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1907-33-1

Basic Information
CAS No.: 1907-33-1
Name: Lithium tert-butoxide
Article Data: 20
Molecular Structure:
Molecular Structure of 1907-33-1 (Lithium tert-butoxide)
Formula: C4H9LiO
Molecular Weight: 80.0559
Synonyms: 2-Propanol,2-methyl-, lithium salt (9CI);Lithium tert-butoxide (6CI,7CI);tert-Butylalcohol, lithium salt (8CI);(1,1-Dimethylethoxy)lithium;2-Methyl-2-propanollithium salt;Lithium t-butoxide;Lithium tert-butanolate;Lithiumtert-butylate;tert-Butanol lithium salt;tert-Butoxylithium;
EINECS: 217-611-5
Density: 0.89 g/mL at 20 °C
Melting Point: °C
Boiling Point: 84.6 °C at 760 mmHg
Flash Point: 11.7 °C
Solubility: vigorous reaction with water
Appearance: clear yellow to brown solution
Hazard Symbols: FlammableF, CorrosiveC, DangerousN
Risk Codes: 11-19-34-37-35-14-67-65-62-51/53-48/20
Safety: 26-36/37/39-45-61-62-6A-43E-16-7/8-43-33
Transport Information: UN 3206 4.2/PG 2
PSA: 23.06000
LogP: 1.21540
Synthetic route
109-72-8, 29786-93-4

n-butyllithium

3965-63-7

tert-butylperoxytrimethylsilane

A

106-98-9

1-butylene

B

111-65-9

octane

C

1000-63-1

n-butyl tert-butyl ether

D

1825-65-6

butoxytrimethylsilane

E

2004-14-0

lithium trimethylsilanolate

F

1907-33-1

lithium tert-butoxide

Conditions
ConditionsYield
In benzene Mechanism; other solvent;
109-72-8, 29786-93-4

n-butyllithium

3965-63-7

tert-butylperoxytrimethylsilane

A

106-98-9

1-butylene

B

1000-63-1

n-butyl tert-butyl ether

C

2004-14-0

lithium trimethylsilanolate

D

1907-33-1

lithium tert-butoxide

Conditions
ConditionsYield
In benzene Further byproducts given;
109-72-8, 29786-93-4

n-butyllithium

3965-63-7

tert-butylperoxytrimethylsilane

A

111-65-9

octane

B

1000-63-1

n-butyl tert-butyl ether

C

2004-14-0

lithium trimethylsilanolate

D

1907-33-1

lithium tert-butoxide

Conditions
ConditionsYield
In benzene Further byproducts given;
109-72-8, 29786-93-4

n-butyllithium

3965-63-7

tert-butylperoxytrimethylsilane

A

1000-63-1

n-butyl tert-butyl ether

B

1825-65-6

butoxytrimethylsilane

C

2004-14-0

lithium trimethylsilanolate

D

1907-33-1

lithium tert-butoxide

Conditions
ConditionsYield
In chloroform Further byproducts given;
In benzene Further byproducts given;
109-72-8, 29786-93-4

n-butyllithium

3965-63-7

tert-butylperoxytrimethylsilane

A

1000-63-1

n-butyl tert-butyl ether

B

2004-14-0

lithium trimethylsilanolate

C

1907-33-1

lithium tert-butoxide

D

106-97-8

n-butane

Conditions
ConditionsYield
In benzene Further byproducts given;
3965-63-7

tert-butylperoxytrimethylsilane

920-36-5, 90269-51-5

(2-methylpropyl)lithium

A

592-13-2

2,5-dimethylhexane

B

33021-02-2

1-(1,1-dimethylethoxy)-2-methylpropane

C

2004-14-0

lithium trimethylsilanolate

D

1907-33-1

lithium tert-butoxide

Conditions
ConditionsYield
In benzene Further byproducts given;
3965-63-7

tert-butylperoxytrimethylsilane

920-36-5, 90269-51-5

(2-methylpropyl)lithium

A

75-28-5

Isobutane

B

33021-02-2

1-(1,1-dimethylethoxy)-2-methylpropane

C

2004-14-0

lithium trimethylsilanolate

D

1907-33-1

lithium tert-butoxide

Conditions
ConditionsYield
In benzene Further byproducts given;
3965-63-7

tert-butylperoxytrimethylsilane

920-36-5, 90269-51-5

(2-methylpropyl)lithium

A

33021-02-2

1-(1,1-dimethylethoxy)-2-methylpropane

B

18269-50-6

isobutoxytrimethylsilane

C

2004-14-0

lithium trimethylsilanolate

D

1907-33-1

lithium tert-butoxide

Conditions
ConditionsYield
In benzene Further byproducts given;
3965-63-7

tert-butylperoxytrimethylsilane

920-36-5, 90269-51-5

(2-methylpropyl)lithium

A

592-13-2

2,5-dimethylhexane

B

33021-02-2

1-(1,1-dimethylethoxy)-2-methylpropane

C

18269-50-6

isobutoxytrimethylsilane

D

2004-14-0

lithium trimethylsilanolate

E

115-11-7

isobutene

F

1907-33-1

lithium tert-butoxide

Conditions
ConditionsYield
In benzene Mechanism; other solvent;
3965-63-7

tert-butylperoxytrimethylsilane

920-36-5, 90269-51-5

(2-methylpropyl)lithium

A

33021-02-2

1-(1,1-dimethylethoxy)-2-methylpropane

B

2004-14-0

lithium trimethylsilanolate

C

115-11-7

isobutene

D

1907-33-1

lithium tert-butoxide

Conditions
ConditionsYield
In benzene Further byproducts given;
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Chemistry

Molecular structure of Lithium tert-butoxide (CAS NO.1907-33-1) is:

Product Name: Lithium tert-butoxide
CAS Registry Number: 1907-33-1
IUPAC Name: lithium 2-methylpropan-2-olate
Molecular Weight: 80.05466 [g/mol]
Molecular Formula: C4H9LiO
H-Bond Donor: 0
H-Bond Acceptor: 1 
EINECS: 217-611-5
Density: 0.89 g/mL at 20 °C
Storage temp.: Flammables area
Water Solubility: vigorous reaction
Sensitive: Moisture Sensitive
Flash Point: 11.7 °C
Enthalpy of Vaporization: 37.89 kJ/mol
Boiling Point: 84.6 °C at 760 mmHg
Vapour Pressure: 46 mmHg at 25°C
Product Categories: LithiumChemical Synthesis;Micro/Nanoelectronics;Organic Bases;Solution Deposition Precursors;Synthetic Reagents

Toxicity Data With Reference

Organism Test Type Route Reported Dose (Normalized Dose) Effect Source
mouse LD50 oral 1682mg/kg (1682mg/kg) BEHAVIORAL: SOMNOLENCE (GENERAL DEPRESSED ACTIVITY)

LUNGS, THORAX, OR RESPIRATION: RESPIRATORY DEPRESSION
Toksikologicheskii Vestnik. Vol. (3), Pg. 37, 1996.

Safety Profile

Moderately toxic by ingestion. When heated to decomposition it emits toxic vapors of Li.
Hazard Codes:
F: Flammable
N: Dangerous for the environment
C: Corrosive
Risk Statements about Lithium tert-butanolate (1907-33-1):
R11 Highly flammable. 
R14 Reacts violently with water. 
R35 Causes severe burns. 
R48/20 Harmful : danger of serious damage to health by prolonged exposure through inhalation. 
R51/53 Toxic to aquatic organisms, may cause long-term adverse effects in the aquatic environment. 
R62 Possible risk of impaired fertility. 
R65 Harmful: may cause lung damage if swallowed. 
R67 Vapours may cause drowsiness and dizziness
Safety Statements about Lithium tert-butanolate (1907-33-1):
S9 Keep container in a well-ventilated place. 
S16 Keep away from sources of ignition - No smoking. 
S29 Do not empty into drains. 
S33 Take precautionary measures against static discharges. 
S36/37/39 Wear suitable protective clothing, gloves and eye/face protection. 
S45 In case of accident or if you feel unwell, seek medical advice immediately (show the label where possible).  
RIDADR: UN 3206 4.2/PG 2
WGK Germany: 3
RTECS: UB8520000
F: 3-10
TSCA: Yes
HazardClass: 4.2
PackingGroup: III

Specification

 Lithium tert-butoxide , its cas register number is 1907-33-1. It also can be called 2-Methyl-2-propanol lithium salt ; Lithium tert-butanolate ; Lithium tert-butylate ; tert-Butoxylithium ; tert-Butyl alcohol, lithium salt ; 2-Propanol, 2-methyl-, lithium salt ; 2-Propanol, 2-methyl-, lithium salt (1:1) ; Lithium 2-methylpropan-2-olate .It is a clear yellow to brown solution.