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Basic Information
| CAS No.: | 1816-92-8 |
|---|---|
| Name: | Azidoacetic acid methyl ester |
| Article Data: | 63 |
| Molecular Structure: | |
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| Formula: | C3H5 N3 O2 |
| Molecular Weight: | 115.092 |
| Synonyms: | Aceticacid, azido-, methyl ester (7CI,9CI); Azidoacetic acid methyl ester; Methyl2-azidoacetate; Methyl azidoacetate |
| Density: | 1.182 g/mL at 25 °C |
| Boiling Point: | 35 °C |
| Flash Point: | 48℃ |
| Hazard Symbols: | Xi |
| Risk Codes: | 5-10-36/37/38 |
| Safety: | 26 |
| PSA: | 76.05000 |
| LogP: | -0.07754 |
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Synthetic route
Conditions
| Conditions | Yield |
|---|---|
| With sodium azide In dimethyl sulfoxide for 20h; | 100% |
| With sodium azide In N,N-dimethyl-formamide for 8h; Inert atmosphere; Reflux; | 97% |
| With sodium azide In methanol; water at 20 - 80℃; for 2.33333h; Inert atmosphere; | 96% |
Conditions
| Conditions | Yield |
|---|---|
| With sodium azide In N,N-dimethyl-formamide at 60℃; for 24h; | 99% |
| With sodium azide In acetonitrile for 20h; Heating; | 93% |
| With sodium azide In N,N-dimethyl-formamide at 20℃; for 4h; | 88% |
Conditions
| Conditions | Yield |
|---|---|
| With triflic azide; N-ethyl-N,N-diisopropylamine In dichloromethane | 44% |
| With imidazole-1-sulfonyl azide hydrochloride; copper(ll) sulfate pentahydrate; potassium carbonate In methanol; dichloromethane at 20℃; |
Conditions
| Conditions | Yield |
|---|---|
| In acetonitrile | 0.59 g (74%) |
Conditions
| Conditions | Yield |
|---|---|
| With sodium carbonate In water; toluene |
- 1816-92-8
Methyl azidoacetate
Conditions
| Conditions | Yield |
|---|---|
| With sodium azide In dimethyl sulfoxide at 20℃; for 10h; Inert atmosphere; |
- 1816-92-8
Methyl azidoacetate
- 1312289-70-5
2-(methoxycarbonyl)phenyl 3-O-prop-2-ynyl-1-thio-β-D-galactopyranoside
- 1312289-73-8
C20H25N3O9S
Conditions
| Conditions | Yield |
|---|---|
| With copper(l) iodide; N-ethyl-N,N-diisopropylamine In tetrahydrofuran at 20℃; Inert atmosphere; | 100% |
- 1816-92-8
Methyl azidoacetate
- 54060-30-9
3-acetylenephenylamine
Conditions
| Conditions | Yield |
|---|---|
| With copper(ll) sulfate pentahydrate; sodium L-ascorbate In tetrahydrofuran; water at 20℃; for 1h; Inert atmosphere; | 100% |
| With copper(l) iodide; sodium L-ascorbate In water; tert-butyl alcohol at 20℃; Reagent/catalyst; Solvent; | 100 %Chromat. |
Conditions
| Conditions | Yield |
|---|---|
| With copper(II) sulfate; sodium L-ascorbate In water at 20℃; Reagent/catalyst; Solvent; | 100% |
Conditions
| Conditions | Yield |
|---|---|
| With copper(II) sulfate; sodium L-ascorbate In water at 20℃; Reagent/catalyst; Solvent; | 100% |
