycine
556-33-2

glycine-glycine-glycine

indan-1,2,3-trione hydrate
485-47-2

indan-1,2,3-trione hydrate

2,3-diphenylcycloprop-2-enecarboxylic acid
17825-58-0

2,3-diphenylcycloprop-2-enecarboxylic acid

(±)-4-({2-[(carboxymethyl)amino]-2-oxoethyl}carbamoyl)-1',3'-dioxo-1,5-diphenyl-1',3'-dihydro-3-azaspiro[bicyclo[3.1.0]hexane-2,2'-indene]-6-carboxylic acid

(±)-4-({2-[(carboxymethyl)amino]-2-oxoethyl}carbamoyl)-1',3'-dioxo-1,5-diphenyl-1',3'-dihydro-3-azaspiro[bicyclo[3.1.0]hexane-2,2'-indene]-6-carboxylic acid

Conditions
ConditionsYield
With acetic acid In methanol; water for 12h; Reflux; diastereoselective reaction;50%
2-aminooctanoic acid
644-90-6

2-aminooctanoic acid

indan-1,2,3-trione hydrate
485-47-2

indan-1,2,3-trione hydrate

2,3-diphenylcycloprop-2-enecarboxylic acid
17825-58-0

2,3-diphenylcycloprop-2-enecarboxylic acid

(±)-(1R,4R,5S,6R)-4-hexyl-1',3'-dioxo-1,5-diphenyl-1',3'-dihydro-3-azaspiro[bicyclo[3.1.0]hexane-2,2'-indene]-6-carboxylic acid

(±)-(1R,4R,5S,6R)-4-hexyl-1',3'-dioxo-1,5-diphenyl-1',3'-dihydro-3-azaspiro[bicyclo[3.1.0]hexane-2,2'-indene]-6-carboxylic acid

Conditions
ConditionsYield
In methanol; water for 10h; Reflux; diastereoselective reaction;42%
L-phenylalanine
63-91-2

L-phenylalanine

indan-1,2,3-trione hydrate
485-47-2

indan-1,2,3-trione hydrate

2,3-diphenylcycloprop-2-enecarboxylic acid
17825-58-0

2,3-diphenylcycloprop-2-enecarboxylic acid

(±)-(1R,4R,5S,6R)-4-benzyl-1',3'-dioxo-1,5-diphenyl-1',3'-dihydro-3-azaspiro[bicyclo[3.1.0]hexane-2,2'-indene]-6-carboxylic acid

(±)-(1R,4R,5S,6R)-4-benzyl-1',3'-dioxo-1,5-diphenyl-1',3'-dihydro-3-azaspiro[bicyclo[3.1.0]hexane-2,2'-indene]-6-carboxylic acid

Conditions
ConditionsYield
In methanol; water for 10h; Reflux; diastereoselective reaction;39%
L-valine
72-18-4

L-valine

indan-1,2,3-trione hydrate
485-47-2

indan-1,2,3-trione hydrate

2,3-diphenylcycloprop-2-enecarboxylic acid
17825-58-0

2,3-diphenylcycloprop-2-enecarboxylic acid

(±)-(1R,4R,5S,6R)-4-isopropyl-1',3'-dioxo-1,5-diphenyl-1',3'-dihydro-3-azaspiro[bicyclo[3.1.0]hexane-2,2'-indene]-6-carboxylic acid

(±)-(1R,4R,5S,6R)-4-isopropyl-1',3'-dioxo-1,5-diphenyl-1',3'-dihydro-3-azaspiro[bicyclo[3.1.0]hexane-2,2'-indene]-6-carboxylic acid

Conditions
ConditionsYield
In methanol; water for 10h; Reflux; diastereoselective reaction;22%
2,3-diphenylcycloprop-2-enecarboxylic acid
17825-58-0

2,3-diphenylcycloprop-2-enecarboxylic acid

phenylmagnesium bromide

phenylmagnesium bromide

1-Benzoyl-2,3-diphenyl-cycloprop-2-en
2892-41-3

1-Benzoyl-2,3-diphenyl-cycloprop-2-en

Conditions
ConditionsYield
(i) (COCl)2, (ii) /BRN= 4720968/, Et2O; Multistep reaction;
2,3-diphenylcycloprop-2-enecarboxylic acid
17825-58-0

2,3-diphenylcycloprop-2-enecarboxylic acid

cis,cis-1,2-Diphenyl-cyclopropan-carbonsaeure-(3)
123121-31-3

cis,cis-1,2-Diphenyl-cyclopropan-carbonsaeure-(3)

Conditions
ConditionsYield
With hydrogen; Lindlar's catalyst
2,3-diphenylcycloprop-2-enecarboxylic acid
17825-58-0

2,3-diphenylcycloprop-2-enecarboxylic acid

acetonitrile
75-05-8

acetonitrile

5-methyl-1,2-diphenyl-6-oxa-4-aza-spiro[2.4]hepta-1,4-dien-7-one
19402-90-5

5-methyl-1,2-diphenyl-6-oxa-4-aza-spiro[2.4]hepta-1,4-dien-7-one

Conditions
ConditionsYield
With triphenylmethyl perchlorate Ambient temperature;
2,3-diphenylcycloprop-2-enecarboxylic acid
17825-58-0

2,3-diphenylcycloprop-2-enecarboxylic acid

acecyclone
641-57-6

acecyclone

9-Carboxy-7,8,10,11-tetraphenyl-9H-cycloheptaacenaphthalin
106437-16-5

9-Carboxy-7,8,10,11-tetraphenyl-9H-cycloheptaacenaphthalin

Conditions
ConditionsYield
In xylene Heating;
2,3-diphenylcycloprop-2-enecarboxylic acid
17825-58-0

2,3-diphenylcycloprop-2-enecarboxylic acid

sodium methylate
124-41-4

sodium methylate

Methyl-N-(1,2-diphenyl-cyclopropenyl-(3))-carbamat
17825-60-4

Methyl-N-(1,2-diphenyl-cyclopropenyl-(3))-carbamat

Conditions
ConditionsYield
Multistep reaction;
2,3-diphenylcycloprop-2-enecarboxylic acid
17825-58-0

2,3-diphenylcycloprop-2-enecarboxylic acid

triphenylmethyl perchlorate

triphenylmethyl perchlorate

1.2-Diphenyl-3-triphenylmethyl-cyclopropenylium-perchlorat

1.2-Diphenyl-3-triphenylmethyl-cyclopropenylium-perchlorat

Conditions
ConditionsYield
With lithium carbonate
2,3-diphenylcycloprop-2-enecarboxylic acid
17825-58-0

2,3-diphenylcycloprop-2-enecarboxylic acid

1,2-Diphenyl-cyclopropenyl-(3)-hexafluorophosphat

1,2-Diphenyl-cyclopropenyl-(3)-hexafluorophosphat

Conditions
ConditionsYield
With hexafluorophosphoric acid; acetic anhydride
2,3-diphenylcycloprop-2-enecarboxylic acid
17825-58-0

2,3-diphenylcycloprop-2-enecarboxylic acid

dimethyl amine
124-40-3

dimethyl amine

N.N-Dimethyl-N'-<2.3-diphenyl-2-cyclopropenyl>-harnstoff
17825-62-6

N.N-Dimethyl-N'-<2.3-diphenyl-2-cyclopropenyl>-harnstoff

Conditions
ConditionsYield
Multistep reaction;
5,5-Dimethyl-1-pyrroline N-oxide
3317-61-1

5,5-Dimethyl-1-pyrroline N-oxide

2,3-diphenylcycloprop-2-enecarboxylic acid
17825-58-0

2,3-diphenylcycloprop-2-enecarboxylic acid

C22H22NO3

C22H22NO3

Conditions
ConditionsYield
In benzene Addition; UV-irradiation;
2,3-diphenylcycloprop-2-enecarboxylic acid
17825-58-0

2,3-diphenylcycloprop-2-enecarboxylic acid

methyl 3,5-diphenyl-1,4-dihydropyridazine-4-carboxylate
60220-49-7

methyl 3,5-diphenyl-1,4-dihydropyridazine-4-carboxylate

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 14 percent / diethyl ether / 480 h / -10 °C
2: sodium methoxide / methanol / 0.08 h / 20 °C
View Scheme
Multi-step reaction with 2 steps
1: 73 percent / diethyl ether / 480 h / -10 °C
2: 96 percent / sodium methoxide / methanol / 0.08 h / 20 °C
View Scheme
2,3-diphenylcycloprop-2-enecarboxylic acid
17825-58-0

2,3-diphenylcycloprop-2-enecarboxylic acid

6,6 dimethyl-3-(3-hydroxypropyl)thio-1-(thiazol-2-yl)-6,7-dihydro-2-benzothiophen-4(5H)-one

6,6 dimethyl-3-(3-hydroxypropyl)thio-1-(thiazol-2-yl)-6,7-dihydro-2-benzothiophen-4(5H)-one

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 14 percent / diethyl ether / 480 h / -10 °C
2: sodium methoxide / methanol / 0.08 h / 20 °C
3: 95 percent / aq. potassium permanganate / acetone / 0.5 h
View Scheme
Multi-step reaction with 3 steps
1: 73 percent / diethyl ether / 480 h / -10 °C
2: 96 percent / sodium methoxide / methanol / 0.08 h / 20 °C
3: 95 percent / aq. potassium permanganate / acetone / 0.5 h
View Scheme

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